• Journal of Powder Materials
• /
• v.27 no.5
• /
• pp.414-419
• /
• 2020

In the present study, we investigated the austenite stability of a sintered Fe-based nanocrystalline alloy. The volume fraction of austenite was measured based on the X-ray diffraction data of sintered Fe-based nanocrystalline alloys, which were prepared by high-energy ball milling and spark plasma sintering. The sintered alloy samples showed a higher volume fraction of austenite at room temperature as compared to the equilibrium volume fraction of austenite obtained using thermodynamic calculations, which resulted from the nanosized crystalline structure of the sintered alloy. It was proved that the austenite stability of the sintered Fe-based alloy increased with a rise in the amount of austenite stabilizing elements such as Mn, Ni, and C; however, it increased more effectively with a decrease in the actual grain size. Furthermore, we proposed a new equation to predict the martensite starting temperature for sintered Fe-based alloys.

• Electrical & Electronic Materials
• /
• v.8 no.2
• /
• pp.196-203
• /
• 1995

We presented Tungsten and Tungsten Nitride thin films deposited by RF and DC sputtering. It deposited at various conditions that determining the resistivity and sheet resistivity by stabilizing the basic theory. We investigated properties of the resistivity and sheet resistivity of these films under various conditions, temperature of substrate, flow rate of the argon gas and content of nitrogen from nitrogen-argon mixtures. As the temperature of substrate increased and the flow rate of the argon gas decreased, the resistivities of these films reduced by structural transformation. We found that these resistivities were depend on the temperature of substrate, flow rate and electric power. Very highly resistive tungsten films obtained at 10W RF power. On the contrary, we found that films deposited by DC sputtering, from which very lowly resistive tungsten films were obtained. Tungsten nitride thin films deposited by reactive DC sputtering and the resistivities of these films increased as the content of nitrogen gas increased from nitrogen-argon mixture. And also we found the results show very good agreement, compared with experimental data.

• Journal of Veterinary Clinics
• /
• v.22 no.3
• /
• pp.259-263
• /
• 2005

To compare cardiopulmonary effects and recovery between total intravenous anesthesia (TIVA) with propofol (PRO group, n=5) and volatile induction/maintenance anesthesia (VIMA) with isoflurane (ISO group, n=5), we investigated changes of heart rate, $SpO_2$, arterial pressure, rectal temperature and respiratory rate during 60 minute anesthesia and 40 minute recovery period in beagle dogs, and investigated recovery (extubation, head lift, sternal position and righting) after 60 minute anesthesia. Rectal temperature was significantly low in ISO group (p<0.05) from 10 to 100 minute. Heart rate was significantly low in ISO group (p<0.05) at 40, 50, 60 minute. Respiratory rate was significantly low in PRO group (p<0.05) at induction and 70 minute. $SpO_2$ tendency was similar. Systolic arterial pressure (SAP) was significantly low in ISO group (p<0.05) at induction and during anesthesia. Recovery was similar in two groups. We concluded that TIVA with propofol is useful in stabilizing rectal temperature and arterial pressure during anesthesia and provide fast and stable recovery.

• Journal of Powder Materials
• /
• v.21 no.1
• /
• pp.55-61
• /
• 2014

Fe-Cr-Al powder porous metal was manufactured by using new electro-spray process. First, ultra-fine fecralloy powders were produced by using the submerged electric wire explosion process. Evenly distributed colloid (0.05~0.5% powders) was dispersed on Polyurethane foam through the electro-spray process. And then degreasing and sintering processes were conduced. In order to examine the effect of cell size ($200{\mu}m$, $450{\mu}m$, $500{\mu}m$) in process, pre-samples were sintered for two hours at temperature of $1450^{\circ}C$, in $H_2$ atmospheres. A 24-hour thermo gravimetric analysis test was conducted at $1000^{\circ}C$ in a 79% $N_2$ + 21% $O_2$ to investigate the high temperature oxidation behavior of powder porous metal. The results of the high temperature oxidation tests showed that oxidation resistance increased with increasing cell size. In the $200{\mu}m$ porous metal with a thinner strut and larger specific surface area, the depletion of the stabilizing elements such as Al and Cr occurred more quickly during the high-temperature oxidation compared with the 450, $500{\mu}m$ porous metals.

• Journal of the Korean Society for Heat Treatment
• /
• v.26 no.3
• /
• pp.105-112
• /
• 2013

The microstructural changes of Fe-20Mn-12Cr-1Cu alloy have been studied during high temperature gas nitriding (HTGN) at the range of $1000^{\circ}C{\sim}1150^{\circ}C$ in an atmosphere of nitrogen gas. The mixed microstructure of austenite and ${\varepsilon}$-martensite of as-received alloy was changed to austenite single phase after HTGN treatment at the nitrogen-permeated surface layer, however the interior region that was not affected nitrogen permeation remained the structure of austenite and ${\varepsilon}$-martensite. With raising the HTGN treatment temperature, the concentration and permeation depth of nitrogen, which is known as the austenite stabilizing element, were increased. Accordingly, the depth of austenite single phase region was increased. The outmost surface of HTGN treated alloy at $1000^{\circ}C$ appeared Cr nitride. And this was in good agreement with the thermodynamically calculated phase diagram. The grain growth was delayed after HTGN treatment temperature ranges of $1000^{\circ}C{\sim}1100^{\circ}C$ due to the grain boundary precipitates. For the HTGN treatment temperature of $1150^{\circ}C$, the fine grain region was shown at the near surface due to the grain boundary precipitates, however, owing to the depletion of grain boundary precipitates, coarse grain was appeared at the depth far from the surface. This depletion may come from the strong affinity between nitrogen and substitutional element of Al and Ti leading the diffusion of these elements from interior to surface. Because of the nitrogen dissolution at the nitrogen-permeated surface layer by HTGN treatment, the surface hardness was increased above 150 Hv compared to the interior region that was consisted with the mixed microstructure of austenite and ${\varepsilon}$-martensite.

• 한국연소학회:학술대회논문집
• /
• 2004.11a
• /
• pp.79-84
• /
• 2004

For the non-premixed interacting jet flames, it has been reported that if eight small nozzles are arranged along the circle of 40 $^{\sim}$ 72 times the diameter of single jet, the flames are not extinguished over 2oom/s. In this research, experiments were extended to the partially premixed cases to reduce both flame temperature and NOx emission. Nine nozzles were used- eight was evenly located along the perimeter of the imaginary circle and one at the geometric centre. The space between nozzles, S, the equivalence ratio, ${\Phi}$, the exit velocity and the role of the jet from the centre nozzle were considered. Normally, flame was lifted and flame base was located inside the imaginary circle made by the nozzle. As nozzles went away from each other, blowout velocity increased and then decreased. The maximum blowout velocity diminished with the addition of air to the fuel stream. When the fuel and/or oxidizer were not fed through the centre nozzle, the maximum blowout velocity obtained by varying Sand ${\Phi}$ was around 160m/s. Optimum nozzle separation distance at which peak blowout velocity obtained also decreased with ${\Phi}$ decrease. Flame base became leaner as approaching to the blowout. It seemed that lots of air was supplied to the flame stabilizing region by the entrainment and partially premixing. To approve this idea and to enhance the blowout velocity, fuel was supplied to the centre region. With the small amount of fuel through the centre nozzle, partially premixed flame could be sustained till sonic velocities. It seemed that the stabilizing mechanism in partially premixed interacting flame was different from that of non-premixed case because one was stabilized by the fuel supply through the centre nozzle but the other destabilized.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.29 no.1 s.232
• /
• pp.71-79
• /
• 2005

For the non-premixed interacting jet flames, it has been reported that if eight small nozzles are arranged along the circle of $40{\sim}72$ times the diameter of single jet, the flames are not extinguished even in 200m/s. In this research, experiments were extended to the partially premixed cases to reduce both flame temperature and NOx emission. Nine nozzles were used- eight was evenly located along the perimeter of the imaginary circle and one at the geometric centre. The space between nozzles, S, the equivalence ratio, ${\phi}$, the exit velocity and the role of the jet from the centre nozzle were considered. Normally, flame was lifted and flame base was located inside the imaginary circle made by the nozzle. As nozzles went away from each other, blowout velocity increased and then decreased. The maximum blowout velocity diminished with the addition of air to the fuel stream. When the fuel and/or oxidizer were not fed through the centre nozzle, the maximum blowout velocity obtained by varying S and ${\phi}$ was around 160m/s. Optimum nozzle separation distance at which peak blowout velocity obtained also decreased with ${\phi}$ decrease. Flame base became leaner as approaching to the blowout. It seemed that lots of air was supplied to the flame stabilizing region by the entrainment and partially premixing. To approve this idea and to enhance the blowout velocity, fuel was supplied to the centre region. With the small amount of fuel through the centre nozzle, partially premixed flame could be sustained till sonic velocities. It seemed that the stabilizing mechanism in partially premixed interacting flame was different from that of non-premixed case because one was stabilized by the fuel supply through the centre nozzle but the other destabilized.

• Journal of the Korean Society of Food Science and Nutrition
• /
• v.32 no.6
• /
• pp.806-811
• /
• 2003

Effects of pH, temperature, light, sugars, organic acids, metal ions, ascorbic acid, thiamine nicotinic acid and pyridoxine on the stability of the color of the cranberry solution were investigated. The pH had marked influences on the color of the cranberry solution: i.e., the color of the cranberry solution was more intense at low pH. It showed characteristic bathochromic shift as the pH of the solution increased. The half-lives of olor value were 34 days at 37$^{\circ}C$, 91 mins at 9$0^{\circ}C$ and 29 mins at 12$0^{\circ}C$. Light gave an adverse effect to the stability of the color. The color degradation can be minimized by shielding the light from the cranberry solution. Among the sugars tested, fructose was the most deleterious followed by sucrose, galactose, maltose and glucose. Fumaric acid was found to be the most effective in stabilizing the color followed by citric acid, malic acid, acetic acid, while tartaric acid was found to be deleterious. Among the metal ions tested N $a^{+}$ and $Mg^{2+}$ were found to be effective in stabilizing the color, while M $n^{2+}$ was found to be the most deleterious followed by F $e^{2+}$, $K^{+}$ and $Ca^{2+}$. Ascorbic acid was found to be deleterious considerably followed by thiamine, while nicotinic acid and pyridoxine were found to be effective in stabilizing the color feebly.or feebly.

• Journal of Powder Materials
• /
• v.18 no.2
• /
• pp.122-128
• /
• 2011

This study investigated the high temperature oxidation behavior of Ni-22.4%Fe-22%Cr-6%Al (wt.%) porous metal. Two types of open porous metals with different pore sizes of 30 PPI and 40 PPI (pore per inch) were used. A 24-hour TGA test was conducted at three different temperatures of $900^{\circ}C$, $1000^{\circ}C$ and $1100^{\circ}C$. The results of the BET analysis revealed that the specific surface area increased as the pore size decreased from 30 PPI to 40 PPI. The oxidation resistance of porous metal decreased with decreasing pore size. As the temperature increased, the oxidation weight gain of the porous metal also increased. Porous metals mainly created oxides such as $Al_2O_3$, $Cr_2O_3$, $NiAl_2O_4$, and $NiCr_2O_4$. In the 40 PPI porous metal with small pore size and larger specific surface area, the depletion of stabilizing elements such as Al and Cr occurred more quickly during oxidation compared to the 30 PPI porous metal. Ni-Fe-Cr-Al porous metal's high-temperature oxidation micro-mechanism was also discussed.

• Journal of the Korea Academia-Industrial cooperation Society
• /
• v.15 no.6
• /
• pp.3827-3831
• /
• 2014

This paper aims to solve the problem deterioration of power fuses. The deterioration of a power fuse is a cause of failure misoperation by a normal current flowing reduplicatively to fuse the element. An extension survey of a load feature rerating power fuse examined the power fuse deterioration removal, the cause of the deterioration of the power fuse, the front-after, and the thermal variation of the inside transformer room electric power equipment. The transformer showed an average improvement of $6[^{\circ}C]$. The temperature of the electrical line showed $7{\sim}8[^{\circ}C]$ improvement. The static condenser and direct reactor was $2{\sim}3[^{\circ}C]$ high-state maintenance the temperature and equipment syntonization relationship. In the subject of study $0.5{\sim}1.0[^{\circ}C]$ stabilizing three phase power fuse temperature differential was. Suggestion in the transformer room environment power equipment between the cause temperature happen elimination to deterioration of power fuse and temperature rise control.