• Title/Summary/Keyword: Temperature Aging

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Phase Transformation Behavior on Aging Treatment in CuAINi Shape Memory Alloy (CuAINi 형상기억합금의 시효처리에 따른 상변태 거동)

  • Yang, G.S.;Kang, J.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.4
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    • pp.213-222
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    • 1993
  • This research was performed to investigate the transformation behavior and shape memory effect of Cu-13.5Al-4.5Ni(wt%) alloy with various aging temperature and time. The results obtained in this study are as follows: Transformation temperature was very increased when aging temperature is at $250^{\circ}C$. The variation of transformation temperature in first reverse transformation cycle and second was very significant, but there was little difference in case of 2nd and 3rd. Transformation temperature at various aging temperature was increased with increasing of aging temperature and time. Microvickers hardness was increased with increasing of aging temperature and time. It was found that ${\alpha}$ and ${\gamma}_2$ phase were created by aging of long time at high temperature.

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Multi-phase Accelerating Test Method of Thermal Aging Considering Heat Generation of Electric Equipment (전기기기의 발열을 고려한 다단계 가속열노화 방법)

  • Lim, Byung-Ju;Park, Chang-Dae;Chung, Kyung-Yul
    • The KSFM Journal of Fluid Machinery
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    • v.16 no.5
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    • pp.18-23
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    • 2013
  • Thermal aging test is performed to qualify the life time of equipment in thermally aged condition. Due to long life time more than 10 years like as in power plant, the equipment is subjected to the accelerated thermal aging condition which is able to shorten the long aging test period by increasing aging temperature. Normally, conservatism of thermal aging test causes to impose unbalanced and excessive thermal load on components of the equipment, and deformation and damage problems of the components. Additionally, temperature rise of each component through heat generation of the electric equipment leads to long-term problem of the test period. Multi-phase accelerating aging test is to perform thermal aging test in multiple aging conditions after dividing into groups with various components of equipment. The groups might be classified considering various factors such as activation energy, temperature rise, glass transition temperature and melting temperature. In this study, we verify that the multi-phase accelerating aging test method can reduce and equalize the thermal over load of the components and shorten aging test time.

Effect of Thermal Aging Temperature on Weight Loss and Glass Transition Temperature of Epoxy Adhesives (열화 온도가 에폭시 접착제의 질량변화 및 유리전이온도에 미치는 영향)

  • Park, Soo-Jin;Kim, Jong-Hak;Joo, Hyeok-Jong;Kim, Joon-Hyung;Jin, Fan-Long
    • Elastomers and Composites
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    • v.41 no.1
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    • pp.19-26
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    • 2006
  • In this study, the effect of thermal aging temperature on the weight loss, glass transition temperature, and morphology of epoxy adhesives cured with amine (D-230), amide (G-5022), and anhydride (HN-2200) was investigated. As a result, the weight loss of three specimens was increased with increasing the thermal aging temperature. The result was attributed to the thermal aging which was occurred at the surface of adhesive specimens at high aging temperature, resulting in increasing the weight loss of the specimens. According to the DSC result, the glass transition temperature of DGEBA/D-230 and DGEBA/G-5022 samples war increased as the aging temperature increased, whereas the glass transition temperature of DGEBA/HN-2200 samples was constant above aging temperature of $150^{\circ}C$ and aging tine of 7 days. The SEM result indicated that the surface of DGEBA/G-5022 specimen showed more rough topography than that of DGEBA/D-230 or DGEBA/HN-2200 specimen after thermal aging. This could be correlated with the result of weight loss.

Application of Electron-Beam Irradiation Combined with Aging for Improvement of Microbiological and Physicochemical Quality of Beef Loin

  • Yim, Dong-Gyun;Jo, Cheorun;Kim, Hyun Cheol;Seo, Kang Seok;Nam, Ki-Chang
    • Food Science of Animal Resources
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    • v.36 no.2
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    • pp.215-222
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    • 2016
  • The combined effects of irradiation and aging temperature on the microbial and chemical quality of beef loin were investigated. The samples were vacuum-packaged, irradiated at 0 or 2 kGy using electron-beam (EB), and stored for 10 d at different aging temperatures (2, 14, or 25℃). The microbial growth, shear values, meat color, and nucleotide-related flavor compounds of the samples were analyzed. The irradiation effect on inactivation of foodborne pathogens was also investigated. The population of Listeria monocytogenes and Escherhia coli O157:H7 inoculated in beef samples decreased in proportion to the irradiation dose. Irradiation reduced the total aerobic bacteria (TAB) over the storage, but higher aging temperature increased the TBA. Thus TAB increased sharply in non-irradiated and high temperature-aged (14, 25℃) beef samples after 5 d. With increasing aging temperature and aging time, shear force values decreased. Lipid oxidation could be reduced by short aging time at low aging temperature. The color a* values of the irradiated beef were lower than those of the non-irradiated throughout the aging period. As aging period and temperature increased, IMP decreased and hypoxanthine increased. Considering microbial and physicochemical properties, irradiation can be used for raw beef to be aged at relatively high temperature to shorten aging time and cost.

The Effect of Dynamic Strain Aging on the High Temperature Plastic Deformation Behaviour of Al-Mg Alloy (Al-Mg 합금의 고온 소성 변형 특성에 미치는 동적 변형 시효의 영향)

  • 이상용;이정환
    • Transactions of Materials Processing
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    • v.5 no.4
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    • pp.327-336
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    • 1996
  • The effect of dynamic strain aging on high temperature deformation behaviour of the A-Mg alloy was investigated by strain rate change tests and stress relaxation tests between 20$0^{\circ}C$and 50$0^{\circ}C$. Yield point, short stress transient and periodic discontinuities on the stress-strain curve were considered as an evidence of the effect of dynamic strain aging. With this criterion two distinct strain rate-temperature regimes could be manifested. Dynamic strain aging was considered to be effective in the high temperature-low strain rate regime, whereas dynamic recovery was a dominant deformation mechanism in the low temperature-high strain rate regime. It was found that dynamic strain aging in the high temperature deformation was governed by the mechcanism of diffusion-controlled, viscous dislocation movement.

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Effects of Two-Step Aging Treatment on the Mechanical Properties of 6061 Al Alloy (A 6061 합금의 기계적 특성에 미치는 2단시효의 영향)

  • Lee, Bo-Bae;Im, Hang-Joon;Jeong, Geol-Chae.
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.2
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    • pp.57-60
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    • 2019
  • The impact of two-step treatment on the mechanical properties of the 6061 Al alloy was investigated by testing the hardness and electrical conductance values. After two-step aging treatment, the hardness and electrical conductivity of the alloy was increased, and if the first aging treatment temperature was lower than the secondary aging treatment temperature, both the hardness and the electrical conductivity were not increased. The higher the temperature of the first aging treatment, the higher the hardness. The temperature of the first aging treatment is $175^{\circ}C$, $150^{\circ}C$, $120^{\circ}C$, and the second is $175^{\circ}C$ and $120^{\circ}C$.

Yielding Behavior and Strain Aging Properties of Bake Hardening Steel with Dual-Phase Microstructure (2상 조직을 갖는 소부경화강의 항복 거동과 변형 시효 특성)

  • Lee, Seung-Wan;Lee, Sang-In;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.30 no.6
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    • pp.315-320
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    • 2020
  • This study deals with the yielding behavior and strain aging properties of three bake hardening steels with dual-phase microstructure, fabricated by varying the annealing temperature. Bake hardening and aging tests are performed to examine the correlation of martensite volume fraction with yielding behavior and strain aging properties of the bake hardening steels with dual-phase microstructure. The volume fraction of martensite increases with increasing annealing temperature. Room-temperature tensile test results show that the yielding behavior changes from discontinuous-type to continuous-type with increasing volume fraction of martensite due to higher mobile dislocation density. According to the bake hardening and aging tests, the specimen with the highest fraction of martensite exhibited high bake hardening with low aging index because solute carbon atoms in ferrite and martensite effectively diffuse to dislocations during the bake hardening test, while in the aging test they diffuse at only ferrite due to lower aging temperature.

Effects of annealing temperature on strain-induced martensite and mechanical properties of 304 stainless steel (304 스테인리스 강의 가공유기 마르텐사이트와 기계적 거동에 미치는 온도의 영향)

  • Lee, S.H.;Choi, C.Y.;Nam, W.J.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.203-206
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    • 2008
  • Transformation of austenite to martensite during cold rolling has been widely used to strengthen metastable austenitic stainless steel grades. Aging treatment of cold worked metastable austenitic stainless steels, including ${\alpha}'$-martensite phase, results in the further increase of strength, when aging is performed in $200^{\circ}C$ to $450^{\circ}C$ temperature range. The purpose of the present study was to evaluate the effect of time and temperature on the stress-strain behavior of cold worked austenitic stainless steels. The amount of ${\alpha}'$-martensite during cold working and aging was examined by ferrite scope and X-ray diffraction (XRD). During aging at $450^{\circ}C$ for 1hr, tensile strength dramatically increased by 150MPa. Deformed metastable austenitic steels containing the "body-centered" ${\alpha}'$-martensite are strengthened by the diffusion of interstitial solute atoms during aging at low temperature.

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Elastic Wave Characteristics of Incoloy 825 with Different Solution Treatment Temperature and Aging Time (용체화처리 온도 및 시효 시간이 다른 Incoloy 825의 탄성파 특성)

  • Lee, Seong-Gu;Choi, Byoung-Chul;Nam, Ki-Woo
    • Journal of the Korean Society of Industry Convergence
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    • v.24 no.3
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    • pp.261-269
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    • 2021
  • This study was evaluated the elastic wave properties according to tension of Incoloy 825 alloy with different solution treatment temperature and aging time. Solution treatment was carried out at 700, 800, 900, and 1000 ℃ for 1 hour, and aging was carried out at 700 ℃ for 1, 5, 10, and 30 hours. As the solution treatment temperature increased, the tensile strength decreased and the elongation increased. However, as the aging time increased, the tensile strength increased and the elongation decreased. The dominant frequency decreased as the solution treatment temperature increased, but increased as the aging time increased. The dominant frequency according to the solution treatment and aging time increased as the tensile strength increased, but increased despite the decrease in elongation.

A Study on the Strain Rate and Temperature Dependence of Yield Stress of Al-Li Alloy (Al-Li합금의 항복응력에 대한 변형속도 및 온도의존성에 관한 연구)

  • Oh, Chang-Sup;Han, Chang-Suk
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.6
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    • pp.311-317
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    • 2011
  • The effect of strain rate on the yield stress of an Al-Li alloy has been investigated at temperatures between 77 and 523 K and over the strain rate range from $1.77{\times}10^{-4}s^{-1}$ to $1.77{\times}10^{-2}s^{-1}$. At testing temperatures below 373 K, the yield stress is almost independent of strain rate at any aging stage. At testing temperatures above 373 K, the yield stress increases linearly with the logarithm of strain rate, and the strain rate dependence increases with increasing testing temperature. The yield stresses of under-aged alloy at temperatures between 373 and 473 K at high strain rates are greater than the yield stress at 77 K. For the alloy under-aged or aged nearly to its peak strength, the temperature range within which the positive temperature dependence of yield stress appears expands to the higher temperature side with increasing strain rate. The strain rate dependence of the yield stress is slightly negative at this aging stage. The yield stress of the over-aged alloy decreases monotonically with decreasing strain rate and with increasing testing temperature above 373 K. The modulus normalized yield stress is nearly constant at testing temperatures below 373 K at any strain rate investigated. And, strength depends largely both on the aging conditions and on the testing temperature. The peak positions in strength vs. aging time curves shift to the side of shorter aging time with increasing testing temperature. For the specimens aged nearly to the peak strength, the positive temperature dependence of yield stress is observed in the temperature range. The shift of peak positions in the aging curves are explained in terms of the positive temperature dependence of cutting stress and the negative temperature dependence of by-passing stress.