• Title/Summary/Keyword: SEM analysis

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Log-based petrophysical analysis of Khatatba Formation in Shoushan Basin, North Western Desert, Egypt

  • Osli, Liyana Nadiah;Yakub, Nur Yusrina;Shalaby, Mohamed Ragab;Islam, Md. Aminul
    • Geosciences Journal
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    • v.22 no.6
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    • pp.1015-1026
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    • 2018
  • This paper aims to investigate the good reservoir quality and hydrocarbon potentiality of the Khatatba Formation, Qasr Field in the Shoushan Basin of the North Western Desert, Egypt by combining results from log-based petrophysical analysis, petrographic description and images from scanning electron microscope (SEM). Promising reservoir units are initially identified and evaluated through well log analysis of three wells in the field of study. Petrophysical results are then compared with petrographic and SEM images from rock samples to identify features that characterize the reservoir quality. Well log results show that Khatatba Formation in the study area has good sandstone reservoir intervals from depths ranging from 12848 ft to 13900 ft, with good effective porosity records of 13-15% and hydrocarbon saturations of greater than 83%. Petrographic analysis of these sandstone reservoir units indicate high concentrations of vacant pore spaces with good permeability that can be easily occupied by hydrocarbon. The availability of these pore spaces are attributed to pore-enhancing diagenetic features, mainly in the form of good primary porosity and dissolution. SEM images and EDX analysis confirmed the presence of hydrocarbon, therefore indicating a good hydrocarbon-storing potential for the Khatatba Formation sandstones.

A Meta Analysis of Using Structural Equation Model on the Korean MIS Research (국내 MIS 연구에서 구조방정식모형 활용에 관한 메타분석)

  • Kim, Jong-Ki;Jeon, Jin-Hwan
    • Asia pacific journal of information systems
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    • v.19 no.4
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    • pp.47-75
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    • 2009
  • Recently, researches on Management Information Systems (MIS) have laid out theoretical foundation and academic paradigms by introducing diverse theories, themes, and methodologies. Especially, academic paradigms of MIS encourage a user-friendly approach by developing the technologies from the users' perspectives, which reflects the existence of strong causal relationships between information systems and user's behavior. As in other areas in social science the use of structural equation modeling (SEM) has rapidly increased in recent years especially in the MIS area. The SEM technique is important because it provides powerful ways to address key IS research problems. It also has a unique ability to simultaneously examine a series of casual relationships while analyzing multiple independent and dependent variables all at the same time. In spite of providing many benefits to the MIS researchers, there are some potential pitfalls with the analytical technique. The research objective of this study is to provide some guidelines for an appropriate use of SEM based on the assessment of current practice of using SEM in the MIS research. This study focuses on several statistical issues related to the use of SEM in the MIS research. Selected articles are assessed in three parts through the meta analysis. The first part is related to the initial specification of theoretical model of interest. The second is about data screening prior to model estimation and testing. And the last part concerns estimation and testing of theoretical models based on empirical data. This study reviewed the use of SEM in 164 empirical research articles published in four major MIS journals in Korea (APJIS, ISR, JIS and JITAM) from 1991 to 2007. APJIS, ISR, JIS and JITAM accounted for 73, 17, 58, and 16 of the total number of applications, respectively. The number of published applications has been increased over time. LISREL was the most frequently used SEM software among MIS researchers (97 studies (59.15%)), followed by AMOS (45 studies (27.44%)). In the first part, regarding issues related to the initial specification of theoretical model of interest, all of the studies have used cross-sectional data. The studies that use cross-sectional data may be able to better explain their structural model as a set of relationships. Most of SEM studies, meanwhile, have employed. confirmatory-type analysis (146 articles (89%)). For the model specification issue about model formulation, 159 (96.9%) of the studies were the full structural equation model. For only 5 researches, SEM was used for the measurement model with a set of observed variables. The average sample size for all models was 365.41, with some models retaining a sample as small as 50 and as large as 500. The second part of the issue is related to data screening prior to model estimation and testing. Data screening is important for researchers particularly in defining how they deal with missing values. Overall, discussion of data screening was reported in 118 (71.95%) of the studies while there was no study discussing evidence of multivariate normality for the models. On the third part, issues related to the estimation and testing of theoretical models on empirical data, assessing model fit is one of most important issues because it provides adequate statistical power for research models. There were multiple fit indices used in the SEM applications. The test was reported in the most of studies (146 (89%)), whereas normed-test was reported less frequently (65 studies (39.64%)). It is important that normed- of 3 or lower is required for adequate model fit. The most popular model fit indices were GFI (109 (66.46%)), AGFI (84 (51.22%)), NFI (44 (47.56%)), RMR (42 (25.61%)), CFI (59 (35.98%)), RMSEA (62 (37.80)), and NNFI (48 (29.27%)). Regarding the test of construct validity, convergent validity has been examined in 109 studies (66.46%) and discriminant validity in 98 (59.76%). 81 studies (49.39%) have reported the average variance extracted (AVE). However, there was little discussion of direct (47 (28.66%)), indirect, and total effect in the SEM models. Based on these findings, we suggest general guidelines for the use of SEM and propose some recommendations on concerning issues of latent variables models, raw data, sample size, data screening, reporting parameter estimated, model fit statistics, multivariate normality, confirmatory factor analysis, reliabilities and the decomposition of effects.

Characterization of crystal phase evolution in cordierite honeycomb for diesel particulate filter by using rietveld refinement and SEM-EDS methods (Rietveld 정밀화법과 SEM-EDS 분석에 의한 DPF용 코디어라이트 하니컴 세라믹스의 결정성장 과정 분석)

  • Chae, Ki-Woong;Kim, Kang San;Kim, Jeong Seog;Kim, Shin-Han
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.31 no.3
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    • pp.116-126
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    • 2021
  • Diesel particulate filter (DPF) is a typical application field of cordierite (Mg2Al4Si5O18) honeycomb. Green body for DPF honeycomb was extruded using slurry paste and sintered at the temperature range of 980~1450℃. Quantitative crystal phase analysis was carried out by using Rietveld refinement method for powder XRD data. In conjunction with the quantitative Rietveld analysis, SEM-EDS analysis was carried for the crystal phases (indialite, cordierite, cristobalite, alumina, spinel, mullite, pro-enstatite). After removing amorphous phase on the sintered surfaces by chemical etching method, the shape and composition of the crystal phases can be clearly identified by SEM-EDS method. By combining the Rietveld refinement method and SEM-EDS analysis, crystal phase evolution process in DPF cordierite ceramics could be clarified. In addition, the coefficient of thermal expansion (CTE) of the DPF honeycombs were measured and compared with the calculated CTEs based on the quantitative crystal phase analysis results.

A Study on Frequency Dependence on Dielectric Properties of Silicone Rubber Sheets (실리콘 고무 시트의 유전특성에 미치는 주파수 의존성에 관한 연구)

  • Lee, Sung Ill
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.33 no.5
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    • pp.405-410
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    • 2020
  • In this study, the following results were obtained by analysis of electric properties with FT-IR, DSC, XRD, and SEM, in the range of temperature 30~160℃ and frequency 0.1~200 kHz, when filling agent (0~100 phr) and silicone oil (0~12 phr) were added to raw silicone rubber. In the case of 100 phr mixed samples, the relative dielectric constant εr gradually decreased from 4.3 to 3.96 as frequency increased, and the dielectric loss tan δ decreased to 0.01 at 300 Hz, then increased to 0.022 at 30 kHz, then decreased to 200 kHz. The FT-IR analysis identified the same binding structure according to the chemical composition of added silica (SiO2). Through DSC analysis, we could determine the change of heat quantity and the glass transition temperature of each specimen. In the XRD analysis, it was found that the images SiO2, TiO2, and Fe2O3 appeared for specimens with 0%, 50% and 100% filling agent. Finally, the SEM analysis confirmed that particles of 0.5 to 1.5 ㎛ size with silica (SiO2) mixing were dispersed evenly.

Archeological Chemical analysis and Characteristic Investigation on Glass Beads Excavated in Sacheon Neukdo Island, Gyeongsangnam-do (경남 사천 늑도 유적 출토 유리구슬의 고고화학적 특성 고찰)

  • Kwon, Yoon-Mi;Kim, Gyu-Ho;Shin, Yong-Min
    • Journal of Conservation Science
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    • v.20
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    • pp.105-117
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    • 2007
  • This study is examined the beads excavated in the Sacheon Neukdo ruins to investigate the features of archaeological chemistry and to compare those of the same type of beads excavated within the Gyeongsang-do area by means of scientific analysis. The samples have been observed the micro-structures by an optical microscope and SEM and confirmed the physical property by density measurement. Chemical property have been analyzed main components such as flux, stabilizers, and colorants by SEM-EDS. Besides, XRD was used to identified the characteristic materials of beads. The white opaque beads, which was initially estimated as sea-shell beads, confirm as amorphous silica material. The glass beads, which are blue type as a result of compositional analysis, it is revealed potash glass group and LCA(Low-CaO, $Al_2O_3$) system. gB ones are revealed only in LCA-A(LCA-CaO<$Al_2O_3$), while purple blue ones in LCA-B(LCA-CaO>$Al_2O_3$).

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Busan Housing Market Dynamics Analysis with ESDA using MATLAB Application (공간적탐색기법을 이용한 부산 주택시장 다이나믹스 분석)

  • Chung, Kyoun-Sup
    • The Journal of the Korea Contents Association
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    • v.12 no.2
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    • pp.461-471
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    • 2012
  • The purpose of this paper is to visualize the housing market dynamics with ESDA (Exploratory Spatial Data Analysis) using MATLAB toolbox, in terms of the modeling housing market dynamics in the Busan Metropolitan City. The data are used the real housing price transaction records in Busan from the first quarter of 2006 to the second quarter of 2009. Hedonic house price model, which is not reflecting spatial autocorrelation, has been a powerful tool in understanding housing market dynamics in urban housing economics. This study considers spatial autocorrelation in order to improve the traditional hedonic model which is based on OLS(Ordinary Least Squares) method. The study is, also, investigated the comparison in terms of $R^2$, Sigma Square(${\sigma}^2$), Likelihood(LR) among spatial econometrics models such as SAR(Spatial Autoregressive Models), SEM(Spatial Errors Models), and SAC(General Spatial Models). The major finding of the study is that the SAR, SEM, SAC are far better than the traditional OLS model, considering the various indicators. In addition, the SEM and the SAC are superior to the SAR.

Performance Evaluation of High Strength Concrete with Composite Fibers in Accordance with High Temperature (복합섬유가 혼입된 고강도 콘크리트의 고온가열에 따른 성능 평가)

  • Kim, Seung-Ki;Kim, Woo-Suk
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.19 no.6
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    • pp.63-71
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    • 2015
  • The objective of the present study is to investigate how elevated temperature ranging from $100^{\circ}C$ to $800^{\circ}C$ as well as room temperature affects the variation of mechanical properties of high strength concrete ($over\;f_{ck}=60MPa\;grade$). In this experiment, specimens were exposed for a period of $2^{\circ}C/min$ to temperatures of $20^{\circ}C$, $100^{\circ}C$, $200^{\circ}C$, $300^{\circ}C$ $400^{\circ}C$, $500^{\circ}C$, $600^{\circ}C$, $700^{\circ}C$ and $800^{\circ}C$, respectively. Accordingly, the study investigated the fire resistance performance of high strength concrete mixed with composite fibers which composed with hybrid fibers and steel fibers. After cooling down to ambient temperature, the following basic mechanical properties were then evaluated and compared with reference values obtained prior to thermal exposure: (i) compressive strength in room temperature; (ii) residual compressive strength; (iii) Poisson's ratio; (iv) weight change; (v) SEM analysis & XRD analysis In addition, XRD and SEM Images analyses were performed to investigate chemical and physical characteristics of high strength concrete with composite fibers according to high temperature.

The Effects of Job-Seeking Stress, Appearance Recognition, Financial Distress, Trust in Government, and Locus of Control on University Students' Happiness (취업스트레스, 외모인식, 재무스트레스, 정부신뢰도, 내외통제성이 대학생의 행복에 미치는 영향)

  • Kim, Min-Koo;Lee, Gyoung-Gun;Lee, Suk-Yong;Chun, Jun-Ha;Han, Yong-Hee
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.40 no.4
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    • pp.171-182
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    • 2017
  • Most people seek a happy life and happiness positively affects sentiment, satisfaction with life, creativity, human relationship, business productivity, and even health and life extension. However, according to a survey in 2013, subjective happiness of adolescents (including university students) was very low compared to other age groups in Korea. Therefore this paper examined the effects of job-seeking stress, appearance recognition, financial situation, trust in government, and locus of control on university students' happiness using SEM (structural equation modeling). 207 university students in Seoul, Korea have been surveyed. At first, an initial experimental SEM model among these variables has been set up and reliability analysis has been conducted. Then multiple regression analyses on job-seeking stress and happiness as well as SEM analysis have been conducted. As a result of these analyses, the SEM model has been revised two times. The final SEM model passed the goodness-of-fit test (using RMR, GFI, NFI, CFI, and IFI indices). The final SEM model showed the followings. First, Higher job-seeking stress (especially sentimental part, rather than environment or action related parts) negatively affects happiness. Second, Trust in government also affects happiness both directly and indirectly. Third, Locus of control is affected both by trust in government and financial situation. Fourth, appearance recognition heavily affects job-seeking stress. In addition, appearance importance is higher than appearance interest, meaning that students who are not very interested in appearance usually recognize the importance of appearance. Finally, happiness is affected neither financial situation nor appearance recognition. Therefore, even either they are in a poor financial situation or not happy with their appearance, they can be happy if they have firm locus of control.

Construction and Refinement of Conceptual Site Model Based on Scrutiny of Oil Contaminated Site (유류오염부지 정밀조사에 기반한 부지개념모델 구축 및 개선)

  • Min Seo Bae;Mingyeong Kim;Juhee Kim;Soonjae Lee;Man Jae Kwon;Ho Young Jo
    • Journal of Soil and Groundwater Environment
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    • v.28 no.2
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    • pp.12-29
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    • 2023
  • Conceptual site model (CSM) development and enhancement for contaminated sites assists in identifying data gaps during the site investigation process. In this study, CSM was developed and enhanced for a contaminated site in Korea as a case study. Site Y was scrutinized four times previously. The site profiles for each scrutiny were reorganized based on the scrutiny reports, and the relevant data was utilized to develop and enhance CSMs. CSM for the first investigation was developed in various forms including table, flowchart, diagram, and narrative formats. CSM was enhanced in a stepwise manner by incorporating the updated profile information obtained in next investigation to existing CSM. The hypothetical data gap analysis between each investigation step was established to meet the purpose of the follow-up investigation. This case study showed that CSM is a useful tool to identify the history and current status of contaminated sites and thereby help in planning supplementary investigations for better site characterization.