• Title/Summary/Keyword: Solvent evaporation

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증발을 고려한 Wafer Spin Coating 박막 예측에 관한 수치 해석적 연구

  • 노영미;임익태;김광선
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 2002.11a
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    • pp.20-26
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    • 2002
  • The fluid flow, mass transfer, heat transfer and film thickness variation during the spin coating process are numerically studied. The model is said to be 1-dimensional because radial variations in film thickness, concentration and temperature are ignored. The finite difference method is employed to solve the equations that are simplified using the similarity transformation. In early time film thinning is due to the radial convective outflow. However that slows during the first seconds of spinning so the film thinning due to evaporation of solvent becomes sole. The time various film thickness is analyzed according to the var ious solvent fraction in the coating liquid and in the bulk of the overlying gas and the temperature variation in the liquid film during the spin coating is estimated.

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Three-dimensional Printing of Shape Memory Alloys

  • Carreno-Morelli, E.;Martinerie, S.;Bidaux, J.E.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.256-257
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    • 2006
  • 3D printing of NiTi alloys has been successfully achieved. A novel printing process has been developed and used, which consists in selective deposition of a solvent on a granule bed. The granules are composed of metal powders and thermoplastic binder, which are mixed and sieved by conventional methods. A sound green strength is obtained after solvent evaporation. Sintered parts exhibit good density, proper phase composition and shape memory behaviour.

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Control of Encapsulation Efficiency and Initial Burst in Polymeric Microparticle Systems

  • Yeo, Yeon;Park, Ki-Nam
    • Archives of Pharmacal Research
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    • v.27 no.1
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    • pp.1-12
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    • 2004
  • Initial burst is one of the major challenges in protein-encapsulated microparticle systems. Since protein release during the initial stage depends mostly on the diffusional escape of the protein, major approaches to prevent the initial burst have focused on efficient encapsulation of the protein within the microparticles. For this reason, control of encapsulation efficiency and the extent of initial burst are based on common formulation parameters. The present article provides a literature review of the formulation parameters that are known to influence the two properties in the emulsion-solvent evaporation/extraction method. Physical and chemical properties of encapsulating polymers, solvent systems, polymer-drug interactions, and properties of the continuous phase are some of the influential variables. Most parameters affect encapsulation efficiency and initial burst by modifying solidification rate of the dispersed phase. In order to prevent many unfavorable events such as pore formation, drug loss, and drug migration that occur while the dispersed phase is in the semi-solid state, it is important to understand and optimize these variables.

Levan acetate를 이용한 hydrocortisone의 방출 제어

  • Im, Seung;Lee, Gi-Yeong;Kim, Dong-Un;Choe, Chun-Sun
    • 한국생물공학회:학술대회논문집
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    • 2001.11a
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    • pp.849-852
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    • 2001
  • The preparation, characterization and drug release behaviour of hydrocortisone(HC) loaded levan acetate microparticles were investigated. Hydrophobic levan acetate was prepared by chemical modification of hydrophilic levan and micro particles were made by dialysis method or solvent evaporation method. The morphology of levan acetate was observed by SEM and drug release profiles were investigated at pH 7.4 and pH 1.2. Newly synthesised levan acetate can be used for carrier of drugs.

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Development of New Fibers Related Sensitivity and Comfortability -Preparation of Polystyrene microcapsules containing Aqueous material and their Application- (감성기능 섬유신소재의 개발(II) -수용성 기능성물질 함유 폴리스티렌 마이크로캡슐의 제조와 섬유에의 응용-)

  • Hong, Ki Jeong;Park, Soo Min
    • Textile Coloration and Finishing
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    • v.9 no.3
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    • pp.33-41
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    • 1997
  • Polystyrene microcapsules were prepared by microencapsulation technique of solvent-evaporation. These microcapsules were characterized by Infrared spectroscopy, thermal analysis, scanning electron microscopy, and shape analysis. Fragrant water was used as a core material. Thermal and pH stabilities of polystyrene microcapsules were relatively excellent. And functional finishing on cotton fabric with microcapsules was applied.

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Thermal stability of polyaniline based conductive polymer blend (Polyaniline계 전도성 고분자의 열안정 특성)

  • 백운석;윤호규;서광석
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.11a
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    • pp.215-218
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    • 1998
  • The thermal stability of polyaniline-camphorsulfonic acid(PANI-CSA) film was studied as a function of temperature and time. A decrease in electrical conductivity of PANI-CSA film occurred when PANI-CSA film is subjected to temperature above 60$^{\circ}C$. From the result of thermogravimetry (TG), it was thought that the deterioration in electrical conductivity of PANI-CSA film was due to evaporation of water and residual solvent.

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Preparation of Microcapsules and Their Application (Poly (L-lactide) Microcapsule) (마이크로캡슐의 제조와 그 응용(폴리락티드 마이크로캡슐))

  • 홍기정;박수민
    • Textile Coloration and Finishing
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    • v.10 no.2
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    • pp.29-36
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    • 1998
  • Poly(L-lactide) microcapsules containing hydrophilic penetrate were prepared by interfacial precipitation method through solvent evaporation from w/o/w emulsion. Effect of four determinative process parameters on the particle size distributions, morphologies, and release properties of microcapsules coated with poly(L-lactide) was investigated. Moreover, susceptible functional cotton fabrics treated with the mentioned microcapsules were prepared and laundry test up to 15 times were done to determine fastness properties. As a result, the prepared poly(L-lactide) microcapsules with a more sharp-distributive, rounder, and more permeable membranes could be prepared by means of protective colloid concentration, solution volume and stirring rate.

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A theoritical study on spin coating technique

  • Tyona, M.D.
    • Advances in materials Research
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    • v.2 no.4
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    • pp.195-208
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    • 2013
  • A comprehensive theory of the spin coating technique has been reviewed and the basic principles and parameters controlling the process are clearly highlighted, which include spin speed, spin time, acceleration and fume exhaust. The process generally involves four stages: a dispense stage, substrate acceleration stage, a stage of substrate spinning at a constant rate and fluid viscous forces dominate fluid thinning behaviour and a stage of substrate spinning at a constant rate and solvent evaporation dominates the coating thinning behaviour. The study also considered some common thin film defects associated with this technique, which include comet, striation, chucks marks environmental sensitivity and edge effect and possible remedies.

Enhanced controlled transdermal release of quinupraqmine from the ethylene-vinyl acetate

  • Shin, Sang-Chul;Kim, Jin;Oh, In-Joon
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.230.1-230.1
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    • 2003
  • In case of oral application of quinupramine, antidepressants, it may cause adverse effects such as diarrhea, nausea due to transient high blood concentration. Ethylene vinyl acetate (EVA) which is heat-processible, flexible, inexpensive material was used for transdermal drug delivery. The purpose of this study was to develop the new transdermal delivery system of quinupramine using EVA polymer matrix that can provide sustained release and avoid the side effects. The EVA matrix containing quinupramine was prepared by solvent-evaporation method. (omitted)

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A Study on the Separation of n-Hexane by Molecular Sieve 5A and the Purification for HPLC use (분자체 5A를 이용한 n-헥산의 분리와 HPLC급으로의 정제에 관한 연구)

  • Choi, Beom Suk;Kim, Young Man;Kim, Sun Tae
    • Analytical Science and Technology
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    • v.6 no.1
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    • pp.21-27
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    • 1993
  • Technical grade n-hexane whose purity is 54% has been purified for HPLC use. Methylcyclopentane, 2-methylpentane, and 3-methylpentane which are hardly isolated by fractional distillation were separated by the liquid-solid chromatography using molecular sieve 5A. UV and fluorescence impurities whose contents are critically regulated for HPLC solvent were removed by the adsorptive separation with alumina and silica gel. The present method also reduced the impurities of color(APHA), acidity, water, residue after evaporation, sulfur, and thiophene content, and the impurity contents were well within the specifications of HPLC solvent.

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