• Journal of Powder Materials
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• v.22 no.4
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• pp.240-246
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• 2015

Anodic aluminum oxide (AAO) has been widely used for the development and fabrication of nano-powder with various morphologies such as particle, wire, rod, and tube. So far, many researchers have reported about shape control and fabrication of AAO films. However, they have reported on the shape control with different diameter and length of anodic aluminum oxide mainly. We present a combined mild-hard (or hard-mild) anodization to prepare shape-controlled AAO films. Two main parameters which are combination mild-hard (or hard-mild) anodization and run-time of voltage control are applied in this work. The voltages of mild and hard anodization are respectively 40 and 80 V. Anodization was conducted on the aluminum sheet in 0.3 mole oxalic acid at $4^{\circ}C$. AAO films with morphologies of varying interpore distance, branch-shaped pore, diameter-modulated pore and long funnel-shaped pore were fabricated. Those shapes will be able to apply to fabricate novel nano-materials with potential application which is especially a support to prevent volume expansion of inserted active materials, such as metal silicon or tin powder, in lithium ion battery. The silicon powder electrode using an AAO as a support shows outstanding cycle performance as 1003 mAh/g up to 200 cycles.

• Transactions of Materials Processing
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• v.29 no.5
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• pp.241-250
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• 2020

In this study, the methodology of the springback prediction of automotive parts applied 3rd generation AHSS was investigated using the response surface model analysis based on a regression model, and the meta model analysis based on a Kriging model. To design the learning data set for constructing the springback prediction models, and the experimental design was conducted at three levels for each processing variable using the definitive screening designs method. The hat-shaped member, which is the basic shape of the member parts, was selected and the springback values were measured for each processing type and processing variable using the finite element analysis. When the nonlinearity of the variables is small during the hat-shaped member forming, the response surface model and the meta model can provide the same processing parameter. However, the accuracy of the springback prediction of the meta model is better than the response surface model. Even in the case of the simple shape parts forming, the springback prediction accuracy of the meta model is better than that of the response surface model, when more variables are considered and the nonlinearity effect of the variables is large. The efficient global optimization algorithm-based Kriging is appropriate in resolving the high computational complexity optimization problems such as developing automotive parts.

• Proceedings of the KWS Conference
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• 2009.11a
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• pp.20-20
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• 2009

저항 점 용접은 1930년대에 Thomson에 의해 방법이 제안된 이후로 자동차, 전자, 항공기, 철도산업등에서 박판 금속(sheet metal)의 접합에 가장 널리 사용되고 있는 공정이다. 특히 자동차 차체와 같이 대부분 박판으로 구성되는 구조물에서는 저항 점 용접의 사용 범위가 매우 넓기 때문에 자동차 산업에서는 가장 기본적인 근본 기술 중의 하나로 인식되고 있다. 보통 자동차 한대를 생산하는데 소요되는 저항 점 용접 타점은 3000~4000개 정도로 자동차 차체 용접 공정의 대부분을 차지하고 있다. 또한 로봇과 연동된 자동화 공정으로 적용되고 있다. 최근의 자동차 차체를 구성하는 금속 재료가 자동차의 경량화, 친화경 소재의 사용자의 요구로 인해 새로운 강판이 사용된다. 자동차의 연비 향상을 위해서 다른 방법보다 자동차의 무게를 감소시키는 것이 가장 효율적이고, 쉽기 때문에 고장력 강판의 사용이 급속하게 증가하고 있다. 뿐만 아니라 차제의 부식성, 내마모성 향상을 위해 도금 처리된 강판의 사용도 활발하게 이루어지고 있다. 최근에 도장 공정 감소를 위해 도금 처리위에 도료 착색을 용이하게 하는 도료의 일부를 금속 표면에 처리된 강판의 개발도 진행되는 등 금속 소재의 변화가 다양하게 진행되고 있다. 이러한 새로운 강종은 기존의 AC 용접이나 DC 용접으로는 용접성 확보에 어려움을 가지고 있어, 새로운 저항 점 용접 공정의 연구 개발이 필요하다. 본 연구에서는 저항 점 용접 공정의 개선을 위해서 인버터 저항 점 용접기에서 용접 공정 중 전류를 제어하기 위한 효율적인 제어기 개발 방법과 개발된 제어기를 바탕으로 용접 중에 용접부의 품질을 예측하여, 용접 전류 및 가압력을 실시간 제어하여 안정적인 용접부의 품질을 갖질 수 있는 지능형 저항 점 용접기의 적응 제어기를 개발하는데 있다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.37 no.10
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• pp.1239-1249
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• 2013

In this study we establish a process to predict hardening behavior considering the Bauschinger effect for zircaloy-4 sheets. When a metal is compressed after tension in forming, the yield strength decreases. For this reason, the Bauschinger effect should be considered in FE simulations of spring-back. We suggested a suitable specimen size and a method for determining the optimum tightening torque for simple shear tests. Shear stress-strain curves are obtained for five materials. We developed a method to convert the shear load-displacement curve to the effective stress-strain curve with FEA. We simulated the simple shear forward/reverse test using the combined isotropic/kinematic hardening model. We also investigated the change of the load-displacement curve by varying the hardening coefficients. We determined the hardening coefficients so that they follow the hardening behavior of zircaloy-4 in experiments.

• Journal of the Korean Society for Precision Engineering
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• v.16 no.4 s.97
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• pp.57-63
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• 1999

A thin metal plate such as detent spring has the shape deformation due to the phenomenon of spring back after press machining and heat treatment process. This requires the correction of spring shape and force in final inspection process. To do correction of the shape deformation the impact force is manually applied to the bended part of detent spring after measuring the shape deformation and spring force. To develop the automatic spring force correction system, applied force of occurring plastic deformation must be derived from the experimental method. But frequent change of spring shape and material makes it difficult to accomplish the experimental method to be applied. This paper describes the analytical method for detent spring force correction system is to be substituted for the experimental method. FEM(Finite Element Method) is used to find the boundary value between elastic and plastic deformation in the analytical method. To confirm the validity of the analytical method, the result of two methods is compared each other at various applied force conditions. It shows that the simulation result of the analytical method is consistent with the result of the experimental method within the error bound ${\pm}$5%. The result of this paper is useful for development of the automatic spring correction system and reduction of the complicated and tedious processes involved in experimental method.

• Korean Journal of Materials Research
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• v.14 no.6
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• pp.402-406
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• 2004

$WSi_2$, $TiSi_2$, $CoSi_2$, and $TaSi_2$ are general silicides used today in semiconductor devices. $WSi_2$ thin films have been proposed, studied and used recently in CMOS technology extensively to reduce sheet resistance of polysilicon and $n^{+}$ region. However, there are several serious problems encountered because $WSi_2$ is oxidized and forms a native oxide layer at the interface between $WSi_2$ and $Si_3$$N_4$. In this study, we have introduced 20 $slm-N_2$ gas from top to bottom of the furnace in order to control native oxide films between $WSi_2$ and $Si_3$$N_4$ film. In resulting SEM photographs, we have observed that the native oxide films at the surface of $WSi_2$ film are removed using the long injector system.

• International Journal of Automotive Technology
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• v.5 no.1
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• pp.55-59
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• 2004

Spot welding is a very important and useful technology in fabrication of thin sheet structures such as the parts in an automobile. However, because the fatigue strength of the spot welding point is considerably lower than that of the base metal due to stress concentration at the nugget edge, the nugget size must be estimated to evaluate a reasonable fatigue strength at a spot welded lap joint. So far, many investigators have experimentally studied the estimation of fatigue strengths of various spot weldments by using a destructive method. However, these destructive methods poses problems so testing of weldments by these methods are difficult. Furthermore, these methods cannot be applied to a real product, and are time and cost consuming, as well. Therefore, there has been a strong, continual demand for the development of a nondestructive method for estimating nugget size. In this study, the effective nugget size in spot weldments have been analyzed by using thermoelastic stress analysis adopting infrared thermography. Using the results of the temperature distribution obtained by analysis of the infared stress due to adiabatic heat expansion under sinusoidal wave stresses, the effective nugget size in spot welded specimens were estimated. To examine the evaluated effective nugget size in spot weldments, it was compared with the results of microstructure observation from a 5％ Nital etching test.

• Proceedings of the Korean Vacuum Society Conference
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• 2013.02a
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• pp.299-299
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• 2013

Indium Tin Oxide (ITO) has widely been used as a transparent conductive oxide (TCE) for photovoltaic devices. Lately, flexibility of ITO becomes an issue as demand of flexible device increases. Several scientists have tried to substitute ITO to different materials such as conductive polymer, graphene, CNT, and metal nanowire because of ITO brittleness. Among the substitute materials, PEDOT:PSS has mostly paid attention because PEDOT:PSS has excellent flexibility and good conductivity. The conductivity of PEDOT:PSS increases up to 1000 S/cm with additives such as DMSO, EG, sorbitol, and so on. In our research group, we introduce a conductive polymer PEDOT:PSS as a buffer layer to improve not only flexibility but also conductivity. As PEDOT:PSS layer forms beneath ITO thin film (20 nm), sheet resistance decreases from $230{\Omega}$/${\Box}$ to $85{\Omega}$/${\Box}$ and crack initiation decreases from 4.5 mm to 3.5 mm as well. We have fabricated organic photovoltaic device and power conversion efficiencies using conventional ITO electrode and ITO/PEDOT:PSS hybrid electrode. The photovoltaic property such as power conversion efficiency for ITO/PEDOT:PSS hybrid electrode is comparable to the value obtained using conventional ITO electrode on glass substrate.

• Structural Engineering and Mechanics
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• v.44 no.6
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• pp.839-856
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• 2012

To enable remodeling of the exterior of buildings more convenient, such finishing materials as curtain walls, metal panels, concrete panels or dry stones need to be easily detached. In this respect, this study proposed a new design of the slab for the purposes. In the new design, the sides of the slab were properly modified, and the capabilities of anchors fixed in the modified slab were experimentally tested. In details, a number of concrete specimens with different sizes and compressive strengths were prepared, and the effect of anchors with different diameters and embedment depths applied in the concrete specimens were tested. The test results of the maximum capacities of the anchors were compared with the number of current design codes and the stress distribution was identified. This study found that the embedment depth specified in the current design code (ACI318-08) should be revised to be more than 1.5 times the edge distance. However, with the steel sheet reinforcement, the experiment acquired higher tensile strength than the design code proposed. In addition, for two types of specimens in the tensile strength experiment, the current design code (ACI 318-08) is overestimated for the anchor depth of 75 mm. This study demonstrated that the ideal breakout failure was attainable for the side slot details of a slab with more than 180 mm of a slab thickness and less than 75 mm of an anchor embedment depth. It is expected that these details of the modified slab can be specified in the upgraded construction design codes.

• Journal of Adhesion and Interface
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• v.12 no.1
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• pp.34-42
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• 2011

The roll coating process is well-known for completely replacement coating system with an existing wet paint process for automotive which has low productivity and is not environment-friendly process. It is very important to evaluate the curing behavior, corrosion resistance and processing property as well as rheological behavior in order to realize a film flexibility and hardness simultaneously. In this study, we have synthesized the polyester resin modified with hydroxyl values and molecular weight to apply the pre-painted system, and then evaluated the curing behavior, deep drawing, tensile strength and rheological properties. It was observed that N-0375-40 of 40 (mg KOH/mol) hydroxyl values showed the most suitable for flexibility, film hardness, and curing behavior.