• 한국지하수토양환경학회:학술대회논문집
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• 한국지하수토양환경학회 2006년도 총회 및 춘계학술발표회
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• pp.16-19
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• 2006

Humin is the insoluble fraction of humic materials and play an important roles in the irreversible sorption of hydrophobic organic contaminants onto soil particles. However, there have been limited knowledge about the sorption and chemical properties of humin due to the difficulties in its separation from the inorganic matrix(mainly clays and oxides). In this study, do-ashed humin was isolated from a soil sample after removing free lipid and alkali-soluble humic fractions followed by dissolution of mineral matrix with 2% HF, and characterized by elemental analysis, C-13 NMR spectroscopic method. Sorption behavior of 1-naphthol with humin was also investigated from aqueous solution. C-13 NMR spectra indicate that humin molecules are mainly made up of aliphatic carbon including carbohydrate, methylene chain etc.. Sorption intensity for 1-naphthol was increased as organic carbon content of humin increased and log Koc values for the 1-naphthol sorption were determined to be ${\sim}3.12$

• 한국연초학회지
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• 제29권2호
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• pp.132-139
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• 2007

This study was performed to apply the more rapid and accurate sample preparation, and the high selectivity and sensitivity of the analyte detection by gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS). QuEChERS (quick, easy, cheap, effective, rugged and safe) method was validated for 49 agrochemicals in the CORESTA Agrochemical Advisory Committee guide and amenable to GC-MS/MS determination. In QuEChERS method, the effects of sorbents (PSA, $C_{18}$ and GCB) and matrix of the analytes in tobacco types (flue-cured, burley and oriental) were investigated. MS/MS acquisition provided high specificity and selectivity for agrochemicals and low limit of quantification. QuEChERS by using PSA alone and the matrix-matched standards gave good recoveries and RSD values in three types of tobaccos. QuEChERS method was no needed to be complex clean-up procedure and would be used as the fast and easy method for agrochemical residue analysis in tobacco.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1987년도 정기총회 및 창립40주년기념 학술대회 학회본부
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• pp.125-128
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• 1987

This paper deals with the topological observability analysis and the derivation of a reliability evaluation formula of a measurement system for state estimation. An analogy of the DC power flow method to the DC circuit analysis is introduced, and all the relationship between power flows and phase angles are replaced by the corresponding current-voltage relation. As a result, a set of topological measurement equation expressed in the form of the incidence matrix is derived for the topological analysis, and the observability test is carried out by examining the rank of the measurement matrix. The reliability evaluation formula was derived experimentally by testing the observability of sample systems of IEEE-14, IEEE-3.0, IEEE-57.

• Carbon letters
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• 제16권2호
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• pp.86-92
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• 2015

Multi-walled carbon nanotube (MWCNT)/polycarbonate (PC) nanocomposite was prepared by direct melt mixing to investigate the effect of the shear rate on the surface resistivity of the nanocomposites. In this study, an experiment was carried out to observe the shear induced orientation of the MWCNT in the polymer matrix using a very simple melt flow indexer with various loads. The compression-molded, should be eliminated. MWCNT/PC nanocomposite sample exhibited lower percolation thresholds (at 0.8 vol%) and higher electrical conductivity values than those of samples extruded by capillary and injection molding. Shear induced orientation of MWCNT was observed via scanning electron microscopy, in the direction of flow in a PC matrix during the extrusion process. The surface resistivity rose with increasing shear rate, because of the breakdown of the network junctions between MWCNTs. For real applications such as injection molding and the extrusion process, the amount of the MWCNT in the composite should be carefully selected to adjust the electrical conductivity.

• 대한조선학회지
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• 제10권1호
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• pp.21-26
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• 1973

A simple matrix method to analyze the ship's transverse frame ring is proposed. In this approach, the frame ring is treated as a plane frame of uniform slender members. The loadings on the frame consist of buoyancy loads, deck loads and cargo loads. The hatch coaming are considered to deflect under the loads. Because of symmetry, only the half of the frame is analyzed. The method is to obtain the forces and moments on each member. The deformation of the frame can be determined from the nodal displacements. For a sample calculation, a frame ring of a 10,000 ton class cargo liner is analyzed on the IBM 1130 computer. The numerical results obtained are proved to be resonable.

• Bulletin of the Korean Chemical Society
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• 제24권9호
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• pp.1308-1312
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• 2003

Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) was used to observe folic acid and its derivatives such as tetrahydrofolate and 5-methyltetrahydrofolate in a vitamin tablet and in foods. Folic acid in a vitamin tablet was determined using angiotensin I as an internal reference. Tetrahydrofolic acid, 5-methyltetrahydrofolic acid, and an oxygenated folate were observed from a human blood sample using graphite plate. The results show that these mass spectrometric methods are useful for quickly obtaining a profile of folates.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2014년도 추계 학술논문 발표대회
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• pp.171-172
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• 2014

This is an experimental study on manufacturing of non-cement matrix. Materials like cement and blowing agent in foamed concrete is replaced by by-products from blast furnace slag and paper ash. Sample 43-PS-1 with density showed lowest. The compressive strength test result, showed a similar trend with density. And it showed that compressive strength of the 40-PS-1 was highest.

• 한국방송∙미디어공학회:학술대회논문집
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• 한국방송공학회 2015년도 추계학술대회
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• pp.54-55
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• 2015

In this paper, we propose a method pursuing robustness in ad hoc network system when the CSI of interferers is unavailable. The non-parametric linear minimum mean square error filter is exploited to achieve large fraction of the MMSE filter transmission capacity employing the perfect covariance matrix information. From the numerical results, we show that the proposed scheme brings substantial transmission capacity gain over conventional MMSE filter using sample covariance matrix.

• 한국반도체및디스플레이장비학회:학술대회논문집
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• 한국반도체및디스플레이장비학회 2003년도 추계학술대회 발표 논문집
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• pp.12-17
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• 2003

We develop Mueller-matrix spectroscopic ellipsometry based on dual compensator configuration. This technique is very powerful for measuring surface anisotropy in nano-scale, especially when materials show depolarization. Dual-rotating compensator configuration is adopted with the rotational ratio of 5:3 originally developed by Collins et al [1]. The instrument can provide 250-point spectra over the wavelength range from 230 nm to 820 nm in one irradiance waveform with minimum acquisition time of $Tc{\approx}10 s$. In this work, the results obtained in transmission modes are presented for the initial attempt. We present calibration procedures to diagnose the system from the utilize data collected in transmission mode without sample. We expect that the instrument will have important applications in thin films and surfaces that have anisotropy and inhomogeneity.

• Bulletin of the Korean Chemical Society
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• 제14권6호
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• pp.696-700
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• 1993

Gold bonding wire of 0.076 mm in diameter used in semiconductor industry, is dissoved in aqua regia. The solution is then evaporated to near dryness several times with a few drops of HCl added to prepare the final sample solution in 5% HCl. The gold matrix is separated from trace impurities by controlled potential deposition. The whole electrolysis has been carried out inside a clean bench. An optimum potential is found to be +0.25 V to give more than 99.9% Au matrix removal with better than 90 analytes remaining in the electrolyte solution. Isotope dilution calibration is employed to get the best accuracy and precision. Analytical results are presented with determination limits of the analytical method.