• 대한화장품학회지
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• 제34권1호
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• pp.9-14
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• 2008

오일/수첨 레시틴/물 계에서 전단력이 다른 두 혼합기로 제조된 나노에멀젼의 안정성에 대하여 연구하였으며, 계면활성제의 농도에 따른 나노에멀젼의 입자 크기와 안정성을 조사하였다. 입자의 크기는 광산란법에 의하여 측정하였으며 입자크기의 시간에 따른 변화를 관찰하였다. 실험 결과 나노 에멀젼 불안정화 과정은 Ostwald ripening에 의해 지배되었다. 입자 크기가 100~200nm 범위에서는 오일에 대한 계면활성제의 비율이 증가함에 따라 안정성이 감소하였으나 입자 크기가 300~400nm의 범위에서는 반대의 경향을 보였다.

• 한국전기전자재료학회논문지
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• 제17권11호
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• pp.1218-1223
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• 2004

Porous silicon materials have been shown to have bright prospects for applications in light emitting, solar cell, as well as light- and chemical-sensing devices. In this report, structures of porous silicon prepared by anodic etching in HF-based solution with various etching times were studied in detail by Atomic Force Microscopy and Small Angle X -ray Scattering technique using the high energy beam line at Pohang Light Source in Korea. The results showed the coexistence of the various pores with nanometer and submicrometer scales. For nanameter size pores, the mixed ones with two different shapes were identified: the larger ones in cylindrical shape and the smaller ones in spherical shape. Volume fractions of the cylindrical and the spherical pores were about equal and remained unchanged at all etching times investigated. On the whole uniform values of the specific surface area and of the size parameters of the pores were observed except for the larger specific surface area for the sample with the short etching time. The results implies that etching process causes the inner surfaces to become smoother while new pores are being generated. In all SAXS data at large Q vectors, Porod slope of -4 was observed, which supports the fact that the pores have smooth surfaces.

• 한국초전도ㆍ저온공학회논문지
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• 제9권4호
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• pp.24-27
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• 2007

The purpose of this work is to develop, integrate, and implement an optical characterization method to evaluate physical properties in coated conductors and investigate the local distribution of the causes of degraded performance. The method that we selected at this moment is Raman scattering spectroscopy, which is accompanied with measurements of local supercurrent transport, phase composition, microstructure, and epitaxy quality for coated conductors that range in size up to multi-meter-length tapes and that embrace the entire tape embodiment (substrate through cap layer). The establishment of Raman spectroscopy as an on-line process monitoring tool is our eventual goal of research, but it requires very robust and cost-effective equipments. We analyzed $YBa_2Cu_3O_7(YBCO)$ thin films grown at various substrate temperatures by using Raman spectroscopy. YBCO films were grown by a high-rate electron-beam co-evaporation method. Raman spectra of YBCO films with lower-transport properties exhibit additional phonon modes at ${\sim}300cm^{-1}$, ${\sim}600cm^{-1}$ and ${\sim}630cm^{-1}$, which are related to second-phases such as $Ba_2Cu_3O_{5.9}$ and $BaCuO_2$. We propose a new method to characterize Raman spectra of coated conductors for an in-line quality control.

• Journal of Welding and Joining
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• 제33권2호
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• pp.8-13
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• 2015

This study was carried out to evaluate mechanical properties of the jointed Al6061/HT590 alloys by friction stir welding (FSW). FSW was conducted under the conditions with tool rotating speed of 500 RPM and traveling speed of 300 mm/min., where Ar gas was introduced to prevent the materials from corrosion during the welding process. Electron back-scattering diffraction (EBSD) was used to characterize microstructures such as grain size, misorientation angle and crystal orientation. Evolution of intermetallic compounds in Al6061 during the process were examined in terms of morphology, size and aspect ratio at three distinct zones Al base material, heat affected zone and stir zone, where transmission electron microscope (TEM) was used. It was revealed that FSW gave rise to refinement of grains as well as growth of intermetallic compounds in Al6061. The morphological changes of intermetallic compounds exerted an influence on mechanical properties, resulting in occurrence of fracture in the part of the base material instead of the jointed parts (heat affected zone and stir zone). This study systematically evaluated the microstructural evolutions during the FSW for joining Al6061 with HT590 and their effect on mechanical properties.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
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• pp.192-192
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• 2011

Hyperthermal ion scattering experiments were conducted with low kinetic energy (<35 eV) cesium ion beams to analyze the UV-photolyzed water-ice films. Neutral molecules (X) on the surface were detected as cesium-molecule ion clusters ($CsX^+$) which were formed through a Reactive Ion Scattering (RIS) process. Ionic species on the surface were desorbed from the surface via a low energy sputtering (LES) process, and were analyzed [1]. Using these methods, the thermal stability of hydronium ion ($H_3O^+$) that was produced by UV light was examined. As the thermal stability of $H_3O^+$ is related with the reaction, $H_3O^+$ + OH + $e^-$ (or $OH^-$) ${\rightarrow}$ $2H_2O$, which is similar or same with the reverse reaction of the auto-ionization of water, the result from this work would be helpful to understand the auto-ionization of $H_2O$ in water-ice that has not been well-understood yet. However, as $H_3O^+$ was not detected through a LES method, the titration experiment of $H_3O^+$ with methylamine ($CH_3NH_2$, MA), MA + $H_3O^+\;{\rightarrow}\;MAH^+$ + $H_2O$, was conducted. In this case, the presence of $MAH^+$ indicates that of $H_3O^+$ in the ice. Thus the pristine ice was photolyzed with UV light for a few minutes and this photolyzed ice was remained at the certain temperature for minutes without UV light. Then MA was adsorbed on that surface so that the population of $H_3O^+$ was found. From the calibration experiments, the relation of $MAH^+$ and $H_3O^+$ was found, so that the thermal stability of $H_3O^+$ can be investigated [2].

• 조명전기설비학회논문지
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• 제22권3호
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• pp.52-58
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• 2008

The importance of. identifying the causes of electrical faults cannot be overstated because of the accidents caused by over-current that take place at the home, the office and electrical facilities due to misuse, poor products and system faults. It is necessary to gather objective, scientific data pertaining to electrical fault investigation in a product liability(PL) environment. To date, no database(DB) has been built concerning the accurate cause analysis of faultyfacilities. In this paper, accident hazard and arc scattering when over-current flows in copper wire was investigated. It was found that when over-current flows in a copper wire, the copper wire became heated and bent and beads were scattered around the wire with a flash. It was determinedthat the fusing current and time was related to the current rise per second. For example, when the current rise per second was largethe fusing current was higher than when the current rise per second was small, and the beads dispersed along a wide area. Fusing time, however, was shorter. The possibility of electrical fault became highest when the fusing current was higher. As the current rise per second is short, the dendrite structure is distributed in the surface of the copper wire. These experimental results can be utilized for a fault process DB system in the investigation and the prevention of electrical faults.

• 한국재료학회지
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• 제11권2호
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• pp.115-119
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• 2001

다발체형성 제조기술을 이용하여 심하게 인발가공된 Cu-Nb 미세복합재료 전선의 전기적 특성과 열처리에 따른 미세조직 변화와의 관계에 대하여 연구하였다. 다발체형성과 인발공정에 의해 제조된 전선에서 Nb필라멘트 단면방향의 형태는 직선이거나 약간 굽은 형태로 나타났다 Nb필라멘트 형태의 차이는 고온에서의 다발체형성 제조공정중의 Nb필라멘트의 파손과 실린더화에 의해 발생하였다. Cu-Nb 미세복합재료의 비저항은 Cu-Nb 계면에서의 전자 산란에 의해 주로 결정된다. $400^{\circ}C$의 어닐링온도 이하에서 전도도의 감소는 침상형태 석출물의 정합변형율과 관계된 산란의 기여가 증가하기 때문이다. 비저항의 비 ($\rho_{295K}$/$\rho_{75K}$)의 약간의 감소는 또한 Nb원자의 석출 때문이다. 50$0^{\circ}C$의 어닐링온도에서 Cu-Nb 미세복합재료의 전도도 중가는 Nb필라멘트의 조대화와 구형화때문이다

• Nuclear Engineering and Technology
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• 제53권2호
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• pp.423-429
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• 2021

The investigation of the utilization of enriched ²⁰⁸Pb as a coolant to enhance the performance of a long-life fast reactor with a Modified CANDLE (Constant Axial shape of Neutron flux, nuclide densities, and power shape During Life of Energy production) burnup scheme has performed. The analyzes were performed on a reactor with thermal power of 800 MegaWatt Thermal (MWTh) with a refueling process every 15 years. Uranium Nitride (enriched ¹⁵N), ²⁰⁸Pb, and High-Cr martensitic steel HT-9 were employed as fuel, coolant, and cladding materials, respectively. One of the Pb-nat isotopes, ²⁰⁸Pb, has the smallest neutron capture cross-section (0.23 mb) among other liquid metal coolants. Furthermore, the neutron-producing cross-section (n, 2n) of ²⁰⁸Pb is larger than sodium (Na). On the other hand, the inelastic scattering energy threshold of ²⁰⁸Pb is the highest among Na, ^natPb, and Bi. The small inelastic scattering cross-section of ²⁰⁸Pb can harden the neutron energy spectrum. Therefore, ²⁰⁸Pb is a better neutron multiplier than any other liquid metal coolant. The excess neutrons cause more production than consumption of ²³⁹Pu. Hence, it can reduce the initial fuel loading of the reactor. The selective photoreaction process was developing to obtain enriched ²⁰⁸Pb. The neutronic was calculated using SRAC and JENDL 4.0 as a nuclear data library. We obtained that the modified CANDLE reactor with enriched ²⁰⁸Pb as coolant and reflector has the highest k-eff among all reactors. Meanwhile, the ^natPb cooled reactor has the lowest k-eff. Thus, the utilization of the enriched ²⁰⁸Pb as the coolant can reduce reactor initial fuel loading. Moreover, the enriched ²⁰⁸Pb-cooled reactor has the smallest power peaking factor among all reactors. Therefore, the enriched ²⁰⁸Pb can enhance the performance of a long-life Modified CANDLE fast reactor.

• 한국시뮬레이션학회논문지
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• 제18권3호
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• pp.113-122
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• 2009

사용자가 요구하는 기능과 특성에 대한 다양한 요구사항은 소프트웨어를 점점 더 복잡하게 만들고 이를 검증하고 검사하는 것은 어려운 문제이다. 게다가 개발된 소프트웨어 코드를 검증하고 검사를 수행하는 과정에서 트레이싱 혹은 로깅 코드를 삽입하는 과정과 검사가 완료되어 삭제하는 과정에서 사용자의 부주의로 버그가 삽일될 수 있는 문제점도 발생한다. 본 논문은 소프트웨어 개발 과정 중에서 검증 및 검사 과정을 지원할 수 있는 Aspect DEVS 검증 틀을 제시한다. Aspect DEVS 검증틀은 관점 지향 프로그래밍 기법을 사용하여 이미 구현되어 있는 소프트웨어와 사용자는 요구사항을 만족하는 지를 확인하는 동시에 소스 코드에 테스팅 코드를 삽입할 때 발생하는 문제들을 해결한다. Aspect DEVS 검증틀을 사용한 검증의 첫 번째 단계는 관찰 대상을 관점 지향 프로그래밍 기법을 사용하여 명세한 하고, 사용자의 요구사항을 DEVS 다이어그램을 명세한 후 이를 DEVSIM++로 구현한다. 마지막으로 프로그램의 수행 과정 중에서 발생하는 이벤트들을 대상으로 구현한 DEVS 모델의 이벤트 입력으로 넣어 소프트웨어가 사용자의 요구사항을 만족하는 지를 검사함으로써 검증 과정 중에 대상 소프트웨어의 수정 없이 검증 및 검사를 수행할 수 있다.

• 한국음향학회지
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• 제27권3호
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• pp.129-139
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• 2008

본 논문의 목적은 탄성판 내에서 진행하는 기본형 램파 모드인 $S_0,\;A_0$ 모드가 사각형 노치에 의해 산란되었을 때, 노치의 2차원 형상에 따른 각 파의 반사계수와 투과계수를 구하는데 있다. 먼저 노치가 있는 부분의 평판의 두께 변화에 따라 노치 부위에 발생 가능한 램파모드의 변화를 고찰하고, 노치 부위의 경계면 형상과 노치 내부에서 진행하는 입사파의 방향에 따라, 노치에 의한 전체 산란 현상을 3가지의 독립된 산란 프로세스로 구분하였다. 그리고 각 프로세스의 경계면에 자유 경계조건과 연속조건을 적용하여 각 프로세스에서 발생된 산란파의 투과 및 반사 계수를 구하였다. 나아가 중첩의 원리를 이용하여 각 프로세스의 산란파를 모드별로 합산하고, 사각형 노치의 폭과 깊이의 변화에 따른 입력파의 에너지 플럭스의 합과 반사 및 투과파의 에너지 플럭스의 합의 차이가 최대 4%에 들도록 하는 정상상태에서의 반사 및 투과계수를 구하고 분석하였다.