• Title/Summary/Keyword: Reference Materials

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The Study of Fast X-ray Fluorescence Analysis Using a SSQ Program (SSQ 프로그램을 이용한 빠른 X-선형광분석법 고찰)

  • Park, Yong Joon
    • Analytical Science and Technology
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    • v.11 no.2
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    • pp.112-119
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    • 1998
  • A Siemens SemiQuant (SSQ) 3000 program, a precalibrated 'standardless' analytical program handling up to 90 elements, was evaluated for the fast analysis of various types of reference materials using a wavelength dispersive X-ray spectrometer. Various types of standard reference materials such as metal discs, metal chips, and geological materials in powder form were analysed and it took 23 minutes of measuring time for 75 elements. Measurements of geological reference materials using different sampling methods were carried out and their data were interactively evaluated. The analysis of materials of a known matrix concentration such as stainless steels provided higher precision value compared to totally unknown samples. The analyses of materials prepared as pressed pellets or fused glass beads provided higher precision values compared to the measurement of loose powders with a foil on the sample surface and helium operation, though their sampling procedures were more complicate and took more time. Since very light elements such as boron, carbon, and oxygen have a strong influence on the matrix effects and also on the calculation of effective matrix corrections, the rhodium Compton check was applied to verify the reliability of the defined light element concentrations of light matrix materials and the defined major sample compounds. Failure of defining correct matrix resulted in an unoptimized matrix correction and therefore in the wrong calculation of the element concentration.

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A Study on the Citing Behavior of Military Scientists by Reference Analysis (참고문헌 분석을 통한 국방과학 연구자들의 인용행태 연구)

  • Kim, Mi-Ra;Lee, Eung-Bong
    • Journal of the Korean Society for Library and Information Science
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    • v.47 no.2
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    • pp.143-159
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    • 2013
  • A series of citation analyses are conducted to find out the characteristics of citation behavior in the field of military science and technology in Korea. The analyses are done against the references at the ends of articles in the Journal of the Korea Institute of Military Science and Technology published during the period 1998-2012. The sample includes 4,563 references from 537 articles. The analyses focused on types of materials, such as monographs, continuous materials, reports, etc., cited by the researchers by year. Lastly, the study aims to suggest the preferences of cited materials. The results of the analyses might provide a guide for a research library to establish an effective acquisition policy and a basis for tangible proof to secure continuous financial support from administration.

A Study of Service Improvement for Electronic Information Room by User's Experience (도서관의 전자정보실 서비스 개선을 위한 이용사례 분석)

  • Lee, Kyung-Min
    • Journal of Korean Library and Information Science Society
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    • v.40 no.4
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    • pp.177-198
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    • 2009
  • The domestic libraries offered users computer environment early to adapt in information age. However, the computer environment is generalized today, so it is needed to change about the role of electronic information room in this point. The author investigated use experience by 78 students who are student in library and information science. They experienced electronic information room and wrote their experience. As a result, they felt most inconvenience in information service of librarians, facilities and equipment and space. To improve the service of electronic information room, it is needed to develop the mission and service policy of electronic information room. And also the librarian must think the room as modern reference room that has digital and analog materials and information technology.

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Open-Ended Coaxial Probe with Protruding Inner Conductor (내심이 돌출된 개방단말 동축선 프로브)

  • Jung Ji-Hyun;Jo Yu-Sun;Kim Se-Yun
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.16 no.1 s.92
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    • pp.26-32
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    • 2005
  • Open-ended coaxial probe is used to measure complex permittivities of materials in a wide bandwidth. Complex permittivity measured by a conventional coaxial probe suffers from severe fluctuation due to instrumental uncertainty when the difference between reflection coeffcients of reference and measuring materials is small. In this paper, open-ended coaxial probe with protruding inner conductor is suggested to increase the difference between reflection coefficients of reference and measuring materials. Its validity is assured by FDTD simulation and actual measurement.

Angle Sensors Based on Oblique Giant Magneto Impedance Devices

  • Kim, Do-Hun;Na, Ji-Won;Jeung, Won-Young
    • Journal of Magnetics
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    • v.14 no.1
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    • pp.42-46
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    • 2009
  • The measurement of external magnetic field orientation using Giant Magneto Impedance (GMI) sensors has been performed. A soft magnetic alloy of $Co_{30}Fe_{34}Ni_{36}$ was electroplated on a Si wafer with a CoFeNi seed layer. V-shaped microwire patterns were formed using a conventional photolithography process. An external magnetic field was generated by a rectangular AlNiCo permanent magnet. The reference direction was defined as the external magnetic field direction oriented in the middle of 2 GMI devices. As the orientation of the magnetic field deviated from the reference direction, variation in the field component along each device introduced voltage changes. It was found that, by taking the voltage difference between the left and right arms of the Vshaped device, the nonlinearity of each device could be significantly reduced. The fabricated angle sensor had a linear range of approximately $70^{\circ}$ and an overall sensitivity of approximately 10 mV.

Evaluation of the proficiency testing results using river water-based reference materials for heavy metal analysis (중금속분석용 하천수 매질표준물질을 이용한 숙련도 결과 평가)

  • Song, Ko-Bong;Kim, Young-Hee;Shin, Sun-Kyoung;Lee, Su-Yeong;Kim, Hyun-Jung;Kang, Hak-Gu;Kim, Il-Gyu;An, Hee-Ju
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.284-294
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    • 2010
  • In this study, river water-based reference materials (RMs), NIER-I08RW and NIER-I09, for trace metal analysis were prepared and certified for Pb, Cd, Cr and Cu with evaluation of uncertainties. The RMs were confirmed to be homogeneous enough to be used as proficiency testing materials since within-bottle homogenieties of the RMs were lower than 0.3 times of targeted standard deviation of proficiency testing. The RMs were distributed to environmental testing laboratories for the proficiency testing and the variation of Z scores of the proficiency testing results were compared for different assigned values. The relative bias, $B_{relative}$, deviations between reference values and consensus values, were lower than ${\pm}$1 except for cadmium of NIERI08RW. The results showed both values were in a good agreement and only 2.9% of Z scores changed by using a different assigned values such as consensus and reference values.

A Study on the Highest Exposure Temperatures of Exposed Reinforced Concrete Structures at Fire (화재에 노출된 철근콘크리트 구조물의 최고노출온도 추정을 위한 연구)

  • Kim, Seong Soo;Lee, Jeong Bae;Kim, Il Kon;Song, Jong Jin
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.17 no.2
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    • pp.94-100
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    • 2013
  • In this paper, Machinery analysis was conducted, in order to predict highest exposure temperatures and the analyze fire damage in the case of fire on reinforced concrete structure. After analyzing differential thermal of reference materials in accordance with temperature of concrete reference core specimen, it turned out that powerful endothermic peak came resulting from evaporation of capillary water and get water untill $200^{\circ}C$, another endothermic peak came resulting from decomposition of calcium hydroxide at $520^{\circ}C$, and then mass of reference materials remarkably decreased due to endothermic reaction. Another powerful endothermic reaction came after decomposition of calcite at $720^{\circ}C$. After analyzing X-ray diffraction of reference materials in accordance with temperature of concrete reference core specimen, it turned out that calcium hydroxide existed until the temperature of $400^{\circ}C$, but CH almost disappeared and CaO appeared from $600^{\circ}C$. The production increased in proportion to the temperature. This is because that calcium hydroxide and calcite are decomposed and CaO is produced when the temperature of concrete increases with fire. It is estimated that calcium hydroxide and calcite are utterly decomposed and peak disappears, and peak of CaO is remarkably formed instead, at the temperature of $700-800^{\circ}C$.

FUSION MATERIALS AND FUSION ENGINEERING R&D IN JAPAN

  • KOHYAMA A.;KONISHI S.;KIMURA A.
    • Nuclear Engineering and Technology
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    • v.37 no.5
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    • pp.423-432
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    • 2005
  • Japanese activities on fusion structural materials R&D have been well organized under the coordination of university programs and JAERI/NIMS programs more than two decades. Where, two categories of structural materials have been studied, those are; reduced activation martensitic/ferritic steels (RAFs) as reference material and vanadium alloys and SiC/SiC composite materials as advanced materials. The R&D histories of these candidate materials and the present status in Japan are reviewed with the emphasis on materials behavior under radiation damage. The importance of IFMIF and technology development for blanket R&D including ITER-TBRG activity is emphasized and the current status of those activities in Japan is also presented.

A Investigation the Aircraft Pilots Licence Acquisition Standard Reference Material Providing (항공기조종사 자격증명취득 표준교재 제공에 관한 고찰)

  • Park, Wontae
    • Journal of Advanced Navigation Technology
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    • v.20 no.6
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    • pp.580-587
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    • 2016
  • In the purpose of suggesting the necessity and proper method of providing the standard reference material for acquiring the aircraft pilot license, this study provides the FAA and ROKAF case study, and positively analyzes the materials of 178 pilots and student pilots who acquired the aircraft pilot license. The result of case study shows that compared to the case of Korea which the restriction on the standard reference material providing exists, the FAA(Federal Aviation Administration) and ROKAF are currently providing the standard reference material. Additionally, the result of positive analysis indicates the fact that the necessity of standard reference material providing is well recognized and its importance also found to be remarkably high. These results represent that the standard reference material providing is necessary for training competent aircraft pilots. Also, this will mitigate the current shortage of aircraft pilots due to the rapid growth of air transportation industry, and this will play an important role in preventing diverse aircraft-related accidents.

A Study of Analytical Sensitivity on TDM Test Kit in Clinical Chemistry (약물검사 키트의 분석 민감도에 대한 연구)

  • Chang, Sang Wu;Kim, Nam Yong;Lee, Hee Gyung;Kim, Hyun Jung;Lee, Yun Jung;Jin, Ok Bae;Kim, Mi Gyung
    • Korean Journal of Clinical Laboratory Science
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    • v.36 no.2
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    • pp.127-130
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    • 2004
  • Analytical sensitivity on TDM test is the lowest concentration that can be distinguished from background noise. The aim of study was to evaluate analytical sensitivity that is also referred to as the lower limit of detection(LLD) about difference between zero calibrator and isotonic saline sample. We tested for 10 days with zero calibrators and 0.85% saline samples while running trilevel control samples under control. Raw data divided by two groups calculated mean and standard deviation from two sample populations and analytical sensitivity by ${\bar{X}}+2SD$. In comparison with isotonic saline samples and zero calibrators, there were significant differences in phenytoin, phenobarbital and vancomycin, etc. Especially analytical sensitivity on phenytoin is at the same level as the upper limit of analytical measurement range with $40{\mu}g/mL$. We think the cause of this is matrix interference. In conclusion, we were sure that standard protocol for analytical sensitivity as lower limit of analytical measurement range on TDM test must be measured with zero standard rather than an isotonic saline sample and type 1 reagent DW for reducing matrix effects within interactions between different materials in a mixture.

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