• Title/Summary/Keyword: TEM-1

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ZnO film growth on sapphire substrate by RF magnetron sputtering (RF 스퍼터링 법에 의한 사파이어 기판상의 ZnO 박막의 성장)

  • Kang Seung Min
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.14 no.5
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    • pp.215-219
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    • 2004
  • ZnO epitaxial films have been grown on a (0001)sapphire substrate by RF magnetron sputtering. The single crystalline ZnO films were grown at the condition of growth rate of about 0.1~0.2 $\mu\textrm{m}$/hr and the substrate temperature of $600^{\circ}C$. The film thickness was about 400~500 nm. The thin film quality and micro-structure have been evaluated by XRD and TEM observation.

Removal of Contaminating TEM-la $\beta-Lactamase$ Gene from Commercial Taq DNA Polymerase

  • Song Jae Seok;Lee Jung Hun;Lee Jung-Hyun;Jeong Byeong Chul;Lee Won-Keun;Lee Sang Hee
    • Journal of Microbiology
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    • v.44 no.1
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    • pp.126-128
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    • 2006
  • This study confirms that Taq DNA polymerase could be contaminated with the $blaTEM-1_a$ gene. It also proposes two different methods that could be used to overcome DNA contamination: (i) DNase I treatment prior to PCR amplification; and (ii) the use of a highly purified Taq DNA polymerase which was devoid of detectable contamination.

Novel Synthesis and Characterization of Pt-graphene/TiO2 Composite Designed for High Photonic Effect and Photocatalytic Activity under Visible Light

  • Ye, Shu;Oh, Won-Chun
    • Journal of the Korean Ceramic Society
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    • v.54 no.1
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    • pp.28-32
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    • 2017
  • The degradation of methyl blue (MB) catalyzed by platinum (Pt)-graphene/$TiO_2$ in dark ambiance was studied. Pt-graphene/$TiO_2$ composites were prepared by simple hydrothermal method. Characterizations of composites were studied by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), specific surface area (BET) analysis, and energy dispersive X-ray (EDX) analysis. UV-spectroscopic analysis of the dyes was performed by measuring the change in absorbance. The degradation of the organic dyes was calculated based on the decrease in concentration of the dyes with respect to regular time intervals. Rate coefficients for the catalytic process were successfully established and reusability tests were performed to test the stability of the used catalysts.

Micro-Raman characterization of isolated single wall carbon nanotubes synthesized using Xylene

  • Choi, Young Chul
    • Carbon letters
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    • v.14 no.3
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    • pp.175-179
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    • 2013
  • Isolated single wall carbon nanotubes (SWCNTs) were synthesized by chemical vapor deposition (CVD) using a liquid precursor (xylene) as a carbon source. Transmission electron microscopy (TEM) and atomic force microscopy confirmed the isolated structure of the SWCNTs. Micro-Raman measurements showed a tangential G-band peak ($1590cm^{-1}$) and radial breathing mode (RBM) peaks ($150-240cm^{-1}$). The tube diameters determined from the RBM frequencies are in good agreement with those obtained from TEM. The chirality of the isolated SWCNTs could be determined based on the energy of the laser and their diameter. A further preliminary study on the nitrogen doping of isolated SWCNTs was carried out by the simple use of acetonitrile dissolved in the precusor.

Microstructural Observation of Cu/Cr Multilayers by Heat Treatment (열처리에 따른 Cu/Cr 다층 박막의 미세 조직 관찰)

  • 양혁수;김기범
    • Journal of the Korean institute of surface engineering
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    • v.28 no.6
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    • pp.376-385
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    • 1995
  • Copper-chromium multilayers with a nominal bilayer thickness of about 400 $\AA$ (200 $\AA$ each) were prepared by dc magnetron sputtering and the evolution of microstructure during heat treatment was investigated by using x-ray diffractometry(XRD), Auger electron spectroscopy(AES) and transmission electron microscopy(TEM). It was observed that an amorphous phase with a thickness of about 40 $\AA$ was formed at the interfaces of the as-deposited Cu/Cr multilayered film using cross-sectional TEM. At elevated temperatures, the Cu(111) reflection showed increasing intensity and decreasing line-width as a result of copper grain growth. The intermixed amorphous phase disappeared after annealing at $250^{\circ}C$ for 1 h and the multilayer structure was stable up to $400^{\circ}C$ for 1 h annealing. At $600^{\circ}C$ annealing, it was observed that the multilayer structure was completely destroyed and copper and chromium phases were fully intermixed.

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First Report of Pasteuria nishizawae Sayre, Wergin, & Nishizawa Attcaking Heterodera glycines in Korea (국내 미기록 콩씨스트선충 기생세균, Pasteuria nishizawae Sayre, Wergin & Nishizawa의 보고)

  • 이영기;김동근;이재국;이수헌;최용철
    • Korean Journal Plant Pathology
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    • v.14 no.6
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    • pp.714-719
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    • 1998
  • Obligate bacterial parasite attacking Heterodera glycines was firstly found from Chungju soybean field in Korea. Diameters of sporangium and central body were 5.6 ${\mu}{\textrm}{m}$ and 1.9 ${\mu}{\textrm}{m}$ under light microscopy (LM), and 3.9 ${\mu}{\textrm}{m}$ and 1.8 ${\mu}{\textrm}{m}$ under transmission electron microscopy (TEM). Endospore showed cup-shaped with smooth-type exosporium without peg-like thickening in polar area under SEM and TEM. Bacteria completed its life cycle in female of soybean cyst nematode after adhering on cuticle of second-stage juvenile. From these results, the Pasteuria found from Chungju was identified with P. nishizawae.

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Effect of surface treatment of graphene nanoplatelets for improvement of thermal and electrical properties of epoxy composites

  • Kim, Minjae;Kim, Yeongseon;Baeck, Sung Hyeon;Shim, Sang Eun
    • Carbon letters
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    • v.16 no.1
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    • pp.34-40
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    • 2015
  • In this study, in order to improve the thermal and electrical properties of epoxy/graphene nanoplatelets (GNPs), surface modifications of GNPs are conducted using silane coupling agents. Three silane coupling agents, i.e. 2-(3,4-epoxycyclohexyl)-ethyltrimethoxysilane (ETMOS), 3-glycidoxypropyltriethoxysilane (GPTS), and 3-glycidoxypropyltrimethoxysilane (GPTMS), were used. Among theses, GPTMS exhibits the best modification performance for fabricating GNP-incorporated epoxy composites. The effect of the silanization is evaluated using transmission electron microscopy (TEM), scanning electron microscopy, thermogravimetric analysis, and energy dispersive X-ray spectroscopy. The electrical and thermal conductivities are characterized. The epoxy/silanized GNPs exhibits higher thermal and electrical properties than the epoxy/raw GNPs due to the improved dispersion state of the GNPs in the epoxy matrix. The TEM microphotographs and Turbiscan data demonstrate that the silane molecules grafted onto the GNP surface improve the GNP dispersion in the epoxy.

Silver Nanoparticles Effect on Antimicrobial and Antifungal Activity of New Heterocycles

  • Kandile, Nadia G.;Zaky, Howida T.;Mohamed, Mansoura I.;Mohamed, Hemat M.
    • Bulletin of the Korean Chemical Society
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    • v.31 no.12
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    • pp.3530-3538
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    • 2010
  • In this study 1-[4-(2-methoxy benzyl)-6-aryl-pyridazin-3(2H)-ylidene] hydrazines were used for the synthesis of new heterocyclic systems such as thiazolidine, phthalazine, pyrazolo, tetrazolo, hydrazide and new pyridazine derivatives to explore the effect of silver nanoparticles on their biological activity efficiency. Structures of the new heterocycles were characterized by the aid of several analytical techniques including; $^1H$-NMR, FTIR and mass spectra. Silver nanoparticles were synthesized by a simple methodology and the formation of silver nanoparticles was confirmed by transmission electron microscopy (TEM) and UV studies. Most of the new prepared heterocycles were evaluated in vitro as new antimicrobial agents. Combination effects of the silver nanoparticles on the antimicrobial activity of the new heterocycles were investigated using the disk diffusion method. Compound 10a exhibited the strongest enhancing effect of silver nanoparticles solution against Aspergillus flavus and Candida albicans.

A Structural Study of the Oxidized High Modulus Pitch Based Carbon Fibers by Oxidation in Carbon Dioxide

  • Roh, Jae-Seung
    • Carbon letters
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    • v.5 no.1
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    • pp.27-33
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    • 2004
  • Structural changes of high modulus carbon fiber by oxidation in carbon dioxide gas using SEM, TEM, and XRD have been observed. It was shown that the originally high modulus carbon fiber is composed of highly ordered graphitic crystalline area and non-crystalline area. It was observed that the La increases during the whole oxidation process. It was shown that the oxidation of high modulus carbon fiber initiates at the non-crystalline area and at the ends of fiber. The large pores developed in fiber by direction of fiber length at high temperature ($1,100^{\circ}C$), and the small pores developed on the fiber surface at low temperature ($900^{\circ}C$). In conclusion, it is found that the oxidation of the carbon fiber was progressed through the imperfection.

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A Surface Study of 304 and 316 Stainless Steel Oxidized between $300^{\circ}C$ and $500^{\circ}C$ ($300^{\circ}C$$500^{\circ}C$사이에서 산회된 304, 316 스테인리스강의 표면특성)

  • 김경록;이경구;강창석;최답천;이도재
    • Journal of the Korean institute of surface engineering
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    • v.32 no.1
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    • pp.43-48
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    • 1999
  • Oxidation behavior of 304 and 316 stainless steels was studied. After solution heat treatment, specimens were polished up to 1$mu \textrm{m}$ using $Al_2O_3$ powder and then subjected to oxidation between $300^{\circ}C$ and 50$0^{\circ}C$ in dry air. TEM and EDS were used for analyzing the components and structure of oxide film. TEM analysis of oxide film revealed that thin amorphous Fe oxide ($Fe_2O_3$) was formed on the top of surface while polycrystalline (Cr, $Fe_2O_3$ was formed below the amorphous Fe oxide layer. The specimens oxidized at $500^{\circ}C$ showed that 316 stainless steel had higher oxidation resistance than 304 stainless steel. These results suggest that Mo component of 316 stainless steel suppresses the formation of Cr carbide which may result in a local Cr depleted area.

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