• 제목/요약/키워드: Scanning Mobility Particle Sizer

검색결과 67건 처리시간 0.021초

Effects of Temperature and Precursor-concentration on Characteristics of TiO2 Nanoparticles in Chemical Vapor Condensation Process -Part I: Real-time Particle Characterization by SMPS (화학기상응축 공정에서 TiO2 나노입자 특성에 미치는 반응온도와 전구체 농도의 영향 - Part I: SMPS를 이용한 실시간 입자특성 평가)

  • Lee, Chang-Woo;Yu, Ji-Hun;Im, Sung-Soon;Yun, Sung-Hee;Lee, Jai-Sung;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • 제13권5호
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    • pp.323-327
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    • 2003
  • Properties of nanoparticles synthesized during gas phase reaction were studied in terms of particle behaviors using real-time particle characterization method. For this study, $TiO_2$ nanoparticles were synthesized in the chemical vapor condensation process(CVC) and their in-situ measurement of particle formation and particle size distribution was performed by scanning mobility particle sizer(SMPS). As a result, particle behaviors in the CVC reactor were affected by both of number concentration and thermal coagulation, simultaneously. Particularly, growth and agglomeration between nanoparticles followed two different ways of dominances from coagulations by increase of number concentration and sintering effect by increased temperature.

Effects of Particle Measuring Conditions on Diesel Nanoparticles Distribution (입자측정조건이 디젤 나노입자의 입경분포에 미치는 영향)

  • Lee, Jin-Wook;Kim, Hong-Suk;Jeong, Young-Il
    • Journal of Korean Society for Atmospheric Environment
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    • 제22권5호
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    • pp.653-660
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    • 2006
  • Due to the stronger exhaust emission regulations and the introduction of advanced technology in Diesel engine, the specific Diesel particulate matters have decreased by about one order of magnitude since the 1980's. In recent years, particle number emissions rather than particulate mass emissions have become the subject of controversial discussions. Recent results from health studies imply that it is possible that particulate mass does not properly correlated with the variety of health effects attributed to Diesel exhaust. Concern is instead now focusing on nano-sized particles. This study has been performed for the better understanding about the Diesel nano-particle measurement and size distribution characteristics in the exhaust system of a turbo charged Diesel engine. A scanning mobility particle sizer(SMPS) system was applied to measure the particle number and size concentration of Diesel exhaust particles. As the experimental results, the number concentrations in the particle size (Dp<200 nm) were very sensitive to dilution conditions. Specially the changes in nano-particle number concentrations(Dp<50 nm) increased along the downstream of exhaust flow. Also we found the dilution conditions were influencing the condensation of SOF and $H_2O$ during dilution and cooling of hot exhaust.

An Analysis of Characteristics of Particulate Matter Exhausted from Diesel Locomotive Engines (디젤기관차 엔진에서 배출되는 입자의 특성분석)

  • 박덕신;김태오;김동술
    • Journal of Korean Society for Atmospheric Environment
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    • 제19권2호
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    • pp.133-143
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    • 2003
  • Numerous evidence have been reported that fine particulate matters can play an important role in threatening human health. Recently concerns on fine particle pollution from various engines may require re-examination of particulate emission standards. The particles emitted by most diesel engines are mainly divided into their size ranges such as Dp< 50 nm and 50 nm< Dp< 1,000 nm. In this work, the number concentration and the size distribution of fine particles emitted from an exhaust manifold of a railroad diesel engine were measured under load test conditions using a scanning mobility particle sizer (SMPS). The fine particles observed were within the range of 7 to 304 nm under different load conditions with two different dilution ratios. The fine particles exhibited unique patterns showing bimodal shapes in size distribution.

반도체 세정 공정 평가를 위한 나노입자 안착 시스템 개발

  • Nam, Gyeong-Tak;Kim, Ho-Jung;Kim, Yeong-Gil;Kim, Tae-Seong
    • Proceedings of the Korean Society Of Semiconductor Equipment Technology
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    • 한국반도체및디스플레이장비학회 2007년도 춘계학술대회
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    • pp.128-131
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    • 2007
  • As the minimum feature size decrease, control of contamination by nanoparticles is getting more attention in semiconductor process. Cleaning technology which removes nanoparticles is essential to increase yield. A reference wafer on which particles with known size and number are deposited is needed to evaluate the cleaning process. We simulated particle trajectories in the chamber by using FLUENT. Charged monodisperse particles are generated using scanning mobility particle sizer (SMPS) and deposited on the wafer by electrostatic force. The experimental results agreed with the simulation results well. We calculate the particles loss in pipe flow theoretically and compare with the experimental results.

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Formation of Silicon Particles Using $SiH_4$ pyrolysis at atmospheric pressure (상압에서 열분해법을 이용한 실리콘 입자 제조)

  • Woo, Dae-Kwang;Nam, Kyung-Tag;Kim, Young-Gil;Kim, Kwang-Su;Kang, Yun-Ho;Kim, Tae-Sung
    • Proceedings of the KSME Conference
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.126-129
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    • 2007
  • The particle formation using pyrolysis has many advantages over other particle manufacturing techniques. The particles by pyrolysis have relatively uniform size and chemical composition. Also, we can easily produce high purity particles. Thus, we studied the formation of silicon particles by pyrolysis of 50% $SiH_4$ gas diluted in Ar gas. A pyrolysis furnace was used for the thermal decomposition of $SiH_4$ gas at $800^{\circ}C$ and atmospheric pressure. The aerosol flow from furnace is separated into two ways. The one is to the Scanning Mobility Particle Sizer (SMPS) for particle size distribution measurement and the other is to the particle deposition system. The produced silicon particles are deposited on the wafer in the deposition chamber. SEM measurement was used to compare the particle size distribution results from the SMPS. Depending on the experimental conditions, particles of high concentration in the $30\sim80$ nm size range were generated.

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Influence of Aftertreatment System on the Size Distribution of Diesel Exhaust Particulate Matter (후처리 장치에 의한 디젤엔진 배출가스의 미세 입자 입경분포 변화)

  • 권순박;김민철;이규원;류정호;엄명도;김종춘;정일룩
    • Transactions of the Korean Society of Automotive Engineers
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    • 제7권7호
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    • pp.113-121
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    • 1999
  • Diesel particulate matter is known to be one of the major harmful emissions produced by diesel engines. Diesel particulates are subject to diesel emission regulations and have lately become the focus in the diesel emission control technology. Thus, the aftertreatment system is adopted at the diesel engine exhaust to reduce the particulate emission. Although this benefit is recognized, it is not clear how the aftertreatment system influences quantitatively the particle size distribution distribution. In this study, the particle size distributions of diesel exhaust were measured using the scanning mobility particle sizer with and without the aftertreatment system. There results showed that the diesel particulate filter and plasm system reduced the number of emitted particles by more than 90% and about 80% respectivley in the particle size range of 20nm∼600nm. On the other hand no significant effect of the diesel oxidation catalyst on the particle number concentration was detected.

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Estimation of Mass Size Distribution of Atmospheric Aerosols Using Real-Time Aerosol Measuring Instruments (실시간 에어로졸 측정장비를 이용한 대기 중 입자상 물질의 무게 농도 분포의 추정)

  • Ji, Jun-Ho;Bae, Gwi-Nam
    • Particle and aerosol research
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    • 제9권2호
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    • pp.39-50
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    • 2013
  • Real-time aerosol measuring instruments have been widely used for the measurement of atmospheric aerosol, diesel particulate matter, or material synthesis. A scanning mobility particle sizer (SMPS) measures the number size distribution of particles using electrical mobility detection technique. An aerodynamic particle sizer (APS) is used to determine the number concentration and the mean aerodynamic diameter of test particles. An electrical low-pressure impactor (ELPI) is a multi-stage impaction device to separate airborne particles into aerodynamic size classes using particle charging and electrical detection techniques. In this study, the performance of these instruments were evaluated to assess their ability to obtain mass concentrations from particle number concentration measurements made as a function of particle size. The effect of determination of particle density on the measurement of mass concentration was investigated for the three instruments.

Nanoparticles Emission Characteristics of Heavy-Duty CNG Engine with Oxidation Catalyst (산화촉매를 장착한 대형 CNG 엔진의 나노입자 배출특성)

  • Kim, T.J.;Kim, H.N.;Choi, B.C.
    • Journal of Power System Engineering
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    • 제12권5호
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    • pp.27-33
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    • 2008
  • Natural gas has been considered one of the most promising alternative fuels for transportation because of its abundance as well as its ability to reduce regulated pollutants. We measured emission characteristics of nanoparticles from lean burn H/D(Heavy-Duty) CNG (Compressed Natural Gas) engine equipped with oxidation catalysts. The experiments were carried out to measure the emission and engine performance according to the ESC test cycle. The CO and THC conversion efficiencies on the best catalyst in the ESC test cycle achieved about 91 % and 83 %, respectively. From the measurement by the SMPS, the number of nanoparticles emitted from H/D CNG engine is reduced by about 99 % which is more than that of 2.5 L diesel engine. The particle number concentrations of H/D CNG engine were almost nanoparticles. Nanoparticles smaller than 30 nm emitted from the H/D CNG engine and diesel engine equipped with a CDPF(Catalyzed Diesel Particulate Filter) were quite similar. However, the particles bigger than 30nm from the CNG engine were smaller than the particles from diesel engine equipped with a CDPF. The higher the CNG engine load, the lower the particle number from engine-out, but it increased slightly at full load.

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Effects of DME Additives on Combustion Characteristics and Nano-particle Distributions in a Single Cylinder Compression Ignition Engine (DME 연료에 첨가제를 혼합하였을 때의 연소 특성 및 배출가스 특성에 관한 연구)

  • Kwon, Seok-Joo;Cha, June-Pyo;Kang, Min-Gu;Lee, Chang-Sik;Park, Sung-Wook;Lim, Young-Kwan
    • Transactions of the Korean Society of Automotive Engineers
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    • 제20권5호
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    • pp.19-25
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    • 2012
  • This study describes effects of DME additives on combustion and exhaust emissions characteristics including nano-particle in a single cylinder compression ignition engine. Considered additives include bio-diesel, n-butanol, and MTBE for increasing kinematic viscosity. Among three additives, n-butanol showed the greatest kinematic viscosity. In addition MTBE showed the highest vapor pressure. In the present study mixing ratios of additives were kept constant at 1 and 10% by volume. Experiments were performed at 1200rpm engine speed and nano-particles were measured by SMPS (Scanning mobility particle sizer) devices. Results of combustion characteristics showed that considered additives had little effects on combustion pressure. However, patterns of heat release rate were dependent on properties of additives. Nano-particles of MTBE were the lowest among considered additives.

Submicrometer Particle Size Distribution of Emissions from Diesel Engines (디젤엔진에서 배출되는 미세 입자의 크기 분포)

  • 김민철;권순박;이규원;김종춘;류정훈;엄명도
    • Journal of Korean Society for Atmospheric Environment
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    • 제15권5호
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    • pp.657-665
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    • 1999
  • Particulate matter produced by diesel engines is of concern to cngine manufactures because of its environmental impact. The majority of diesel particles are in the range of smaller than 1 ${\mu}{\textrm}{m}$. Because of their tiny volume, ultrafine diesel particles contribute very little to the total mass concentration which is currently regulated for automobile emissions. Ultrafinc particles are known to have deleterious effects upon human health cspecially because they penetrate deeply human respiratory tract and have negative effects on the health. In this study, the engine exhaust gas was diluted in a dilution tunnel and the particle size distribution was measured using the scanning mobility particel sizer system. Measurements of the number and the mass concentrations of the diesel exhaust were made under different engine ooperating conditions. The dilution sampling system provided a common basis for collection of the exhaust by cooling and diluting the source emission prior to the measurement. The measurement results showed that the particle size distributions of the exhaust from the diesel vehicles equipment with either heavy-duty or lignt-duty diesel engines, were similar in the particle size range of 0.08~0.2${\mu}{\textrm}{m}$.

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