• 한국식품과학회지
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• 제28권5호
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• pp.959-964
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• 1996

동진 품종의 현미를 2분도미, 5분도미, 7분도미로 도정하여, 도정도에 따른 쌀의 수화와 쌀가루의 이화학적 성질 및 호화 특성을 조사하였다. 쌀의 도정도가 증가하면 일반성분 중에서 단백질, 회분, 지방질, 섬유소의 함량이 감소되고, 쌀의 수분 증가량은 감소되고 SEM으로 관찰하였을 때 틈이 점점 현저하였다. 도정도가 증가할수록 쌀가루의 물결합능력, 팽윤력과 용해도는 증가하였다. 아밀로그람에서의 초기 호화온도는 도정도가 증가할수록 낮아졌고 최고점도, breakdown과 consistency는 높아졌다.

• Rapid Communication in Photoscience
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• 제4권3호
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• pp.54-58
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• 2015

Under the condition of femtosecond impulsive nonlinear optical irradiation, the bright and narrowed blue emission of silicon nanocrystal was observed. This synthetic method produced very small (~ 4 nm) oxide-capped silicon nanocrystal having probably ultra small emitting core (~ 1 nm) inferred from luminescence. By controlling the stirring condition, very high efficiencies of luminescence ( 4 fold higher) were obtained compared with the other conventional femtosecond laser fragmentation methods, which was attributed to the differences in hydration shell structure during the femtosecond laser induced irreversible phase transition reaction. When we properly adjusted the irradiation times of the white light continuum and stirring condition, very homogeneous luminescent silicon nanocrystal bands having relatively sharp lineshape were obtained, which can be attributable to the luminescent core site isolated and free from the surface defects.

• 한국세라믹학회지
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• 제39권7호
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• pp.617-621
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• 2002

Calcium aluminosulfate (3CaO.3Al$_2$O$_3$.CaSO$_4$or $C_4$A$_3$S) was prepared by chemical synthesis from the nitrate salts and aluminum sulfate. $C_4$A$_3$S was the main phase after calcination at 110$0^{\circ}C$. The specific surface areas after calcination at 110$0^{\circ}C$ and 130$0^{\circ}C$ were about 2.5 and 1.0 $m^2$/g, respectively. Hydration was investigated by XRD, DSC, SEM, EDS, conduction calorimetry and analysis of the liquid phase. Calorimetry showed that the induction period was longer than that of a sample prepared by conventional solid state sintering and this was attributed to the formation of amorphous coatings in abundance of $Al_2$O$_3$ and SO$_3$. Crystalline hydration products, principally calcium monosulfoaluminate hydrate and Al(OH)$_3$, appeared subsequently.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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• pp.429-432
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• 2008

Large area members such as foundation concrete of underground structures in power plants have an effect on structural stability and durability of the structure due to danger of crack occurrence and shrinkage crack that occur owing to the difference of temperature by heat of hydration between inside and outside of the members at initial age. And a construction for waterproofness is performed additionally to protect marine structures from osmosis of seawater because the structures adjoin below the surface of sea. So, if a rise of the heat of hydration, crack, and corrosion of bars are controled effectively using a composite such as fluosilicate salt in concrete production process of a initial construction, expenses are cut down and construction hours are reduced by securing durability through improvement of watertightness. The property tests of adiabatic temperature by hydration are carried out at initial age about standard concrete and test concrete using a fluosilicate salt composite to evaluate an effect on improvement of watertightness for concrete structures in this study. And the experiments such as a permeability test of hardened concrete, a water absorption test, a compression strength test and a elongation test are carried out and the results from these are described.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2019년도 춘계 학술논문 발표대회
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• pp.36-37
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• 2019

In domestic construction industry progress, construction and quality control of large structures are considered to be important as the superstructure and mass scale of structures. In the case of mass concrete, high hydration heat caused by cement hydration generates temperature stress by generating internal temperature difference with the concrete surface. These temperature stresses cause cracks to penetrate the concrete structure. A method of lowering the heat generation by incorporating Urea in order to reduce the concrete temperature crack has been proposed. In this study, the heat function coefficient for the FEM temperature crack analysis of the mass concrete containing the element was derived and the adiabatic temperature rise test was carried out according to the incorporation of the element. As a result of this experiment, the maximum temperature of 41 ± 1℃ was obtained irrespective of the amount of urea, and the maximum temperature decreased by 16.9℃ in concrete containing 40kg/㎥ of urea.

• 한국응용과학기술학회지
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• 제15권3호
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• pp.47-53
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• 1998

The polyimide film surface was modified with KOH aqueous solutions or sulfuric acid. The film thickness was increased by about 10% through the modification of film surface. Hydrolysis of amide bonds and hydration of water induced the increase. The polarity of the film surface increased and identified by contact angle measurement. The depth and roughness of modified was increased. After treatment of surface with water, alkyl and 4-pentyloxyaniline were introduced on the film surface by complex formation between anionic species formed on the imide surface and ammonium ion. The newly introduced alkyl group was identified by FT-IR spectroscopy. Surface polarity reduced dramatically and the roughness was increased after introduction of ammonium salt.

• Bulletin of the Korean Chemical Society
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• 제24권10호
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• pp.1437-1443
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• 2003

Thermal decomposition of hydrated surface layer of $Mg(OH)_2$ at $500^{\circ}C$ in vacuum turned non-porous MgO into porous one with high surface area of around $270 m^2$/g. Most of its surface area, 74 %, was from micropores, and rest of it was from mesopores in wedge-shaped slits, exhibiting bimodal size distribution centered around 30 and 90${\AA}$. Rehydration followed by subsequent dehydration at $300 ^{\circ}C$ in dynamic vacuum further raised the surface area to 340 $m^2$/g. Fraction of microporous surface area was increased to 93%, and the shape of the mesopores was modified into parallel slits with a specific dimension of 32 ${\AA}$. Application of $Fe_2O_3$ over MgO via iron complex formation did not alter the pore characteristics of MgO core, except slightly increased pore dimension. Over the course of the modification, $Fe_2O_3$ stayed on the surface possibly via spill-over reaction.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2008년도 춘계 학술발표회 제20권1호
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• pp.989-992
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• 2008

본 연구에서는 선일공업(주)의 축적된 기술력을 바탕으로 초고강도(150MPa급) 콘크리트를 당사 기술 연구소 신축시 노출콘크리트에 적용함으로써, 이에 대한 사례를 소개하고자 한다. 현장적용에 앞서 실내실험 및 레미콘 배치플랜트 실험(이하 B/P Test)을 통해 콘크리트의 기초물성(슬럼프플로우, 공기량, 50cm도달시간, 경시변화, 압축강도) 및 생산성을 평가하였으며, 다음으로 실구조물과 동일한 벽체두께 거푸집종류 노출콘크리트용 콘 등을 고려하여 제작한 모의부재를 대상으로 Mock-up Test를 실시하여 충진성, 표면마감성(육안관찰) 및 수화열을 평가하였다. 그 결과 슬럼프플로우, 공기량, 50cm도달시간, 경시변화 및 압축강도는 요구조건에 만족한 결과를 보였으며, 수화열 계측결과는 온도균열지수 0.78로 유해한 균열발생을 제한할 지수를 나타냈다. 현장타설시 초고강도 콘크리트의 높은 단위용적중량으로 인해 거푸집 터짐현상이 발생하였기 때문에, 재타설시에는 재발방지를 위해 거푸집을 보강하고 타설시간을 조정하였다. 또한 노출표면의 극대화를 위해 저주파(1차) 및 고주파(2차)로 2회에 걸쳐 진동다짐을 실시하였지만 표면곰보가 발생하였다. 따라서 향후 초고강도 콘크리트를 노출콘크리트에 적용할 경우, 다양한 변수조건에 대한 체계적인 시공관리계획 및 시공방법개선이 중요할 것으로 판단된다.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2010년도 춘계 학술대회 제22권1호
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• pp.475-476
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• 2010

Hydration products formed on the steel surface may impose the resistance to corrosion of steel when a concrete is exposed to a salt environment. In the present study, ordinary Portland cement (OPC), calcium aluminate cement (CAC) and calcium hydroxide are applied as coating materials on the steel surface to consider the hydrations of each binder at corrosion. Corrosion is measured in terms of the corrosion potential and galvanic current to detect the effects in mitigating the corrosion behavior.

• 한국환경보건학회지
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• 제29권1호
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• pp.34-42
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• 2003

The objective of this study is to investigate the waste recycling possibility, practicability, economic efficiency and acid gas sorbent use of the hard-shelled mussel. This study is to investigate the hydration/calcination reaction and fixed bed reactor. The physical-chemical characteristics of the hard-shelled mussel were analyzed by ICP SEM-EDX, BET and pore volume. Thus, the results could be summarized as follows; Hard-shelled mussel can be used as iron-manufacture and chemical sorbents considering more than 53.7% of the mussel is lime content. The SO$_2$removal efficiency of the hard-shelled mussel after calcined hydration increased thirty times as a result of the higher pore size, specific surface area and pore volume. Also, the CaO content, pore volume, pore size distribution and specific surface area greatly influenced the SO$_2$ and NOx removal reactivity. The optimum particle diameter average of hard-shelled mussel was $\pm$100 mesh, which was applied to the sorbent on the medium/small scale waste incinerator and flue gas desulfurization processes.