• 제목/요약/키워드: Sintered properties

검색결과 1,953건 처리시간 0.021초

기계적합금화 공정에 의해 제조된 PbTe 소결체의 열전특성 (Thermoelectric Properties of PbTe Sintered Body Fabricated by Mechanical Alloying Process)

  • 이길근;정해용;이병우
    • 한국분말재료학회지
    • /
    • 제8권2호
    • /
    • pp.110-116
    • /
    • 2001
  • Abstract To investigate the effect of mechanical alloying process to thermoelectric properties of PbTe sintered body, Pb-Te mixed powder with Pb : Te : 1 : 1 composition was mechanically alloyed using tumbler-ball mill. Thermoelectric properties of the sintered body were evaluated by measuring of the Seebeck coefficient and specific electric resistivity from the room temperature to 50$0^{\circ}C$. Sintered body of only mechanically alloyed PbTe powder showed p-type behavior at the room temperature, and occurred type transition from p-type to n-type at about 30$0^{\circ}C$. PbTe sintered body which was fabricated using heat treated powder in $H_2$ atmosphere after mechanical alloying showed stable n-type behavior under 50$0^{\circ}C$. N-type PbTe sintered body fabricated by mechanical alloying process had 4 times higher power factor than that fabricated by the melt-crushing process. Application of a mechanical alloying process to fabricate of n-type PbTe thermoelectric material seemed to be useful to increase the power factor of PbTe sintered body.

  • PDF

Influence of Cooling Condition of Casted Strips on Magnetic Properties of Nd-Fe-B Sintered Magnets

  • Jung, Hwaebong;Kim, Sumin;Moon, Hongjae;Oh, Yoon S.;Lee, Young-Joo;Lee, Hyun-Sook;Lee, Wooyoung
    • Metals and materials international
    • /
    • 제24권6호
    • /
    • pp.1422-1431
    • /
    • 2018
  • We investigated the additional (secondary) cooling effect of casted strips on the magnetic properties of Nd-Fe-B sintered magnets. The Nd-Fe-B sintered magnets were fabricated with the casted strips prepared without and with additional cooling. Additional cooling was achieved by blowing Ar gas at various pressures (0.1, 0.3, and 0.6 MPa) on the free-side surface of the strips during the strip-casting process. The higher magnetic properties of $H_c$, $B_r$, and $(BH)_{max}$ of the final Nd-Fe-B sintered magnets were obtained for 0.1 MPa rather than for 0.0 MPa. The best microstructure of the columnar grains in the casted strips was produced with the aid of a lower pressure of gas on the free-side surface. It was found that the microstructure of the strips affects the distribution of grains grown in the sintered magnets. This report demonstrates that the improved magnetic performance of Nd-Fe-B sintered magnets was achieved via additional gas cooling.

사출성형 및 열간가압 소결법으로 제작된 지르코니아 세라믹 임플란트의 소결물성 및 미세구조적 결함 (Sintered Properties and Microstructural Defects of Zirconia Ceramic Implant Fabricated by Injection Molding and Hot Isostatic Pressing (HIP))

  • 박현정;박정식;이종국
    • 열처리공학회지
    • /
    • 제36권4호
    • /
    • pp.215-222
    • /
    • 2023
  • 3Y-TZP (3 mol% yttria-stabilized tetragonal zirconia polycrystals, 3Y-TZP) ceramics are emerging as dental implant materials due to their superior optical and mechanical properties as well as excellent biophysical properties, in spite of low bioactivity. In this study, we investigated to sintered properties and microstructural defects of dental zirconia implants fabricated by ceramic injection molding and post-HIP (Hot isostatic pressing) processing and analyzed the processing parameters related with the obtainment of its high sinterd density. Sintered and microstructural parameters, i.e, apparent density, grain size and phase composition of zirconia implants fabricated by injection molding were dependent on the fixtute size and implant type. Maximum sintered density of 99.2% and minimum grain size of 0.3-0.4 ㎛ were obtained from large-scaled 2-body sample. In 1-body ceramic implant, high sintered density of 99.5% was obtained, but it had a little monoclinic phase and wide grain size distribution.

The Application of P/M Advanced Techniques to Sintered Gears

  • Chongxi, Bao;Zhouqiang, Shen;Zhengping, Shu
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
    • /
    • pp.987-988
    • /
    • 2006
  • The processes of P/M affect the properties of sintered gears. The different techniques of P/M lead to the different properties of sintered gears. This paper summarizes new progress in powder metallurgy for sintered gears. These progresses include warm compaction, high velocity compaction, sinter hardening, high temperature sintering, infiltration, CNC powder press and surface densification etc.

  • PDF

Barium Hexaferrite 폐자석의 재활용 (Recycling of Waste Barium Hexaferrite Magnets)

  • 박인용
    • 자원리싸이클링
    • /
    • 제9권2호
    • /
    • pp.18-25
    • /
    • 2000
  • 등방성 영구자석의 제조과정에서 발생되고 있는 barium hexaferrite 폐 자석으로 소결체를 제조하여 물리적, 자기적 특성을 조사하였다. 소결체는 XRD, XRF, SEM 및 자기적 성질을 측정하였다 폐 영구자석을 분쇄하고 조립화하여 폐 영구자석 분말 과립과 시판용 과립을 일정비율로 혼합. 성형하고 소결하였다. 폐 영구자석 분쇄분말의 함량에 따라 자기적 특성은 점차 감소하지만 소결 온도 $1150~1200^{\circ}C$ 에서 영구자석으로서 요구되는 자기적 특성값을 나타내었다.

  • PDF

비소성 황토를 치환한 고강도 콘크리트의 고온 역학적 특성 평가를 위한 초음파 속도 분석 (Ultrasonic pulse velocity analysis for high- temperature mechanical properties of high strength concrete replacing non-sintered hwangto )

  • 김태형;김원창;이태규
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2023년도 가을학술발표대회논문집
    • /
    • pp.273-274
    • /
    • 2023
  • In this study, ultrasonic pulse velocity was analyzed to evaluate the high-temperature mechanical properties of concrete mixed with non-sintered hwangto. The W/B of the specimens was set at 0.41, the percentage of non-sintered hwangto admixture was set at two levels of 15,30%. The target temperature of the specimen is set to 6 levels of 20, 100, 200, 300, 500, 700 ℃, and the heating rate is set to 1℃/min. The result showed that the amount of non-sintered hwangto incorporated into the concrete tends to results in lower compressive strength. Ultrasonic pulse velocity showed similar trends, but differed in some areas.

  • PDF

분말입도에 따른 Nd-Fe-B 소결자석의 미세조직 변화 및 자기적 특성 (Microstructure and Magnetic Properties of Nd-Fe-B Sintered Magnet with the Variation of Particle Size)

  • 신동원;김동환;박영철;김정곤
    • 한국분말재료학회지
    • /
    • 제23권6호
    • /
    • pp.447-452
    • /
    • 2016
  • Neodymium-iron-boron (Nd-Fe-B) sintered magnets have excellent magnetic properties such as the remanence, coercive force, and the maximum energy product compared to other hard magnetic materials. The coercive force of Nd-Fe-B sintered magnets is improved by the addition of heavy rare earth elements such as dysprosium and terbium instead of neodymium. Then, the magnetocrystalline anisotropy of Nd-Fe-B sintered magnets increases. However, additional elements have increased the production cost of Nd-Fe-B sintered magnets. Hence, a study on the control of the microstructure of Nd-Fe-B magnets is being conducted. As the coercive force of magnets improves, the grain size of the $Nd_2Fe_{14}B$ grain is close to 300 nm because they are nucleation-type magnets. In this study, fine particles of Nd-Fe-B are prepared with various grinding energies in the pulverization process used for preparing sintered magnets, and the microstructure and magnetic properties of the magnets are investigated.

Influence of Nitrogen/Hydrogen Atmospheres on Sintered Properties of P/M Components

  • Philips, Thomas;Koh, Kyung-Sug
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
    • /
    • pp.818-819
    • /
    • 2006
  • The effect of individual gas constituents in a sintering atmosphere is examined to optimize the sintered properties of Iron-Carbon P/M components. The influence of sintered properties is reviewed as a function of hydrogen percentages and dew point in the sintering zone. Microstructures, porosity, pore morphology and dimensional changes are the subject of this review. The effects of CO containing atmospheres are compared against the non CO atmospheres in terms of hardness, carbon control and dimensional changes.

  • PDF

Development of Sintered Parts for Variable Valve Timing Unit

  • Nishita, Takashi
    • 한국분말야금학회:학술대회논문집
    • /
    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
    • /
    • pp.690-691
    • /
    • 2006
  • Variable valve timing unit, which is able to decrease environmental load and improve fuel economy is loaded onto many automobiles recently. This unit consists mainly of sprocket, housing and rotor. These parts are requested different properties according to environment. We produce sintered parts for variable valve timing unit by selecting compact, sinter process and special treatment according to demanded properties. In this paper, demanded properties of sintered parts for variable valve timing unit and adopted technique to satisfy them are presented.

  • PDF

$CdZnS_{1-y}Te_{y}$ 소결막의 전기 및 광학적 성질 (Electrical and Optical Properties of Sintered $CdZnS_{1-y}Te_{y}$ films)

  • 최용우;임호빈
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 1991년도 추계학술대회 논문집
    • /
    • pp.17-19
    • /
    • 1991
  • Pastes consisting of $CdZnS_{1-y}Te_{y}$ powder, 20wt/o of $CdCl_2$as a sintering aid and appropriate amount of Propylene Glycol(P.G) have been coated on glass substrates and were sintered at the temperature of $625^{\circ}C$ to find energy band gap, transmittance and electrical properties of the sintered films. The resistivity of sintered film increases with increasing Te content. X-ray diffraction patterns show that $CdZnS_{0.9}Te_{0.1}$ sintered film is in the single film in the two phase region. The transmittance of the sintered film decreases with increasing the Te content.