• Journal of Periodontal and Implant Science
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• 제42권2호
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• pp.59-63
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• 2012

Purpose: This study evaluated the surface characteristics and bond strength produced using a novel technique for coating hydroxyapatite (HA) onto titanium implants. Methods: HA was coated on the titanium implant surface using a super-high-speed (SHS) blasting method with highly purified HA. The coating was performed at a low temperature, unlike conventional HA coating methods. Coating thickness was measured. The novel HA-coated disc was fabricated. X-ray diffraction analysis was performed directly on the disc to evaluate crystallinity. Four novel HA-coated discs and four resorbable blast medium (RBM) discs were prepared. Their surface roughnesses and areas were measured. Five puretitanium, RBM-treated, and novel HA-coated discs were prepared. Contact angle was measured. Two-way analysis of variance and the post-hoc Scheffe's test were used to analyze differences between the groups, with those with a probability of P<0.05 considered to be statistically significant. To evaluate exfoliation of the coating layer, 7 sites on the mandibles from 7 mongrel dogs were used. Other sites were used for another research project. In total, seven novel HA-coated implants were placed 2 months after extraction of premolars according to the manufacturer's instructions. The dogs were sacrificed 8 weeks after implant surgery. Implants were removed using a ratchet driver. The surface of the retrieved implants was evaluated microscopically. Results: A uniform HA coating layer was formed on the titanium implants with no deformation of the RBM titanium surface microtexture when an SHS blasting method was used. Conclusions: These HA-coated implants exhibited increased roughness, crystallinity, and wettability when compared with RBM implants.

• Applied Microscopy
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• 제26권3호
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• pp.379-388
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• 1996

Structure of premartensite in $Ti_{50}Ni_{49}Fe_1\;and\;Ti_{50}Ni_{50}$ prepared by self-propagating high temperature synthesis (SHS) method has been investigated by a detailed transmission electron microscopy. $Ti_{50}Ni_{49}Fe_1$ consists of microdomain area and needle type domain area. On the other hand, $Ti_{50}Ni_{50}$ consists of microdomain-free and microdomain area, and needle type domain area. Various types of extra superreflections, such as 1/2<100>, 1/2<110> and 1/4<210> type superreflection have been observed in the selected area electron diffractions from microdomain area. Such extra superreflections are due to transformation from B2 structure to distorted B2 structure or premartensite. The present study shows that incommensurate phase forms as an intermediate phase during martensitic transformation. Particularly, in Fe-free $Ti_{50}Ni_{50}$, two types of matrix phases have been observed, microdomain and microdomain-free area. Types of extra superreflections in $Ti_{50}Ni_{50}$ are different from those in $Ti_{50}Ni_{49}Fe_1$, i.e. 1/7<321> type superreflections have been observed, instead of 1/2<110>, 1/2<100>, 1/4<210> types in $Ti_{50}Ni_{49}Fe_1$.

• 한국세라믹학회지
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• 제34권5호
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• pp.473-482
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• 1997

Titanium carbide(TiC) has a poor sinterability due to the strong covalent bond. Thus, it is generally fabricated by either hot pressing or pressureless-sintering at elevated temperature by the addition of sintering aids such as nickel(Ni), molybdenum(Mo) and cobalt(Co). However, these sintering methods have the following disadvantages; (1) the complicated process, (2) the high energy consumption, and (3) the possibility of leaving inevitable impurities in the product, etc. In order to reduce above disadvantages, we investigated the optimum conditions under which dense titanium carbide bodies could be synthesized and sintered simultaneously by high pressure self-combustion sintering(HPCS) method. This method makes good use of the explosive high energy from spontaneous exothermic reaction between titanium and carbon. The optimum conditions for the nearly full-densification were as follows; (1) The densification of sintered body becomes high by increasing the pressing pressure from 400kgf/$\textrm{cm}^2$ upto 1200 kgf/$\textrm{cm}^2$. (2) Instead of adding the coarse graphite or activated carbon, the fine particles of carbon black should be added as a carbon source. (3) The optimum molar ratio of carbon to titanium (C/Ti) was unity. In reality, titanium carbide body which were prepared under optimum conditions had relatively dense textures with the apparent porosity of 0.5% and the relative density of 98%.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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• pp.276-279
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• 2002

$Bi_{2}Sr_{2}CaCu_{2}O_{x}$ was prepared by the conventional method of solid state reaction and SHS method. The samples were annealed in different atmosphere in order to examine the influence of atmospheres on the carbon contents in the $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ compound. The lowest carbon content in $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ could be attended when the sample was annealed in $O_{2}$ at $800^{\circ}C$ for 100 hours. The $CO_{2}$ in air pollute the samples and increase the carbon content in the sintering process. The critical current density of the $Bi_{2}Sr_{2}CaCu_{2}O_{x}$ samples will decrease with the increasing carbon contents in the samples. The impurity carbon will deposit in the grain boundary, which makes critical current density lower.

• 제어로봇시스템학회논문지
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• 제6권9호
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• pp.831-835
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• 2000

The uniformity of themperature on a wafer is a wafer is one the most important parameters to conterol the RTF(Rapid Thermal Process) with proper input signals. It is impossible to achieve the uniformity of temperature without the exact estimation of temperature ar all points on the wafer. There fore, it is difficult to understand the internal dynamics as well as the structural complexities of the RTP, which is aprimary obstacle to measure the distributed temperatures on the wafer accurately. Furthermore, it is also hard to accomplish desirable estimation because only a few pyrometers are available in the general equipments. In the paper, a thermal model based on the chamber grometry of the AST SHS200 RTP system is developed to effectively control the thermal uniformity on the wafer. First of all, the estimation method of one-point measurement is developed, which is properly extended to the case of multi-point measurements. This thermal model is validated through simulation and experiments. The proposed work can be utilized to building a run-by -run or a real-time control of the RTP.

• 자원리싸이클링
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• 제6권4호
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• pp.31-37
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• 1997

본 논문은 SHS(Self propagating High-temperature Synthesis)법을 이용하여 $WO_3$/Mg 계로부터 W을 제련시 산침출로 인하여 발생하는 Mg 폐액으로부터 Mg-ferrite분말을 회수하는 방법에 대한 것으로, 습식법 주에서 단분산성 구형 초미립자들을 하소 공정없이 직접제조가능하다는 장점을 가진 수열합성법을 이용하여 Mg-ferrite분말을 회수하는 것을 중심 내용으로 하고 있다. 산침출 Mg 폐액으로부터 수열법에 의한 Mg-Ferrite 분말 회수시 폐용액의 pH와 pHwhwjf제는 분말의 특서에 크게 영향을 주었다. 분말회수의 최적조건은 ${Fe}^{2+}$ : ${Mg}^{2+}$몰비가 2:1, 반응온도가$ 200^{\circ}C$, 반응시간이 1시간, pH=12, 산소분압이 2000psi였고, 이때 제조된 분말은 단분산성, 균일한 입도분포를 가진 구형입자이었다.

• 대한전기학회논문지:시스템및제어부문D
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• 제49권2호
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• pp.62-67
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• 2000

The uniformity of temperature on a wafer is one of the most important parameters to control the RTP (Rapid Thermal Process) with proper input signals. Since it is impossible to achieve the uniformity of temperature without exact estimation of temperature at all points on the wafer, the difficulty of understanding internal dynamics and structural complexities of the RTP is a primary obstacle to accurately measure the distributed temperatures on the wafer. Furthermore, it is also hard to accomplish desirable estimation because only few pyrometers have been commonly available in the general equipments. In the paper, a thermal model based on the chamber geometry of the AST SHS200 RTP system is developed to effectively control the thermal uniformity on the wafer. First of all, the estimation method of one-point measurement is developed, which is properly extended to the case of multi-point measurements. This thermal model is validated through certain simulation and experiments. The work can be usefully contributed to building a run-by-run or a real-time controls of the RTP.

• Steel and Composite Structures
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• 제46권3호
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• pp.353-366
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• 2023

This paper presents a finite-element analysis (FEA) of aluminum alloy rectangular hollow sections (RHSs) and square hollow sections (SHSs) with circular through-openings under three-point and four-point bending. First, a finite-element model (FEM) was developed and validated against the corresponding test results available in the literature. Next, using the validated FE models, a parametric study comprising 180 FE models was conducted. The cross-section width-to-thickness ratio (b/t) ranged from 2 to 5, the hole size ratio (d/h) ranged from 0.2 to 0.8 and the quantity of holes (n) ranged from 2 to 6, respectively. Third, results obtained from laboratory test and FEA were compared with current design strengths calculated in accordance with the North American Specifications (NAS), the modified direct strength method (DSM) and the modified Continuous strength method (CSM). The comparison shows that the modified CSM are conservative by 15% on average for aluminum alloy RHSs and SHSs with circular through-openings subject to bending. Finally, a new design equation is proposed based on the modified CSM after being validated with results obtained from laboratory test and FEA. The proposed design equation can provide accurate predictions of flexural capacities for aluminum alloy RHSs and SHSs with circular through-openings.

• 한국과학교육학회지
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• 제28권4호
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• pp.282-290
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• 2008

R&E 프로그램은 한국과학영재학교와 과학 고등학교의 과학영재들을 위한 사사교육 프로그램으로, 1년 동안 현직 과학자와 과학교사가 멘토로 참여하며 학생들이 실제 연구 과제를 수행하는 프로그램이다. 이 연구에서는 R&E 프로그램의 주요 목적인 연구 중심의 자기 주도적 학습, 과학적 탐구능력과 창의적인 문제해결능력의 신장, 과학자의 생활과 자세에 대한 인식과 희망 전공 등의 항목에 대해서 R&E 프로그램을 경험한 한국과학기술원 학부과정 신입생 182명을 대상으로 사사교육 프로그램의 효과에 대해서 스스로 어떻게 평가하고 있는지, 설문조사를 통하여 이들의 인식을 조사하였다. 그 결과는 첫째, 프로그램 참여를 통하여 동료들과의 협력(81.0%), 전문 과학지식의 습득(80.8%), 과학자의 생활과 자세에 대한 이해(77.5%), 과학에 대한 흥미(68.7%), 과학적 탐구방법(62.7%), 창의적 사고력(61.5%) 등의 순으로 향상되었다고 긍정으로 인식하였다. 둘째, KAIST 신입생들 사이에 출신 고등학교에 따라서 통계적으로 유의미한 차이가 나타났으며, 과학적 탐구방법 향상(p<.01), 연구과제에 관한 전문적인 과학지식 향상(p<.01)의 항목이었다. 이러한 결과는, 과학자로서의 품성 및 자질 함양, 과학적 탐구능력과 창의적 사고력 향상이라고 하는 과학영재를 위한 사사교육으로서 R&E 프로그램의 목적이 충분히 달성되고 있을 가능성을 보여준다.

• 한국항해항만학회:학술대회논문집
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• 한국항해항만학회 2016년도 춘계학술대회
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• pp.199-201
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• 2016

항해장비의 성능이 고도화되고 있으나 해기사의 항해기기 운용능력, 즉 해양사고 저감을 위한 항해사의 위험 예견 능력과 회피의무의 중요성은 지속적으로 증대되고 있다. 이 능력과 의무는 항해사의 인지능력으로도 표현할 수 있다. 해기능력이 상이한 각 선교팀이 선박 조종시뮬레이터로 인명구조조선을 실시하여 나타난 선박의 항적을 기반으로 인지상황 발생 초기대응별 사례를 분석하고, 단계별 항적, ROT 값 등 분석 자료를 인지교육모델, 해기사의 상황인식평가 기초자료로 활용하고자 한다.