• Title/Summary/Keyword: Sub-Kelvin

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Review on innovative small refrigeration methods for sub-Kelvin cooling

  • Dohoon, Kwon;Junhyuk, Bae;Sangkwon, Jeong
    • Progress in Superconductivity and Cryogenics
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    • v.24 no.4
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    • pp.71-77
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    • 2022
  • Sub-Kelvin cooling has been generally demanded for the fields of low temperature physics, such as physical property measurements, astronomical detection, and quantum computing. The refrigeration system with a small size can be appropriately introduced when the measurement system does not require a high cooling capacity at sub-Kelvin temperature. The dilution refrigerator which is a common method to reach sub-Kelvin, however, must possess a large 3He circulation equipment at room temperature. As alternatives, a sorption refrigerator and a magnetic refrigerator can be adopted for sub-Kelvin cooling. This paper describes those coolers which have been developed by various research groups. Furthermore, a cold-cycle dilution refrigerator of which the size of the 3He circulation system is minimized, is also introduced. Subsequently, a new concept of dilution refrigerator is proposed by our group. The suggested cooler can achieve sub-Kelvin temperature with a small size since it does not require any recuperator and turbo-molecular vacuum pump. Its architecture allows the compact configuration to reach sub-Kelvin temperature by integrating the sorption pump and the magnetic refrigerators. Therefore, it may be suitably utilized in the low temperature experiments requiring low cooling capacity.

Characterization of O2 ionosorption induced potential changing property of SnO2 nanowire with Kelvin force microscopy (KFM)

  • Heo, Jinhee;Won, Soonho
    • Journal of Ceramic Processing Research
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    • v.13 no.spc2
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    • pp.359-362
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    • 2012
  • We have employed Kelvin force microscopy (KFM) system to measure the potential change of a single SnO2 nanowire which had been synthesized on the Au thin film by a thermal process. By using the KFM probing technique, Rh coated conducting cantilever can approach a single SnO2 nanowire in nano scale and get the potential images with oscillating AC bias between Au electrode and cantilever. Also, during imaging the potential status, we controlled the concentration of oxygen in measuring chamber to change the ionosorption rate. From the results of such experiments, we verified that the surface potential as well as doping type of a single SnO2 nanowire could be changed by oxygen ionosorption.

A Study of the Ferroelectric Properties of PbZr0.4Ti0.6O3 (PZT) Grains Using Kelvin Force Microscopy Analysis

  • Heo, Jin-Hee
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.6
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    • pp.275-278
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    • 2010
  • We have examined the Ferroelectric properties of $PbZr_{0.4}Ti_{0.6}O_3$ (PZT) grains by monitoring the surface potential through the utilization of Kelvin force microscopy. Hysteretic and time dependent behaviors of small and large grains were compared with each other. The smaller grain yields had smaller values of surface potential. However, the normalized voltage versus surface potential behavior indicates that the smaller grains became saturated earlier with respect to the writing voltages than did the larger grains. On the other hand, the surface potential hysteresis loop obtained from the smaller grains showed a similar shape to what might be obtained from a Zr rich PZT film. In contrast the hysteresis loop of the larger grain looks like that obtained from a Ti-rich film. In addition, the time dependent behaviors of the smaller grains also revealed a better response than the response of larger grains. The overall ferroelectric properties of the smaller grains seem better than corresponding properties for larger grains. The Ti/Zr ratio of the PZT film which was examined in this study was 60/40.

Nanoscopic Understanding of Phase Transition of Epitaxial VO2 Thin Films (에피택셜 VO2 박막의 상전이에 대한 미시적 이해)

  • Kim, Dong-Wook;Sohn, Ahrum
    • Journal of the Korean institute of surface engineering
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    • v.50 no.3
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    • pp.141-146
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    • 2017
  • We investigated configuration of metallic and insulating domains in $VO_2$ thin films, while spanning metal-insulator phase transition. Kelvin probe force microscopy, of which spatial resolution is less than 100 nm, enables us to measure local work function (WF) at the sample surface. The WF of $VO_2$ thin films decreased (increased) as increasing (decreasing) the sample temperature, during the phase transition. The higher and lower WF regions corresponded to the insulating and metallic domains, respectively. The metallic fraction, estimated from the WF maps, well explained the temperature-dependent resistivity based on the percolation model. The WF mapping also showed us how the structural defects affected the phase transition behaviors.

Mapping of Work Function in Self-Assembled V2O5 Nanonet Structures

  • Park, Jeong Woo;Kim, Taekyeong
    • Journal of the Korean Chemical Society
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    • v.61 no.1
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    • pp.12-15
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    • 2017
  • We presented a mapping the work function of the vanadium pentoxide ($V_2O_5$) nanonet structures by scanning Kelvin probe microscopy (SKPM). In this measurement, the $V_2O_5$ nanonet was self-assembled via dropping the solution of $V_2O_5$ nanowires (NWs) onto the $SiO_2$ substrate and drying the solvent, resulting in the networks of $V_2O_5$ NWs. We found that the SKPM signal as a surface potential of $V_2O_5$ nanonet is attributed to the contact potential difference (CPD) between the work functions of the metal tip and the $V_2O_5$ nanonet. We generated the histograms of the CPD signals obtained from the SKPM mapping of the $V_2O_5$ nanonet as well as the highly ordered pyrolytic graphite (HOPG) which is used as a reference for the calibration of the SKPM tip. By using the histogram peaks of the CPD signals, we successfully estimated the work function of ~5.1 eV for the $V_2O_5$ nanonet structures. This work provides a possibility of a nanometer-scale imaging of the work function of the various nanostructures and helps to understand the electrical characteristics of the future electronic devices.

A Study on Electrostatic Discharging in Ultrapure and Electrolyzed Waters Using Kelvin's Thunderstorm Effect (캘빈방전 효과를 이용한 초순수 및 전해이온수의 정전기 방전 연구)

  • Kim, Hyung-won;Jung, Youn-won;Choi, In-sik;Choi, Byung-sun;Choi, Donghyeon;Ryoo, Kun-kul
    • Journal of the Semiconductor & Display Technology
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    • v.21 no.1
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    • pp.5-11
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    • 2022
  • Despite the increasing importance of manufacturing and application R&D for ultrapure deionized water and electrolyzed ion water, various and systematic studies have not been conducted until now. In this study, the electrostatic discharge (ESD) behavior of electrolyzed ion water using a proton exchange membrane(PEM) was evaluated according to the type, flow rate, and bubble of electrolyzed ion water. In addition, by observing that Oxidation Reduction Potential (ORP) value returns to the unique value of electrolyzed ion water after electrostatic discharge, the possibility of two types of ions participating in electrostatic discharge ((H2O)n+ (assumed)) and ions for maintaining the characteristics of electrolyzed water could be inferred. In order to confirm the chemical structure and characteristics of the cations, in-depth research related to water molecular orbital energy or band gap should be followed.

Current Trend of Ultrahigh Vacuum Low Temperature Scanning Tunneling Microscopy (초고진공 저온 주사터널 현미경 장치의 최신 경향)

  • Ham, Ungdon;Yeom, Han Woong
    • Vacuum Magazine
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    • v.3 no.4
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    • pp.14-18
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    • 2016
  • In this article, we will summarize recent advances in ultrahigh vacuum (UHV) low-temperature scanning tunneling microscopy (STM) during the last decade. Leading STM groups have finished or are constructing UHV milli-Kelvin high magnetic field STM capable of a few tens of milli-Kelvin and ~ 10 tesla. Applications with UHV sub-Kelvin high magnetic STM have been increased since mid-2000's. Active research using UHV low temperature tuning fork atomic force microscopes and UHV photon low-temperature scanning tunneling microscopes will be introduced. Considering these advances of UHV low-temperature STM we will discuss next trend in STM in the near future.

Thermodynamic Properties of Bismuth Trifluoride from Vapour Pressure Measurements (증기압 측정으로부터 BiF3의 열역학적 계산)

  • ;S. Blairs
    • Journal of the Korean Ceramic Society
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    • v.31 no.6
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    • pp.685-693
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    • 1994
  • Sublimation vapour pressures and sublimation enthalpy of anhydrous bismuth trifluoride have been measured by the continuous gravimetric Cnudsen-effusion method from 639-7 to 782.8 K. Additional effusion measurements have also been made from 750.6 to 863.1 K by the torsion-effusion method. Based on a correlation of subHo298.15 and subSo298.15, a recommended P(T) equation has been obtained for BiF3(s); logP= -C/T+5.2375logT-3.205$\times$10-3+4.661$\times$104/T2+1.348 where P is in Pa, T in Kelvin, subHo298.15 in kJ mol-1 and C=( subHo298.15-13.5149)/1.9146$\times$10-2. Condensation coefficients and their temperature dependence have been derived from the effusion measurements.

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Pressure Swing Adsorption Based Hydrogen Purification Vessel 3D Modeling and Feasibility Study (Pressure Swing Adsorption 기반 수소정제용기 3차원 모델링 및 타당성 검증 연구)

  • CHA, YOHAN;CHOI, JAEYOO;JU, HYUNCHUL
    • Transactions of the Korean hydrogen and new energy society
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    • v.32 no.4
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    • pp.197-204
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    • 2021
  • Pressure swing adsorption is a purification process which can get pure hydrogen. The purification process is composed of four process: compression, adsorption, desorption and discharge. In this study the adsorption process was simulated by using the Fluent and validated with experimental results. A gas used in experiment is composed of H2, CO2, CH4, and CO. Adsorption process conducted under 313 kelvin and 3 bar and bituminous-coal-based (BPL) activated carbon was used as the adsorbent. Langmuir model was applied to explain the gas adsorption. And diffusion of all the gases was controlled by micro-pore resistances. The result shows that, the most adsorbed gas was carbon dioxide, followed by methane and carbon monoxide. And carbon monoxide took the least amount of time to reach the maximum adsorption amount. The molar fraction of the off-gas became the same as the molar fraction of the gas supplied from the inlet after adsorption reached the equilibrium.

FUNCTIONAL RELATIONS INVOLVING SARAN'S HYPERGEOMETRIC FUNCTIONS FE AND F(3)

  • Kim, Yong-Sup;Hasanov, Anvar
    • The Pure and Applied Mathematics
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    • v.19 no.1
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    • pp.43-57
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    • 2012
  • By simply splitting the hypergeometric Saran function $F_E$ into eight parts, we show how some useful and generalized relations between $F_E$ and Srivas- tava's hypergeometric function $F^{(3)}$ can be obtained. These main results are shown to be specialized to yield certain relations between functions $_0F_1$, $_1F_1$, $_0F_3$, ${\Psi}_2$, and their products including different combinations with different values of parameters and signs of variables.