• 제목/요약/키워드: Reference Material

검색결과 1,349건 처리시간 0.031초

Measurements of the rheological properties of standard reference material 2490 using an in-line micro-Fourier rheometer

  • Smith R. S.;Glasscock J. A.
    • Korea-Australia Rheology Journal
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    • 제16권4호
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    • pp.169-173
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    • 2004
  • The control of the rheological properties of a fluid during processing is important and can determine the efficiency of the production in addition to the performance of the final product. The vast majority of process fluids are viscoelastic, hence an instrument that measures both the viscous and elastic properties of the material during processing would be of great practical use. However, most in-line instruments commercially available to date are only capable of measuring viscosity at a single shear rate. An in-line rheometer that measures both the viscous and elastic properties of fluids over a wide range of shear rates simultaneously has been described in a previous publication (Glasscock et at., 2003) in which the results of measurements on flowing sunflower oil were presented. Before this instrument can be used in an industrial situation, it must be demonstrated that the generated results are the same as, or bear some fixed relationship to, the results obtained by conventional off-line rheometers. To this end, the present investigation describes the measurements of a standard reference fluid, polyisobutylene dissolved in 2,6,10,14-tetramethylpentadecane, labelled SRM2490 by the National Institute of Standards and Technology (NIST) in the USA. The results obtained using the in-line rheometer show remarkably good correlation for viscosity, using a modified Cox­Merz rule, with the results supplied with the reference material from NIST.

새로운 CMOS 전압-전류 안정화 회로 설계 (The New Design of CMOS Voltage-Current Reference Circuit for Stable Voltage-Current Applications)

  • 김영민;황종선
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.2
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    • pp.1239-1243
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    • 2004
  • A novel voltage-current reference circuit for stable voltage-current applications is Proposed. Circuits for a positive and for a negative voltage-current reference are presented and are designed with commercial CMOS technology. The voltage-current reference that is stable over ambient temperature variations is an important component of most data acquisition systems. These results are verified by the HSPICE simulation $0.8{\mu}m$ parameter. As the result, the temperature dependency of output voltage and output current each is $0.57mV/^{\circ}C$, $0.11{\mu}A/^{\circ}C$ and the power dissipation is 1.8 mV on 5V supply voltage.

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인증표준물질(CRM)을 이용한 소변 중 대마 대사체 분석법 평가 (Analysis of 11-nor-9-carboxy-Δ9-tetrahydrocannabinol in urine with certified reference material)

  • 고범준;김진영;김종상;이정직;정재철;서승일;인문교
    • 분석과학
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    • 제23권1호
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    • pp.83-88
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    • 2010
  • 대검찰청 마약감식실은 대마 흡연여부를 판별하는 수단인 소변 중 대마 대사체 성분 분석법 에 대한 신뢰도 평가를 위하여 인증표준물질을 이용한 시험을 실시하였다. 시험에 사용된 인증표준물질은 미국 NIST에서 판매하는 Standard Reference Material 1507b로, 11-nor-${\Delta}^9$-tetrahydrocannabinol-9-carboxylic acid (THCCOOH)가 함유된 냉동 건조 소변이었다. NIST에서 구매한 인증표준물질의 농도값과 실험실에서 측정한 농도값을 비교 평가해 본 결과, 약 95% 신뢰수준에서 일치하였다.

공동주택의 표준자재 범용화를 위한 정보요소의 연계 및 개발방안 연구 (Study on the Linking Method of Information Factors in order to use in wide of Standard Material into Apartment Housing Construction)

  • 박근수;임석호
    • 한국주거학회:학술대회논문집
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    • 한국주거학회 2008년 추계학술발표대회 논문집
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    • pp.448-451
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    • 2008
  • This study is under doing to suggest application manual using assembling reference plane design & standard finish material basis upon material classification code as a tool of a linkage between building design and construction standarization in order to enlarge the applicability of house building material that is produced by the module plant. We can say the goal of building standardization intend not only the improvement of construction productibility but also guarantee of subsequent performance through automatization basis upon informationalization of building design. For a etabilishing of this condition, it is neccessary to link the standardization's result of material--design--construction field. According to this neccessity, we are going to suggest information factor that can make relative business manager easily approach to the standardization practical task.

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Development of a Chloroform Reference Material for the Proficiency Testing of Hazardous Compounds in Commercial Consumer Chemical Products Under the Consumer Chemical Products and Biocide Safety Management Act (K-BPR)

  • Lee, Sang Tak;Lee, Jae-ung;Kim, Joo-Hyon;Oh, Han Bin
    • Mass Spectrometry Letters
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    • 제10권4호
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    • pp.112-116
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    • 2019
  • In this study, a chloroform consumer chemical product (CCP) reference material (RM) is successfully developed, with potential to be used in the proficiency testing of hazardous compounds in CCPs for analysis and testing agencies. Validation experiments are rigorously conducted to evaluate whether the RM meets the requirements set by the ISO 13528 and ISO Guide 35, using a reliable GC/MS method for the analysis of chloroform. The obtained calibration plot linearity, limit of detection (LOD), and limit of quantitation (LOQ) are excellent. The developed RM meets the homogeneity and stability requirements; the between-unit (sbb) and within-unit (swb) standard deviations are less than 2.5%, and the stability is found to be guaranteed for 50 days.

기준신호 보상회로를 이용한 더블 샘플링 방식의 비냉각형 볼로미터 검출회로 설계에 관한 연구 (A Study on Double Sampling Design of CMOS ROIC for Uncooled Bolometer Infrared Sensor using Reference Signal Compensation Circuit)

  • 배영석;정은식;오주현;성만영
    • 한국전기전자재료학회논문지
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    • 제23권2호
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    • pp.89-92
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    • 2010
  • A bolometer sensor used in an infrared thermal imaging system has many advantages on the process because it does not need a separate cooling system and its manufacturing is easy. However the sensitivity of the bolometer is low and the fixed pattern noise(FPN) is large, because the bolometer sensor is made by micro electro mechanical systems (MEMS). These problems can be fixed-by using the high performance readout integrated circuit(ROIC) with noise reduction techniques. In this paper, we propose differential delta sampling circuit to remove the mismatch noise of ROIC itself, the FPN of the bolometer. And for reduction of FPN noise, the reference signal compensation circuit which compensate the reference signal by using on-resistance of MOS transistor was proposed.

기준저항 보상회로를 이용한 비냉각형 볼로미터 검출회로의 설계에 관한 연구 (A Study on the Design of a ROIC for Uncooled Bolometer Thermal Image Sensor using Reference Resistor Compensation)

  • 유승우;곽상현;정은식;성만영
    • 한국전기전자재료학회논문지
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    • 제22권2호
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    • pp.119-122
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    • 2009
  • As infrared light radiates, the CMOS Readout IC (ROIC) for the microbolometer typed infrared sensor detects voltage or current which is caused by the variation of resistance in the bolometer sensor. A serious problem we may have in designing the ROIC is the value of bolometer and reference resistors will be changed due to process variation. Since each pixel does not have the same value of resistance, fixed pattern noise problems happen during the sensor operations. In this paper, we propose a novel technique to compensate the fluctuation of reference resistance with taking account of process variation. By using a comparator and a cross coupled latch, we will make the value of reference resistor same as the bolometer's.

가구소재의 화재전파해석을 위한 열해리 물성 평가 (Estimation of Pyrolysis Properties for Fire Propagation Analysis of Furniture Materials)

  • 김성찬
    • 한국화재소방학회논문지
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    • 제27권4호
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    • pp.41-46
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    • 2013
  • 본 연구는 가구류를 구성하는 주요 재료의 열적조건에 따른 반응특성과 화염전파해석에 필요한 열해리 물성을 제공하기 위해 열중량분석을 수행하였다. 실험대상 시편은 가구류에 널리 적용되는 MDF 판재와 코팅재, 합성피혁과 쿠션재 등이며 가열율 $10^{\circ}C/min$, 최대 온도 $600^{\circ}C$까지 실험을 수행하였다. 실험결과 MDF 소재의 경우 $324^{\circ}C$에서 피크 반응을 나타냈었으며 MDF 코팅재의 경우 초기 피크반응온도가 $270{\sim}280^{\circ}C$로 감소하였다. 합성피혁과 폼 소재의 경우 재료를 구성하는 폴리머의 종류에 따라 기준온도와 기준 반응율이 차이를 보였으나 기준온도는 $270^{\circ}C$$420^{\circ}C$ 정도로 비교적 유사한 경향을 나타냈다. Lyon 등이 제시한 방법에 의해 반응상수와 활성화 에너지를 산정하기 위해 시편의 기준 온도와 기준 반응율을 제시하였으며 이러한 기초 물성연구를 통해 화염전파특성을 이해함과 동시에 화재해석의 신뢰성을 향상시키는데 기여하고자 한다.

MRAM용 HSPICE 마크로 모델과 midpoint reference 발생 회로에 관한 연구 (HSPICE Macro-Model and Midpoint-Reference Generation Circuits for MRAM)

  • 이승연;이승준;신형순
    • 대한전자공학회논문지SD
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    • 제41권8호
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    • pp.105-113
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    • 2004
  • MRAM (Magneto-resistive Random Access Memory)은 자성체의 스핀 방향을 정보원으로 하는 비휘발성 메모리로 magneto-resistance 물질을 정보 저장 소자로 사용한다. 본 논문에서는 MRAM 시뮬레이션시 MTJ (Magnetic Tunneling Junction)의 hysteretic 특성, asteroid 특성, R-V 특성을 HSPICE에서 재현할 수 있는 새로운 macro-model을 제안하고 HSPICE에 적용하여 그 정확도를 검증하였다. 또한 종래의 reference cell 회로에 비하여 정확한 중간 저항 값을 유지하는 새로운 reference cell 회로를 제안하고 이를 본 논문에서 제안한 macro-model을 이용하여 검증하였다.

공간주파수대역에서 기저대역 확장을 통한 원전 대비시험편과 대비 보정 시험편의 초음파 영상 개선 (Ultrasonic Images Enhancement of the SS Reference Specimen and the Reference Calibration Block for NPPs by the Combining Bases of Support for Spatial Frequency)

  • 박치승;김선진
    • 한국재료학회지
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    • 제13권10호
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    • pp.651-657
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    • 2003
  • Ultrasonic microscope has been used to detect the defects on surface or inner solid. Conventionally, it has used at a single operating frequency. The resolution and quality of the measured images are determined by a characteristic of the transducer of the ultrasonic microscope. The conventional ultrasonic microscope has been used envelope detector to detect the amplitude of reflected signal, but the changes in amplitude is not sensitive enough for specimen with microstructure that in phase. In this paper, we have studied multi-frequency depth resolution enhancement with ultrasonic reflection microscope for the reflectors of a stainless steel reference specimen and a reference calibration block to be used as the material in nuclear power plants for ISI, PSI. Increased depth resolution can be obtained by taking two, three-dimensional images at more that one frequency and numerically combining the results. As results of the experiment, we could get enhanced images with the rate of contrast in proportion and high quality signal distribution for the image to the changing rate of depth for the reflectors of the two kinds of specimens.