• Title/Summary/Keyword: Pulse characterization

Search Result 147, Processing Time 0.024 seconds

Investigating of the Properties of ZnO Film Synthesized by Pulsed Laser Deposition (펄스레이저 증착법에 의해 성장된 ZnO 박막의 특성 관찰)

  • Choi, Jae-wan;Ji, Hyun-jin;Jung, Chang-Uk;Lee, Bo-Hwa;Kim, Gyu-Tae
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.24 no.2
    • /
    • pp.108-111
    • /
    • 2011
  • The semiconducting material of ZnO in II-VI group was well known as its good application for photo electronics, chemical sensors and field effect transistors due to the remarkable optical properties with wide energy band gap and great ionic reactivities. Up to now the growth of a good quality of ZnO film has been issued for better performances. Even though there were many deposition methods for making ZnO films, pulse laser deposition methods have been preferred for high crystalline films. In this report, the ZnO film was also created by pulsed laser deposition technique which also showed high crystalinity. By controlling several factors when deposited, it was investigated that the optimal condition for ZnO film formation. Mainly, oxygen partial pressures and growth temperatures were changed when ZnO films were synthesized and followed the characterization by HRXRD and AFM.

The Characterization of the Increase of Membrane Conductance after Depolarization in Single Rat Adrenal Chromaffin Cells

  • Lim, Won-Il;Kim, Sang-Jeong;Kim, Jun
    • The Korean Journal of Physiology and Pharmacology
    • /
    • v.2 no.1
    • /
    • pp.95-100
    • /
    • 1998
  • The conductance change evoked by step depolarization was studied in primarily cultured rat adrenal chromaffin cells using patch-clamp and capacitance measurement techniques. When we applied a depolarizing pulse to a chromaffin cell, the inward calcium current was followed by an outward current and depolarization-induced exocytosis was accompanied by an increase in conductance trace. The slow inward tail current which has the same time course as the conductance change was observed in current recording. The activation of slow tail current was calcium-dependent. Reversal potentials agreed with Nernst equation assuming relative permeability of $Cs^+\;to\;K^+$ is 0.095. The outward current and tail current were blocked by apamin (200 nM) and d-tubocurarine (2 mM). The conductance change was blocked by apamin and did not affect membrane capacitance recording. We confirmed that conductance change after depolarization comes from the activation of the SK channel and can be blocked by application of the SK channel blockers. Consequently, it is necessary to consider blocking of the SK channel during membrane capacitance recording.

  • PDF

Synthesis of graphene nano-sheet without catalysts and substrates using fullerene and spark plasma sintering process

  • Jun, Tae-Sung;Park, No-Hyung;So, Dea-Sup;Lee, Joon-Woo;Lim, Hak-Sang;Ham, Heon;Shim, Kwang Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.23 no.1
    • /
    • pp.27-30
    • /
    • 2013
  • Catalyst-free graphene nano-sheets without substrates have been synthesized using fullerene and a high direct current (dc) pulse in the spark plasma sintering (SPS) process. Graphene nano-sheets were synthesized directly in the gas phase of carbon atoms which are generated from fullerene at a temperature of $600^{\circ}C$. Characterization has been carried out by scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HR-TEM), Raman spectroscopy (Raman), X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD).

Systematic Approach of Internal Parameters for Equivalent Electrical-Circuit Modeling(EECM) of a Li4Ti5O12(LTO) cell (Li4Ti5O12(LTO) 배터리 등가회로 모델링을 위한 내부 파라미터 체계적 해석)

  • Lee, Pyeong-Yeon;Yoon, Chang-O;Park, Jin-Hyeong;Kim, Jonghoon
    • The Transactions of the Korean Institute of Power Electronics
    • /
    • v.23 no.3
    • /
    • pp.174-181
    • /
    • 2018
  • This study introduces a systematic approach to selecting the internal parameters applied to the equivalent electrical-circuit model (EECM) of a lithium titanium oxide ($Li_4Ti_5O_{12}$; LTO) rechargeable cell. Based on the dynamic characteristic of the cell, a simplified EECM consisting of an open-circuit voltage (OCV), an ohmic resistance, and an RC ladder is fabricated. To select the internal parameters of a simplified EECM, experiments on discharge capacity, OCV, and discharge/charge resistances are performed using hybrid pulse power characterization and direct current internal resistance (DCIR) measurements over the full state-of-charge (SOC) range. The experimental results of the LTO rechargeable cell highlight the importance of correct selection of internal parameters that can reduce EECM errors. This study clearly provides experimental procedures, internal parameters results, and EECM guidelines for adaptive control-based SOC estimation for LTO rechargeable cells.

Thermal Stability of Silicon-containing Diamond-like Carbon Film (실리콘 함유 DLC 박막의 내열특성)

  • Kim, Sang-Gweon;Kim, Sung-Wan
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.23 no.2
    • /
    • pp.83-89
    • /
    • 2010
  • Diamond-like carbon (DLC) coating was studied to be a good tribological problem-solver due to its low friction characteristics and high hardness. However, generally hydrogenated DLC film has shown a weak thermal stability above $300^{\circ}C$. However, the silicon doping DLC process by DC pulse plasma enhanced chemical vapor deposition (PECVD) for the new DLC coating which has a good characterization with thermal stability at high temperature itself has been observed. And we were discussed a process for optimizing silicon content to promote a good thermal stability using various tetramethylsilane (TMS) and methane gas at high-temperature. The chemical compositions of silicon-containing DLC film was analyzed using X-ray photoelectron spectroscopy (XPS) before and after heat treatment. Raman spectrum analysis showed the changed structure on the surface after the high-temperature exposure testing. In particular, the hardness of silicon-containing DLC film showed different values before and after the annealing treatment.

Probing of Microscale Phase-Change Phenomena Based on Michelson Interforometry (Michelson 간섭계를 응용한 미세 상변화 현상 계측)

  • Kim, Dong-Sik;Park, Hui-Gwon;Grigoropoulos, Costas-P.
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.25 no.8
    • /
    • pp.1140-1147
    • /
    • 2001
  • Experimental schemes that enable characterization of phase-change phenomena in the microscale regime are essential for understanding the phase-change kinetics. Particularly, monitoring rapid vaporization on a submicron length scale is an important yet challenging task in a variety of laser-processing application, including steam laser cleaning and liquid-assisted material ablation. This paper introduces a novel technique based on Michelson interferometry for probing the liquid-vaporization process on a solid surface heated by a KrF excimer laser pulse(λ=248nm, FWHM=24ns) in water. The effective thickness of a microbubble layer has been measured with nanosecond time resolution. The maximum bubble size and growth rate are estimated to be of the order of 0.1㎛ and 1m/s, respectively. The results show that the acoustic enhancement in the laser induced vaporization process is caused by bubble expansion in the initial growth stage, not by bubble collapse. This work demonstrates that the interference method is effective for detecting bubble nucleation and microscale vaporization kinetics.

Prevalence and Characterization of Vancomycin-Resistant Enterococci in Chicken Intestinles and Humans of Korea

  • Seong, Chi-Nam;Shim, Eun-Sook;Kim, Shin-Moo;Yoo, Jin-Cheol
    • Archives of Pharmacal Research
    • /
    • v.27 no.2
    • /
    • pp.246-253
    • /
    • 2004
  • The prevalence, genotype for antibiotic resistance and antibiotic susceptibility of vancomycin resistant enterococci (VRE) were determined. And molecular typings of the Enterococcus faecium isolates were analyzed. Prevalence of VRE in chickens, healthy children and intensive care unit (ICU) patients was 41.6%,7.9%, and 20.4%, respectively. Forty out of 54 isolates from chicken intestines, and 9 out of 11 from ICU patients were identified as Enterococcus faecium. Eleven out of 13 isolates from non-hospitalized young children were E. gallinarium. Twelve strains of E. faecalis were isolated from chicken intestines. The gene for the antibiotic resistance in E. faecium, and E. faecalis was vanA, while that in E. gallinarium was vanC1. E. faecium isolates were resistant to most of antibiotics except ampicillin and gentamicin. Molecular typing of the E. faecium strains obtained by pulse field gel electrophoresis and repetitive sequence-based PCR suggest that VRE transmit horizontally from poultry to humans, especially young children, via the food chains in Korea.

Characteristics of Rh- Pd- Pt Three-Way Catalysts with Double-Layer Washcoat on the Hydrothermal Aging (이중층 워시코트 Rh-Pd-Pt 삼원촉매의 열적 열하에 따른 반응 특성)

  • Choi Byungchul;Jeong Jongwoo;Son Geonseog;Jung Myunggun
    • Transactions of the Korean Society of Automotive Engineers
    • /
    • v.14 no.1
    • /
    • pp.8-16
    • /
    • 2006
  • The research was conducted to characterize of Rh-Pd-Pt TWC with a double-layer washcoat for gasoline vehicle. The physical characteristics on surface of catalyst were inspected by BET, SEM and TEM. The characteristics of catalytic reaction were examined by the TPD/TPR and CO-pulse chemisorption. The catalyst $6Hx(0.35\times11\times3)$ showed superior conversion performance after hydrothermal aging process, which was due to small difference of the surface area between. the fresh and the aged catalyst. The CO-chemisorption and surface area were superior in the 600 cpsi catalyst than other catalysts, this catalyst also shown the higher conversion efficiency of the exhaust emissions. From the TPR test, the conversion performance of the aged catalyst was decreased by the agglomeration and sintering of the PM and metal oxides. From the TPD result, it was found that the NO chemisorption was happed on the bottom-layer washcoat with Pd, and the NO chemisorption was re-happened on the upper-layer washcoat with Pt and Rh in the desorption process.

Development and Characterization of Multi-Segmented Tissue Equivalent Proportional Counter for Microdosimetry (마이크로 도시메트리용 다분할 조직등가비례계수기의 개발과 특성 평가)

  • Nam, Uk-Won;Park, Won-Kee;Lee, Jaejin;Pyo, Jeonghyun;Moon, Bong-Kon;Moon, Myung Kook;Lim, Chang Hwy;Lee, Suhyun;Kim, Sunghwan
    • Journal of Sensor Science and Technology
    • /
    • v.24 no.2
    • /
    • pp.101-106
    • /
    • 2015
  • We designed, developed and characterized a multi-segmented tissue equivalent proportional (TEPC) counter for microdosimetry. The energy resolution of the multi-segmented TEPC was about 12% for $^{241}Am$ 5.45 MeV alpha particles. The resolution was better than 33% for a single un-segmented TEPC. A compact and low power consumption TEPC could be made by using digital pulse processor (DPP). We also successfully calibrated the TEPC by using $^{252}Cf$ standard neutron source in Korea Research Institute of Standards and Science (KRISS). According to the results, the TEPC is useful for several application of radiation monitoring such as a neutron monitor, air crew monitor and space dosimeter.

Electrodeposition and characterization of Ni-W-Si3N4 alloy composite coatings

  • Choi, Jinhyuk;Gyawali, Gobinda;Lee, Soo Wohn
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2015.05a
    • /
    • pp.171-172
    • /
    • 2015
  • $Ni-W-Si_3N_4$ alloy composite coatings were prepared by pulse electro-deposition method using nickel sulfate bath with different contents of tungsten source, $Na_2WO_4.2H_2O$, and dispersed $Si_3N_4$ nano-particles. The structure and micro-structure of coatings was separately analyzed by X-ray diffraction (XRD) and scanning electron microscope (SEM). Results indicated that nano $Si_3N_4$ and W content in alloy had remarkable effect on micro-structure, micro-hardness and scratch resistant properties. Tungsten content in Ni-W and $Ni-W-Si_3N_4$ alloy ranged from 7 to 14 at.%. Scratch test results suggest that as compared to Ni-W only, $Ni-W-Si_3N_4$ prepared from Ni/W molar ratio of 1:1.5 dispersed with 20 g/L $Si_3N_4$ has shown the best result among different samples.

  • PDF