• Title/Summary/Keyword: Separation condition

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Evaluation of Structural Integrity of Crossover Leg Piping System with Dynamic Whip Restraints (원자로냉각재계통 중간배관과 동적거동 구속장치와의 접촉으로 인한 배관 건전성 평가)

  • Yang, J.S.;Kim, B.N.;Oh, S.K.;Oh, C.H.;Lee, D.H.
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.636-643
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    • 2001
  • Interference between the crossover leg of the reactor coolant system (RCS) and the pipe whip restraints (PWR) has brought a degradation issue of the integrity of the Reactor Coolant System in Westinghouse type nuclear power plants (NPPs) of Korea. According to the gap Inspect ion carried out during planned overhaul (Year 2000), interference between the crossover leg and the PWR was found in each RCS loop. This plant has had the high vibration problem on the RC pump 'B'. The reason for the high vibration in the RC pump 'B' had been massively surveyed and it was found that the crossover leg of RCS contacted with the PWR in hot condition. Since the contact between the crossover leg and the PWR changes the dynamic characteristics of the piping system for the RCS, this is considered as one reason for the high vibration. And a possibility of overstress on the crossover leg due to the contact with the PWR should be evaluated. Through performing RCS integrity analyses, subsequent actions were initiated to increase the gap between those parts. As the results of the appropriate separation between two parts, it was reported that there was no unusual noise or vibration during plant heat-up. In this paper, the evaluations for the gap between the crossover leg and the PWR and the structural integrity due to loop binding is described.

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Determination of Ginseng Saponins by Reversed-Phase High Performance Liquid Chromatography (역상 고속액체크로마토그라피를 이용한 홍삼 사포닌의 정량)

  • Kim, Cheon-Suk;Kim, Se-Bong
    • Korean Journal of Medicinal Crop Science
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    • v.9 no.1
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    • pp.21-25
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    • 2001
  • Major saponins in ginseng were analysed using reverse phase high performance liquid chromatography with binary mobile phase gradient control system instead of normal phase column. The optimum condition were as following : reverse phase column; ${\mu}{\beta}ondapak\;C_{18}$ column (Waters, $3.9mm{\times}300\;mm,\;5{\mu}m$), methyl cyanaide/water binary mobile phase gradient control system, solvent flow rate; 1.5 ml/min, and UV($203{\mu}m$ ) detector. The complete separation of ginsenoside $Rb_1,\;Rb_2,\;Rc,\;Rd,\;Re,\;Rf\;and\;Rg_1$ was achieved within 55 min. The Regression coefficients of the calibration curves for seven ginsenosides were 0.99.

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Separation Characteristics of Barium Ion in Water Using Capacitive Deionization (CDI) Process (축전식탈염(CDI) 공정을 이용한 수용액 중 바륨 이온 분리 특성 연구)

  • Nam, Dong Hyun;Rhim, Ji Won
    • Membrane Journal
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    • v.29 no.6
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    • pp.355-361
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    • 2019
  • We studied the removal of barium ions that may be contained in industrial wastewater using the existing capacitive deionization (CDI). The 30 mg/L BaCl2 (barium chloride dihydrate) solution was used as the feed solution, and the flow rate was set to 10 mL/min. The adsorption conditions were varied from 1.2 V to 3, 5 and 7 min, and the desorption conditions were -1, -1.5, -2 V and 1, 2 and 3 min, respectively, to select the most efficient conditions. As a result, barium ion removal efficiency of 64.4% was obtained under the adsorption conditions of adsorption of 1.2 V/7 min and the desorption -1 V/1 min. For the desorption voltages and time, under the same experimental conditions, the removal efficiency of CDI for 30 mg/L NaCl aqueous solution with the same concentration as barium showed 69.9% removal efficiency under the adsorption conditions of and the desorption conditions of 1.2 V/7 min desorption -1 V/1 min, respectively.

Separation and Performance lest of Wnitening Agent in Rhodiola Sachalinensis (홍경천에 포함된 미백성분의 분리 및 성능검사)

  • 최두영;안소영;이승기;한정선;김은철;이향복;신정현;김은기;노경호
    • KSBB Journal
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    • v.19 no.3
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    • pp.169-173
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    • 2004
  • The Rhodiola Sachalinensis 5 g were mixed and extracted with methanol 150 $m\ell$ at the room temperature for 12 h. The effluents were collected and grouped into the two. Un this experimental condition, the mobile phase composition were linearly changed as follows; water/methanol : 90/10 - 30/70 (vol. %, for 5 min), 30/70 - 10/90 (vol. %, for 15 min) and an analytical column (3.9 ${\times}$ 25 em, 15 $\mu\textrm{m}$ particle size, and 300 ${\AA}$ pore size) was utilized. The performance of the extracted Rhodiola Sachalinensis as a whitening agent was not favorable, so it classifies the Rhodiola Sachalinensis extractions with two fractions and collects each fraction for whitening agent assay. For the in-vivo melanin production ratio assay that used melanin-a cell in 10 ppm concentration, it was 58.6%, the first fraction of the effluents collected between 1.0 and 4.0 min, while it was 60% between 10.4 and 17.6 min for the second fraction, which were more efficient than that of arbutin, 45.6%.

Effect of Alloying Elements on the Microstructure and Texture of the Secondary Ingots made by Al Used Beverage Cans (알루미늄 폐캔을 이용한 2차지금의 미세조직 및 집합조직에 미치는 합금원소의 영향)

  • 박차용;고흥석;강석봉
    • Resources Recycling
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    • v.9 no.2
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    • pp.46-52
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    • 2000
  • Aluminum can to can recycling was divided into two stpes. The first step was composed of the processes such as collection of used beverage cans (UBC), shredding, magnetic separation, De-laquiring, melting and casting. The second one was remelting and casting, heat treating, hot and cold rolling, annealing, and can making. In this study, the effect of alloying elements on the microstructure and texture of the secondary ingots made by Al UBC was investigated. In aluminum can to can recycling, the second phase particles appeared in the solidification stage must be controlled by heat treatment. The optimum heat treatment condition was $615^{\circ}C$ for 5hrs. the texture in hot rolled sheet was depressed with increasing Mn content, on the other hand, Si and Fe elements promoted the texture development. The textures of can-body sheet should be controlled in the hot rolling and annealing stage because can was formed from cold rolled sheet without heat treatment.

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Sulfuric Acid Leaching of Zinc and Manganese from Spent Zinc-Carbon Battery (황산에 의한 폐망간전지로부터 아연과 망간의 침출)

  • Sohn Hyun-Tae;Ahn Jong-Gwan;Sohn Jeong-Soo;Park Kyoung-Ho;Park In-Yong
    • Resources Recycling
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    • v.11 no.4
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    • pp.44-50
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    • 2002
  • Characteristics on the sulfuric acid leaching of zinc and manganese from the spent zinc-carbon battery powders obtained by cushing and magnetic separation, were investigated with the variation of sulfuric acid concentration, reaction temperature, stir-ring speed and solid/liquid ratio. The sample powders were composed of Zn metal, ZnO, $MnO_2$ and $Mn_2$$O_3$. and it was found that the selective leaching of zinc was difficult in this system. At the condition of S/L ratio 1:10, IM H$_2$$SO_4$, $60^{\circ}C$ and 200 rpm, leaching rate of Zn and Mn are 92% and 35% respectively. The concentration of Zn and Mn in the leaching solution are 19.5 g/l, 7.8 g/l and pH of that solution is 0.75. It was confirmed at reducing agent should be added to increase e leaching rate of manganese with sulfuric acid.

Efficient Usage of Secondary Scramble Code via Optical Repeater in W-CDMA System (W-CDMA 시스템에서 광중계기를 이용한 secondary-스크램블 코드의 효율적 활용방안에 대한 연구)

  • Jeon, Eun-Sung;Park, Jun-Hyo;Yang, Jang-Hoon;Kim, Dong-Ku
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.34 no.8C
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    • pp.731-741
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    • 2009
  • Optical repeater is often installed at the isolated area. Spatial separation makes it possible to reduce the inter-code interference when secondary scrambling codes are used for traffic connected through repeater. In this paper, we propose five secondary scrambling code usage scenarios with the aids of optical repeater to maximize the user capacity. In order to evaluate the performance, dynamic system level simulation is performed. We also propose a base station-repeater switching where each active users can change access points by comparing the channel condition from base station and repeater thorough secondary common pilot channel (S-CPICH) signal to noise-interference ratio (SINR). Moreover, primary-secondary scramble code replacing scheme is proposed which replaces secondary scramble code with primary scramble code when a call using primary scramble code is ended and its corresponding OVSF code is available to users using the secondary scramble code

A study on treatment of emulsified oil waste water in vessels by electrochemical treatment system (전기화학적 처리장치에 의한 유화된 선저폐수의 처리에 관한 연구)

  • Kwon K. S.;Jeong H. J.;Lee B. H.
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.6 no.3
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    • pp.45-53
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    • 2003
  • Discharging untreated bilge to the ocean is a cause of marine pollution. In general, bilge water contains free and/or emulsified forms of oil. Free form of oil can easily be separated by gravimetric flotation and/or proper filtration processes. However, those simple physicochemical processes could not separate emulsified oil without adding proper chemicals. Electrolytic flotation is one of promising technologies able to fulfill the effluent standard requirement, which is below 15 ppm of oil content. In this research, Electrochemical process consisting of electrochemical flotation basin was studied for the treatment of emulsified oil. In order to estimate, the effectiveness of oil separation equipment influent concentration of oil and HRT(Hydraulic retention time) were considered. Also, lab-scale electrochemical process was designed and operated in the condition of various HRT, current density, and electrode gap. Through the research, following results were obtained. From the experiment of bench scale electrochemical treatment process, it was demonstrated that the emulsified oil was treated effectively and the removal efficiency of emulsified oil from wastewater was increased with HRT and current density.

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Comprehensive proteome analysis using quantitative proteomic technologies

  • Kamal, Abu Hena Mostafa;Choi, Jong-Soon;Cho, Yong-Gu;Kim, Hong-Sig;Song, Beom-Heon;Lee, Chul-Won;Woo, Sun-Hee
    • Journal of Plant Biotechnology
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    • v.37 no.2
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    • pp.196-204
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    • 2010
  • With the completion of genome sequencing of several organisms, attention has been focused to determine the function and functional network of proteins by proteome analysis. The recent techniques of proteomics have been advanced quickly so that the high-throughput and systematic analyses of cellular proteins are enabled in combination with bioinformatics tools. Furthermore, the development of proteomic techniques helps to elucidate the functions of proteins under stress or diseased condition, resulting in the discovery of biomarkers responsible for the biological stimuli. Ultimate goal of proteomics orients toward the entire proteome of life, subcellular localization, biochemical activities, and their regulation. Comprehensive analysis strategies of proteomics can be classified as three categories: (i) protein separation by 2-dimensional gel electrophoresis (2-DE) or liquid chromatography (LC), (ii) protein identification by either Edman sequencing or mass spectrometry (MS), and (iii) quanitation of proteome. Currently MS-based proteomics turns shiftly from qualitative proteome analysis by 2-DE or 2D-LC coupled with off-line matrix assisted laser desorption ionization (MALDI) and on-line electrospray ionization (ESI) MS, respectively, to quantitative proteome analysis. Some new techniques which include top-down mass spectrometry and tandem affinity purification have emerged. The in vitro quantitative proteomic techniques include differential gel electrophoresis with fluorescence dyes, protein-labeling tagging with isotope-coded affinity tag, and peptide-labeling tagging with isobaric tags for relative and absolute quantitation. In addition, stable isotope labeled amino acid can be in vivo labeled into live culture cells through metabolic incorporation. MS-based proteomics extends to detect the phosphopeptide mapping of biologically crucial protein known as one of post-translational modification. These complementary proteomic techniques contribute to not only the understanding of basic biological function but also the application to the applied sciences for industry.

Isolation and Quantitative Analysis of Cinnamtannin B-1 from Osmunda japonica Thunb (고비로부터 Cinnamtannin B-1의 분리 및 함량 분석)

  • Kim, Min Suk;Woo, Kyeong Wan;Lee, Ki Ho;Lee, Hyun Joo;Lee, Seon Yu;Kang, Byoung Man;Jeon, Byung Hun;Cho, Jung Hee;Cho, Hyun Woo
    • Korean Journal of Pharmacognosy
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    • v.47 no.3
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    • pp.232-236
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    • 2016
  • In traditional Korean medicine, Osmunda japonica Thunb has been used as hemostasis and antipyretic treatment. The main compound "cinnamtannin B-1" was obtained by column chromatographic separation, and its structure was determined by spectroscopic methods, including $^1H$, $^{13}C$ NMR, and IT-TOF-ESI MS. Ash, moisture and extract content and acidinsoluble ash were monitored as identification test to establish the analytical methods. The optimum reflux extraction condition was 100% methanol extracted 30 min for 2 times. A quantitative analysis using HPLC method exhibited that the main compound at 24.7 min and its content was 0.96% in methanol extraction.