• Title/Summary/Keyword: Specimen stability

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Wear Resistance of c-BN Surface Modified 316L Austenitic Stainless Steel by R.F. Sputtering (R.F. sputtering 방법에 의해 c-BN 표면처리된 316L 오스테나이트계 스테인리스 강의 내마모특성 향상)

  • Lee, Kwang-Min;Jeong, Se-Hoon;Park, Sung-Tae
    • Korean Journal of Materials Research
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    • v.20 no.4
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    • pp.194-198
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    • 2010
  • Cubic boron nitride (c-BN) is a promising material for use in many potential applications because of its outstanding physical properties such as high thermal stability, high abrasive wear resistance, and super hardness. Even though 316L austenitic stainless steel (STS) has poor wear resistance causing it to be toxic in the body due to wear and material chips, 316L STS has been used for implant biomaterials in orthopedics due to its good corrosion resistance and mechanical properties. Therefore, in the present study, c-BN films with a $B_4C$ layer were applied to a 316L STS specimen in order to improve its wear resistance. The deposition of the c-BN films was performed using an r.f. (13.56 MHz) magnetron sputtering system with a $B_4C$ target. The coating layers were characterized using XPS and SEM, and the mechanical properties were investigated using a nanoindenter. The friction coefficient of the c-BN coated 316L STS steel was obtained using a pin-on-disk according to the ASTM G163-99. The thickness of the obtained c-BN and $B_4C$ were about 220 nm and 630 nm, respectively. The high resolution XPS spectra analysis of B1s and N1s revealed that the c-BN film was mainly composed of $sp^3$ BN bonds. The hardness and elastic modulus of the c-BN measured by the nanoindenter were 46.8 GPa and 345.7 GPa, respectively. The friction coefficient of the c-BN coated 316L STS was decreased from 3.5 to 1.6. The wear property of the c-BN coated 316L STS was enhanced by a factor of two.

Characteristics of the Progressive Brittle Failure around Circular Opening by Scaled Model Test and Discrete Element Analysis (축소 모형시험과 개별 요소 해석에 의한 원형 공동 주변의 점진적 취성파괴 특성에 관한 연구)

  • Jeon Seok-Won;Park Eui-Seob;Bae Seong-Ho
    • Tunnel and Underground Space
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    • v.15 no.4 s.57
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    • pp.250-263
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    • 2005
  • Progressive and localized brittle failures around an excavated opening by the overstressed condition can act as a serious obstacle to ensure the stability and the economical efficiency of construction work. In this paper, the characteristics of the brittle failure around an circular opening with stress level was studied by the biaxial compressive test using sealed specimen and by the numerical simulation with $PFC^{2D}$, one of the discrete element codes. The occurring pattern and shape of the brittle failure around a circular opening monitored during the biaxial loading were well coincided with those of the stress induced failures around the excavated openings observed in the brittle rock masses. The crack development stages with stress level were evaluated by the detailed analysis on the acoustic emission event properties. The microcrack development process around a circular opening was successfully visualized by the particle flow analysis. It indicated that the scaled test had a good feasibility in understanding the mechanism of the brittle failure around an opening with a high reliability.

Dimensional Stability of Waterlogged Archaeological Wood in PEG, Lactitol and Sucrose Treatment (수침목재의 PEG, 락티톨, 슈크로오스 처리에 의한 치수안정화 효과)

  • Lee, Hyo Sun;Kang, Ae Kyung;Park, Sang Jin
    • Journal of Conservation Science
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    • v.8 no.1 s.11
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    • pp.28-32
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    • 1999
  • The performance of dimensional stabilization of lactitol, PEG (Mw, 4000), and sucrose was evaluated for thin sections of oak wood (Quercus sp.) that had been buried in underground for presumably 1500 years. Thin wood sections of the specimen were soaked for three and seven days in each stabilizing agent with wide concentration ranges of 10, 30, 50, and $70\%$ by weight. Sucrose showed the largest weight gain among three agents, and the shrinkage of cross sections were found to be $1\%\;and\;4\%$ for three and seven days soaking, respectively. The result showed that sucrose among three stabilizing agents used was the best for the dimensional stabilization of the oak wood.

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Inspection about Influences on the Weld Parts through the Change of the Position of Welding Torch and the Voltage During CO2 Welding (CO2용접에서 용접 토치의 위치변화와 전압이 용접부에 미치는 영향고찰)

  • Kim, Bub-Hun;Kim, Won-Il;Lee, Chil-Soon
    • Journal of the Korean Society of Industry Convergence
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    • v.14 no.2
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    • pp.59-65
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    • 2011
  • $CO_2$ Welding which uses $CO_2$ instead of inert gas is most widely used in industrial sites. Welding rod for $CO_2$ Welding is roughly divided into solid wire and flux cored wire. $CO_2$ Welding has higher efficiency than any other welding methods, and also economic and speedy to handle, that's why is used frequently for welding general structures. As most of studies about $CO_2$ Welding are focused on metallurgical changes of successful joints, they developed theories about the change of configuration on weld parts. This study is especially focused on not only the change of configuration on weld parts, but also the change of the penetrating depth through changing the position of welding torch. For inspection, applied AWS A5.20 E70-1 among welding wires and fixed moving angles of torch, but controled the values of voltage and the position of welding. Also Automatic Feed Mechanism is used for exact movement of material, specimen is a piece of steel for general structures. By measuring and analyzing the configuration of sliced section and the values of welding leg length and welding throat after welding, the outcome about the changes turned out.

Load transfer test of circular anchorage system according to ETAG 013 (ETAG 013 규정에 따른 원형 정착구의 하중전달실험)

  • Kim, Bum-Joon;Kim, Hyun-Gi
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.5
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    • pp.167-175
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    • 2018
  • Load transfer experiments have been carried out to evaluate the performance of the anchorage and it has been stated that the specimens were manufactured and tested according to ETAG 013. On the other hand, the amount of spiral reinforcement and auxiliary reinforcement exceeded the amount specified in ETAG 013. In this study, the load transfer test method and the criteria specified in ETAG 013 were considered and the PT anchorage system was applied to manufacture specimens with high strength concrete and a high tensile prestressing strand. A load transfer test according to ETAG 013 was performed to evaluate the performance of the circular anchorage. As a result, it was confirmed that ETAG 013 is a very strict specification that does not satisfy the performance of an anchorage unless the specimens of an appropriate size and spiral reinforcement are used. To assess the stability of the specimens, increasing the size of the specimen by 15%, rather than increasing the amount of auxiliary reinforcement, is considered to be the correct method in accordance with ETAG 013.

Electrochemical Characterization of Anodic Tin Oxides with Nano-Porous Structure (나노 구조를 가지는 다공성 주석 산화물의 전기화학적 특성)

  • Lee, Jae-Wook;Park, Su-Jin;Shin, Heon-Cheol
    • Korean Journal of Materials Research
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    • v.21 no.1
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    • pp.21-27
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    • 2011
  • A nano-porous structure of tin oxide was prepared using an anodic oxidation process and the sample's electrochemical properties were evaluated for application as an anode in a rechargeable lithium battery. Microscopic images of the as-anodized sample indicated that it has a nano-porous structure with an average pore size of several tens of nanometers and a pore wall size of about 10 nanometers; the structural/compositional analyses proved that it is amorphous stannous oxide (SnO). The powder form of the as-anodized specimen was satisfactorily lithiated and delithiated as the anode in a lithium battery. Furthermore, it showed high initial reversible capacity and superior rate performance when compared to previous fabrication attempts. Its excellent electrode performance is probably due to the effective alleviation of strain arising from a cycling-induced large volume change and the short diffusion length of lithium through the nano-structured sample. To further enhance the rate performance, the attempt was made to create porous tin oxide film on copper substrate by anodizing the electrodeposited tin. Nevertheless, the full anodization of tin film on a copper substrate led to the mechanical disintegration of the anodic tin oxide, due most likely to the vigorous gas evolution and the surface oxidation of copper substrate. The adhesion of anodic tin oxide to the substrate, together with the initial reversibility and cycling stability, needs to be further improved for its application to high-power electrode materials in lithium batteries.

ECOLOGICAL RESPONSE OF STREAMS IN KOREA UNDER DIFFERENT MANAGEMENT REGIMES

  • Lee Chang-Seok;Cho Yong-Chan;Shin Hyun-Cheol;Moon Jeong-Suk;Lee Byung-Cheon;Bae Yang-Seop;Byun Hwa-Geun;Yi Hoon-Bok
    • Water Engineering Research
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    • v.6 no.3
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    • pp.131-147
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    • 2005
  • Today, a trend that tries to return the artificial space of a river to a natural one is expanding. But in Korea, which lies in the monsoon climate zone, rivers endure flood damage every year. Moreover, climatic change from global warming causes severe variations in precipitation patterns. Until recently, river restoration practices in Korea have followed partial restoration. These restorative treatments transformed artificial structures of the stream to natural ones and introduced natural vegetation by imitating natural or semi-natural streams. Treatment transformed the riparian structure and increased the diversity of micro-topography and vegetation. Furthermore, restoration recovered species composition, increased species diversity, and inhibited the establishment of exotic species. In particular, the Suip stream, which was left to its natural process for approximately 50 years, recovered its natural features almost completely through passive restoration. An urban stream, the Yangjae, and a rural stream, the Dongmoon, were restored partially by applying ecological principles. On the contrary, technological treatment applied to recover flood damage induced species composition far from the natural vegetation and decreased species diversity. Additionally, this treatment increased exotic species. The same results were found also in benthic invertebrate and fish fauna. The above-mentioned results reflect the importance of ecological considerations in river management.

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Properties and Manufacturing of Low Melting Alloy Impregnated Wood Composites for using Domestic Thinned Logs of Juglans mandshurica (국산 가래나무 간벌재활용을 위한 금속주입목재의 제조 및 특성)

  • Park, Kye-Shin;Lee, Hwa-Hyoung
    • Korean Journal of Agricultural Science
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    • v.37 no.3
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    • pp.457-464
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    • 2010
  • The low melting alloy impregnated wood composites with natural grain of thinned Juglans mandshurica was made and evaluated in this study. And the proper manufacturing conditions was also investigated in this study. The low melting alloy with bismuth(Bi) and tin(Sn) which are harmless to humans, was applied for this novel composites, which showed not only no defects of discoloration, delamination, swelling, and cracking, because of high dimensional stability and low thickness swelling, but also much improved performance such as high bending strength, high hardness, low abrasion, high thermal conductivity as floor materials. This study also suggested the proper impregnating condition, such as 10 minutes of the preliminary vacuum time, $187^{\circ}C$ of the heating temperature and 10 minutes of the maintaining pressure time at the pressure of 30kgf/$cm^2$. The produced composites showed 9 times higher density for small specimen, 6.6 times for actual size sample and great increase in bending strength from 102.05N/$mm^2$ to 189.47N/$mm^2$ for small size sample and to 205.4N/$mm^2$ for actual size sample, also great increase in hardness from 15.1N/$mm^2$ to 73.38N/$mm^2$ for small size sample and 64.87N/$mm^2$ for actual size sample. And the composites demonstrated great decrease in abrasion depth and in water absorption.

Assessment of Shear Band Characteristics in Granular Soils Using Digital Image Analysis Technique for Plane Strain Tests (평면변형률 시험에서 이미지 해석을 통한 사질토의 전단면 특성 평가)

  • Jang, Eui-Ryong;Jung, Young-Hoon;Kim, Jun-Young;Chung, Choong-Ki
    • Journal of the Korean Geotechnical Society
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    • v.27 no.4
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    • pp.51-65
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    • 2011
  • Shear banding, the localization of deformation into thin zones, has a quite practical relevance, as stability and deformation characteristics of earth structures are controlled by the soil behavior within the shear band. In this study, for understanding occurrence and developed pattern of shear band, plane strain compression tests were performed on three soils with different particle-size distribution under various conditions. Digital images were captured during the experiments; then, deformation of a specimen was evaluated by digital image analysis technique. The characteristics of a shear band were evaluated from the state shortly after post-peak occurrence to critical state. Additionally, the statistical procedure was developed to determine the reasonable thickness of a shear band.

Measurement of Mechanical Property and Thermal Expansion Coefficient of Carbon-Nanotube-Reinforced Epoxy Composites (탄소나노튜브로 강화된 에폭시 복합재료의 기계적 물성과 열팽창 계수 측정)

  • Ku, Min Ye;Kim, Jung Hyun;Kang, Hee Yong;Lee, Gyo Woo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.5
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    • pp.657-664
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    • 2013
  • By using shear mixing and ultrasonication, we fabricated specimens of well-dispersed multi-walled carbon nanotube composites. To confirm the proper dispersion of the filler, we used scanning electron microscopy images for quantitative evaluation and a tensile test for qualitative assessment. Furthermore, the coefficients of thermal expansion of several specimens having different filler contents were calculated from the measured thermal strains and temperatures of the specimens. Based on the microscopy images of the well-dispersed fillers and the small deviations in the measurements of the tensile strength and stiffness, we confirmed the proper dispersion of nanotubes in the epoxy. As the filler contents were increased, the values of tensile strength increased from 58.33 to 68.81 MPa, and those of stiffness increased from 2.93 to 3.27 GPa. At the same time, the coefficients of thermal expansion decreased. This implies better thermal stability of the specimen.