• Title/Summary/Keyword: Surface crystal

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Effect of Surface Energy Anisotropy on the Equilibrium Shape of Sapphire Crystal

  • Choi, Jung-Hae
    • Journal of the Korean Ceramic Society
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    • v.39 no.10
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    • pp.907-911
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    • 2002
  • Using the two-dimensional Wulff plot, the equilibrium shape of a sapphire crystal was investigated as a function of surface energy anisotropy. Depending on the relative values of surface energy for various facet planes, the projected shape of equilibrium sapphire was determined to be rectangle, parallelogram, hexagon or octagon. The results are compared with the experimentally observed shapes of internal cavities of submicron range in sapphire single crystals.

A Study on the ELID Grinding Properties of Single Crystal Sapphire Wafer using Ultrasonic Table (초음파 테이블을 이용한 단결정 사파이어 웨이퍼의 ELID 연삭가공 특성 연구)

  • Hwang, JinHa;Kwak, Tae-Soo;Lee, Deug-Woo;Jung, Myung-Won;Lee, Sang-Min
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.12 no.4
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    • pp.75-80
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    • 2013
  • Single crystal sapphire being used in high technology industry is a brittle material with a high hardness and excellent physical properties. ELID(Electrolytic In-Process Dressing) grinding technology was applied to material removal machining process of single crystal sapphire wafer. Ultrasonic vibration which added to material using ultrasonic table was adopted to efficient ELID grinding of sapphire materials. The evaluation of the ground surface of single crystal sapphire wafer was carried out by means of surface measuring by using AFM(Atomic Force Microscope), surface roughness tester and optical microscope device. As the results of experiment, it was shown that more efficient grinding was conducted when using ultrasonic table. In case of using #170 grinding wheel, surface roughness of ELID ground specimen in using ultrasonic table was superior to ELID ground specimen without ultrasonic table. However, In case of using #2000 grinding wheel, surface roughness of ELID ground specimen in using ultrasonic table was inferior to ELID ground specimen without ultrasonic table.

Synthesis of zeolite MFI films on alumina and silicon supports using seed crystals (알루미나와 실리콘 지지체에 종자결정에 의한 제올라이트 MFI 필름의 합성)

  • Ko, Tae-Seog
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.1
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    • pp.38-44
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    • 2008
  • Contiuous c-oriented zeolite MFI films $(<35{\mu}m)$ were prepared by hydrothermal secondary growth of silicalite-1 seed crystal in the surface of alumina porous substrate and silicon substrate. The supported films were characterized with scanning electron microscopy and X-ray diffraction. Effect of substrate surface roughness were investigated and a mechanism for c-oriented film formation and characteristic dom-like defects formation which is observed after seeding growth was discussed. The roughness of substrate plays an important role.

Homogeneous Liquid Crystal Alignment on Anisotropic YSnO Surface by Imprinting Method (임프린팅법을 이용한 YSnO 박막의 표면 이방성 획득과 액정 배향 특성 연구)

  • Oh, Byeong-Yun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.33 no.1
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    • pp.21-24
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    • 2020
  • We investigated a solution-driven Yttrium Tin Oxide (YSnO) film that was imprinted using a parallel nanostructure as a liquid crystal (LC) alignment layer. The imprinting process was conducted at the annealing temperature of 100℃. To evaluate the effect of this process, we conducted surface analyses including atomic force microscopy (AFM). During imprinting, the surface roughness was reduced, and anisotropic characteristics were observed. Planar LC alignment was observed at a pretilt angle of 0.22° on YSnO film. Surface anisotropy induced by imprinting method forces LC to align along the direction of the parallel nanostructure, which is an alternative to conventional polyimide treated using a rubbing process.

Nanodeformation Behaviors of the Single Crystal Silicon and the Pyrex glass 7740 during Nanoscratch (나노스크래치 공정에서 단결정 실리론 및 파이렉스 7740 의 나노변형거동)

  • 신용래;윤성원;강충길
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.363-366
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    • 2003
  • In nanomachining processes, chemical effects are more dominant factor compared with physical deformation. For example, during the nanoscratch on a silicon surface in the atmosphere, micro protuberances are formed due to the mechanochemical reaction between the diamond tip and the surface. On the contrary, in case of chemically stable materials, such as ceramics or glasse, the surface protuberance are not formed. The purpose of this study is to understand effects of the mechanochemical reaction between tip and surfaces on deformation behaviors of hard-brittle materials. Nanometerscale elasoplastic deformation behavior of single crystal silicon (100) was characterized with the surface protuberance phenomena, and compared with that of borosilicate (Pyrex glass 7740).

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On the strong attractive force dependence of the surface phase transition : Qualitative consideration from the occupation statistics (표면상변이의 강인력 의존성 : 점유통계를 이용한 정성적 고찰)

  • 김철호
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.4
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    • pp.573-577
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    • 1997
  • Surface phase transition is known to be observed at the system that there exists a strong attractive potential between particles adsorbed. This study presents a dependence of the surface phase transition on strong attractive force using a simple occupation statistical method. It was found that the system exhibits a phase transition from the vacuum phase into the population phase and the critical pressure also increases with the temperature. This fact indicates that these results explain well qualitatively the surface phase transition.

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Nanomachining on Single Crystal Silicon Wafer by Ultra Short Pulse Electrochemical Oxidation based on Non-contact Scanning Probe Lithography (비접촉 SPL기법을 이용한 단결정 실리콘 웨이퍼 표면의 극초단파 펄스 전기화학 초정밀 나노가공)

  • Lee, Jeong-Min;Kim, Sun-Ho;Kim, Tack-Hyun;Park, Jeong-Woo
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.20 no.4
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    • pp.395-400
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    • 2011
  • Scanning Probe Lithography is a method to localized oxidation on single crystal silicon wafer surface. This study demonstrates nanometer scale non contact lithography process on (100) silicon (p-type) wafer surface using AFM(Atomic force microscope) apparatuses and pulse controlling methods. AFM-based experimental apparatuses are connected the DC pulse generator that supplies ultra short pulses between conductive tip and single crystal silicon wafer surface maintaining constant humidity during processes. Then ultra short pulse durations are controlled according to various experimental conditions. Non contact lithography of using ultra short pulse induces electrochemical reaction between micro-scale tip and silicon wafer surface. Various growths of oxides can be created by ultra short pulse non contact lithography modification according to various pulse durations and applied constant humidity environment.

The Surface Recrystallization Behavior of Single Crystal CMSX-2 (단결정 CMSX-2의 표면재결정 거동)

  • Jo, Chang-Yong;Na, Yeong-Sang;Kim, Hak-Min;Kim, Woo-Yeol;Bae, Cha-Hurn;Lee, Sang-Lae
    • 연구논문집
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    • s.23
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    • pp.15-27
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    • 1993
  • The single crystal specimens were solidified by modified Bridgeman method. The surface recrystallized single crystal specimens were prepared by shot peening followed by heat treatment. The surface recrystallization begins at the dendrite cores on the surface. The recrystallized grains grew into the inner side of the specimen. The growth of recrystallized grains was inhibited by the pores and eutectic phases. The primary $\gamma'$ phases were dissolved at the recrystallized grain boundaries during the grain growth. The grain growth of recrystallized grains was similar to the cellular type transformation. No orientation relationships were found bewteen the recrystallized grains and the parent phase.

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Pretilt Angle Generation for Nematic Liquid Crystal on a Homeotropic Alignment Layer (수직배향층에서의 네마틱액정의 프리틸트각 발생)

  • 서대식;김형규;이승희
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.2
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    • pp.130-132
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    • 2001
  • The mechanisms of pretilt angle generation in nematic liquid crystal (NLC) with negative dielectric anisotropy on a rubbed polyimide (PI) surface for homeotropic alignment were studied. The pretilt angle of negative type NLC was smaller than that of the positive type NLC for all rubbing strength regions on the rubbed PI surface. The pretilt angle generated in NLC does not attributable to steric interaction between the fluorine moiety of NLC and the polymer surface on the rubbed PI surface. Consequently, the mechanism of the pretilt angle generation for homeotropic alignment is different from the one for homogeneous alignment.

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