• Title/Summary/Keyword: Temperature curing

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A Study on the Physical Property of Epoxy Resin Due to After-Curing Condition (후경화 조건에 따른 에폭시 수지의 물성에 관한 연구)

  • Han, Jeong-Young;Kim, Myung-Hun;Kang, Sung-Soo
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.21 no.6
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    • pp.976-981
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    • 2012
  • In this study, hardness, microstructure and temperature of glass transition are measured respectively by using SEM (Scanning electron microscope) and DSC (Differential scanning calorimeter) to analyze the effects on material properties by after-curing in the epoxy resin. As the result of hardness test according to the after-curing conditions, the higher the temperature of after-curing, hardness and heat resistance are, the higher hardness is. As a result of microstructure for each specimen by SEM, it could be confirmed that the specimen with after-curing has more dense fracture surface. It is also found that temperatures of glass transitions by DSC are comparatively higher in the specimens with after-curing, and the differences between after-curing conditions are negligible.

The Plastic Cracking Properties of Fly Ash Concrete with Various Curing Conditions (양생조건에 따른 플라이애쉬 콘크리트의 소성수축균열 특성)

  • Nam, Jae-Hyun;Park, Jong-Hwa
    • Journal of the Korea Institute of Building Construction
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    • v.7 no.1 s.23
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    • pp.91-98
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    • 2007
  • In this study, the property and plastic cracking pattern of concrete were compared and analyzed with the replacement ratio of fly ash 0, 5, 10, 15, 20% by cement weight. And curing conditions of concrete were given variously such as indoors(with wind speed as 0, 300, 500m/min), outdoors and chamber. The hydration temperature had a tendency to decrease as the replacement ratio of fly ash increased, and in the case of the wind speed 0m/min, it was showed that the moment that the amount of evaporation of water from surface of reference concrete was more than the volume of bleeding was 90 min since casting concrete. The time that the crack initiated had a tendency to be more quickly as the replacement ratio of fly ash increased. The number, length, width and area of crack in the indoor curing, exposed outdoor curing, enclosed outdoor curing had a tendency to decrease as the replacement ratio of fly ash increased. The crack had a tendency to decrease in sequence of exposed outdoor, enclosed outdoor curing, indoors curing. The outbreak of cracking by the change of temperature and humidity was affected by relative humidity more than temperature and the cracking had a tendency to increase as relative humidity lowered.

Relationship between Compressive Strength of Geo-polymers and Pre-curing Conditions

  • Kim, Hyunjung;Kim, Yooteak
    • Applied Microscopy
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    • v.43 no.4
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    • pp.155-163
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    • 2013
  • Meta-kaolin (MK) and blast furnace slag (BS) were used as raw materials with NaOH and sodium silicate as alkali activators for making geo-polymers. The compressive strength with respect to the various pre-curing conditions was investigated. In order to improve the recycling rate of BS while still obtaining high compressive strength of the geo-polymers, it was necessary to provide additional CaO to the MK by adding BS. The specimens containing greater amounts of BS can be applied to fields that require high initial compressive strength. Alkali activator(s) are inevitably required to make geo-polymers useful. High temperature pre-curing plays an important role in improving compressive strength in geo-polymers at the early stage of curing. On the other hand, long-term curing produced little to no positive effects and may have even worsened the compressive strength of the geo-polymers because of micro-structural defects through volume expansion by high temperature pre-curing. Therefore, a pre-curing process at a medium range temperature of $50^{\circ}C$ is recommended because a continuous increase in compressive strength during the entire curing period as well as good compressive strength at the early stages can be obtained.

Quality Inspection for Cast-In-Place Concrete with the Device to Record Curing Temperature (양생온도 이력 기록장치를 이용한 현장타설 콘크리트의 품질검사)

  • Cho, Yeong-Kweon;Kim, Kwan-Ho;Kim, Meyong-Won;Lee, Jun-Gu;Yoo, Jung-Hoon
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.11a
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    • pp.351-354
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    • 2005
  • Quality of concrete required to achieve the desired levels of strength and durability depend on the effectiveness of the curing method. During cold weather, the concrete at the time of placement should be taken to prevent damage to concrete due to freezing. Since the cement-water reaction is exothermic by nature, the temperature within mass concrete can be quite high. The temperature control for massive sections should be taken more careful than for shallow sections. However, in the constructing hydraulic structures, the curing temperature control for concrete had been very difficult to be taken in a proper way because the conditions constructing them are poor and contractors are small enterprises. For several. reasons including above, Rural Research Institute has developed a device and program for recording curing temperature history in cold weather concrete and mass. As there are two major advantages of the device, namely cheapness and availability, this program and device has been recommended to the use of curing temperature control in cold weather concrete and mass.

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Temperature Properties of Vertical Reinforcements in Wall Structures in Relation to the Different Methods of Bubble Sheet Installation in Winter (겨울철 버블시트 포설방법 변화에 따른 벽식구조 수직철근의 온도 특성)

  • Kim, Tae-Woo;Lee, Jea-Hyeon;Kyung, Yeong-Hyeok;Lee, Jong-Gyo;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.05a
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    • pp.11-12
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    • 2017
  • This study aims to analyze the properties of the temperature change in vertical reinforcements in outdoor wall structures in winter in relation to the different methods of bubble sheet installation, and to subsequently determine the possibility of initial frost damage to the concrete as a result of low temperature. As for the experimental variables, double bubble sheets were used as curing materials, and the curing method was to model the part where the slab and the wall intersect and the rebar is exposed, and to measure the change of temperature around the exposed rebar in accordance with the change of the coating curing. It was found that by employing curing method B, which is to install the bubble sheet between the vertical reinforcements, the most vulnerable area, which is 50mm below(④) the surface of the concrete, would be lowered to sub-zero temperature 20 hours later than when using curing method A, and that therefore it is more effective to install the bubble sheet between the vertical reinforcements for the prevention of initial frost damage.

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Analysis of cure behavior of low temperature curing liquid silicone rubber (LSR) for multi-material injection molding (이중사출 성형을 위한 저온 경화 액상실리콘고무 (LSR)의 경화 거동 분석)

  • Hyeong-min Yoo
    • Design & Manufacturing
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    • v.17 no.1
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    • pp.1-5
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    • 2023
  • In multi-material injection molding, since two or more materials with different process conditions are used, it is essential to maximize process efficiency by operating the cooling or heating system to a minimum. In this study, Liquid silicone rubber (LSR) that can be cured at a low temperature suitable for the multi-material injection molding was selected and the cure behavior according to the process conditions was analyzed through differential scanning calorimetry (DSC). Dynamic measurement results of DSC with different heating rate were obtained, and through this, the total heat of reaction when the LSR was completely cured was calculated. Isothermal measurement results of DSC were derived for 60 minutes at each temperature from 80 ℃ to 110 ℃ at 10 ℃ intervals, and the final degree of cure at each temperature was calculated based on the total heat of reaction identified from the Dynamic DSC measurement results. As the result, it was found that when the temperature is lowered, the curing start time and the time required for the curing reaction increase, but at a temperature of 90 ℃ or higher, LSR can secure a degree of cure of 80% or more. However, at 80 ℃., it was found that not only had a relatively low degree of curing of about 60%, but also significantly increased the curing start time. In addition, in the case of 110 ℃, the parameters were derived from experimental result using the Kamal kinetic model.

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Experimental Study of Strength Development in High Flow Concrete as following of Curing Temperature (초기 재령에서의 양생 온도 조건에 따른 고유동 콘크리트의 조기강도 발현 성상에 관한 실험적 연구)

  • 이도범;김효락;박지훈;최일호
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.19-22
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    • 2003
  • This study is carried out (1) checking the development of compressive strength of high flowing concrete at early age, changing water-binder ratio, curing temperature, and type of aggregate, and (2) suggesting basic date that helping cost and schedule plan in future construction. As the result of this study, we find that high curing temperature is effective for the development of compressive strength of concrete at early age on the condition of each water-binder ratio, and after making the compressive prediction formula related to the curing temperature by maturity, the result of the formular is similar to the temperature-compressive strength-age measured data

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The Measurement of Exothermic Temperature During Polymerization of Various Direct Resins. (각종 치과용 다이렉트 레진의 중합 반응시 열 측정)

  • Yun, Joung-Hyun
    • The Journal of the Korean dental association
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    • v.11 no.1
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    • pp.37-40
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    • 1973
  • The auther measured exothermic tempreature of the 5 kinds of direct resins during polymerization. Direct resins were mixed into the rubber cup(550-600㎣ in volume) with grass rod at room temperature (23.6℃) for 30 seconds and thermometer was placed approximately at the geometric center of the resin mass in the rubber cup. Polymer-monomer ratio was determined by instruction of the packages. The results were as follows. 1) The heat generated during polymerization was under 47.3℃. 2) The time at which the highest temperature is reached during polymerization was within 20.5 minutes. 3) Slow curing resins produced lower heat than quick curing resins and quick curing resins presented higher temperature than slow curing resins. 4) The highest temperature was sustained momentarily.

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The Effect of Heat Curing Methods on the Protection against Frost Damage at Early Age of the Concrete Under Extremely Cold Climate

  • Jung, Eun-Bong;Shin, Hyun-Sup;Han, Min-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.13 no.6
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    • pp.513-521
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    • 2013
  • This study aimed to examine whether heat curing methods of concrete subjected to $-10^{\circ}C$ could be effective by varying the combination of heating cable and surface heat insulations. Three different concrete specimens incorporating 30% fly ash with 50% W/B were fabricated to simulate wall, column and slab members with dimensions of $1600{\times}800{\times}200$ mm for slab, $800{\times}600{\times}200$ mm for wall and $800{\times}800{\times}800$ mm for column. For heat curing combinations, Type-1 specimens applied PE film for slab, plywood for wall and column curing. Type-2 specimens applied double layer bubble sheet (2LB) and heating coil for slab, and 50 mm styrofoam for wall and column curing. Type-3 specimen applied 2LB for slab, electrical heating mat for wall and column inside heating enclosure. The test results revealed that the temperature of Type 1 specimen dropped below $0^{\circ}C$ beginning at 48 hours after placement due to its poor heat insulating capability. Type 2 and 3 specimens maintained a temperature of around $5{\sim}10^{\circ}C$ after placement due to favorable heat insulating and thermal resistance.

Effect of cyclic Change of Wet Bulb Temperature During Yellowing Stage on Chemical Properties of Flue-Cured Tobacco (황색종 cyclic 건조엽의 화학성분 특성)

  • Lee, Chul-Hwan;Jin, Jeong-Eui;Han, Chul-Soo
    • Journal of the Korean Society of Tobacco Science
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    • v.20 no.1
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    • pp.19-25
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    • 1998
  • The bulk curing experiment to the improve the quality of flue-cured leaves were carried out to evaluate relationship between cyclic curing and conventional curing method. We studied the effect of the cyclic change of wet bulb temperature at the yellowing stage of flue curing on chemical properties of cured leaves. The wet bulb temperature was automatically controlled between preset high($38^{\circ}C$) and low point ($35^{\circ}C$) everyone hour cyclically during 12 hours after starting luring. As a result, the acceleration of the increase in the chemical properties of cured leaves were observed. As to the chemical properties, there was decreased in citric acid, increased in malic acid of the nonvolatile organic acids and all higher fatty acids content of leaves cured by this method compared with in that of conventional curing method, while a major chemical compounds in relation to aromatic essence of cigarette smoke in essential oil components of lured leaves was mostly higher in this method than those of conventional ones, and it was evaluated that there was decreased in CO, TPM, Tar, and $CO_2$ content of the cigarette smoke comparing to the conventional luring method.

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