• Title/Summary/Keyword: Pre-curing

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Mineral and Compressive Strength Characteristics of Calcium Silicate and Calcium Sulfoaluminate Mixed Cement in Carbon Dioxide Atmosphere (이산화탄소 분위기에서 칼슘실리케이트와 칼슘설포알루미네이트 혼합시멘트의 광물 및 압축강도 특성)

  • Dae-geun Lee;Sun-Mok Lee;Jung-Jun Park;Ki-Yeon Moon;Kye-Hong Cho;Jin-Sang Cho
    • Resources Recycling
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    • v.32 no.6
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    • pp.10-17
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    • 2023
  • Calcium silicate cement (CSC) is an environmentally sustainable, low-carbon cement and has garnered significant attention in recent studies. However, the pre-curing step required to activate the carbon dioxide reaction and to handle the sample. This study aimed to examine the viability of extending the application of CSC without pre-curing by enhancing initial strength by mixing calcium sulfoaluminate (CSA) fast-hardening cement into CSC. The investigation assessed changes in compression strength and Q-XRD mineral characteristics concerning variations in the mixing ratio of CSC and CSA fast-hardening cement within a carbon dioxide atmosphere. The compressive strength results indicated that the 3-day and 7-day strengths were 14.18 MPa and 22.98 MPa, respectively, under the 50% CSC condition, meeting the type 1 cement KS standard. Mineral characteristics analysis revealed an increase in calcite mineral, a byproduct of the carbon dioxide reaction, contributing to strength enhancement. Even after seven days, substantial quantities of unreacted rankinitene and pseudowollastonite were observed, as well as dicalcium silicate and yeelimite, which are hydrated minerals. This observation was confirmed the possibility of strength improvement after 7 days.

Hot AC Anodising as a Cr(VI)-free Pre-treatment for Structural Bonding of Aluminium

  • Lapique, Fabrice;Bjorgum, Astrid;Johnsen, Bernt;Walmsley, John
    • Journal of Adhesion and Interface
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    • v.4 no.2
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    • pp.21-29
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    • 2003
  • Hot AC anodising has been evaluated us pre-treatment for aluminium prior to structural adhesive bonding. Phosphoric and sulphuric acid hot AC anodising showed very promising adhesion promoter capabilities with durability comparable with the best standard DC anodising procedures. AC anodising does not required etching prior to anodising and offers u pre-treatment time down to 20 seconds. The interface/interphase between the aluminium substrate and the adhesive was investigated in order to get a better understanding of the involved adhesion mechanisms and to explain the long-tenn properties. The alkaline medium formed at the oxide layer/adhesive interface has been shown to induce a partial dissolution of the oxide layer leading to the formation of metallic ions which diffuse in the adhesive (EPMA measurements). The effect of diffusion of the Al ions on adhesion and joint durability is still uncertain but studies showed that pre-bond moisture affected the joints durability and to some extent the diffusion length. specially for DC anodised samples. So far no direct correlation could be established between the diffusion length d and the joints durability but new trials with better control over the elapsed time between bonding and adhesive curing are expected to help getting a better understanding of the involved mechanisms.

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Effects of Salt Concentration in Soybean Sauce on the Physicochemical Properties of Pre-rigor Ground Hanwoo Muscle

  • Kim, Hyun-Wook;Choi, Ji-Hun;Choi, Yun-Sang;Kim, Hack-Youn;Han, Doo-Jeong;Kim, Tae-Hyun;Lee, Sung-Ki;Kim, Cheon-Jei
    • Food Science of Animal Resources
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    • v.31 no.3
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    • pp.389-397
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    • 2011
  • This study was conducted to examine the effect of salt concentration in soybean sauce (ganjang) on pre-rigor ground Hanwoo (Korean native cattle) muscle. Although adding soybean sauce reduced pH of pre-rigor Hanwoo muscle, it improved the water holding capacity (WHC), cooking loss, total protein solubility, myofibrillar fragmentation index (MFI), 2-thiobar-bituric acid (TBA) values, and textural properties by increasing salt concentration in the soybean sauce. In particular, adding soybean sauce inhibited lipid oxidation despite increasing salt concentration. An increased salt concentration in the soybean sauce in pre-rigor Hanwoo muscle tended to make the meat have lower lightness and higher redness and yellowness values. Although soybean sauce had a significantly lower pre-rigor salting effect than sodium chloride in terms of cooking loss and total protein solubility (p<0.05), soybean sauce improved myofibrillar fragmentation and lipid oxidation when compared with sodium chloride. Furthermore, no significant differences in textural properties were observed between adding soybean sauce and sodium chloride at the same salt concentrations. Therefore, soybean sauce can be a functional curing material for pre-rigor muscle.

Cure Kinetics of Epoxy/Diamine System Modified with Malononitrile by Barrett Method and Integral Method (Malononitrile에 의해 개질된 Epoxy/Diamine계의 경화반응 속도론: Barrett Method와 Integral Method)

  • Cheon, In-Suk;Don, Yun-Seung;Sim, Mi-Ja;Kim, Sang-Uk
    • Korean Journal of Materials Research
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    • v.4 no.5
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    • pp.574-580
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    • 1994
  • This study is about cure kinetics of DGEBA/MDA/MN(malononitrile) system by Barrett method and Integral method using DSC dynamic run. Curing behavior was shown through DSC and the heat change involved in a reaction could be measured directly with DSC. The kinetic parameters such as activation energy, pre-exponential factor and reaction order were given by Barrett method and Integral method obtained in an assumption that the area of DSC enthalpic analysis curve was propotional to the enthalpic change.

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A Study on Pre-treatment and Performance Evaluation for Printing RFID Antenna with Conductive Paste (RFID 안테나용 전도성 프린팅을 위한 PET 직물의 최적 전처리 공정연구 및 성능평가)

  • Hong, Jinpyo;Jung, Chando;Yoon, Seokhan;Choi, Sanghyun
    • Textile Coloration and Finishing
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    • v.25 no.4
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    • pp.287-291
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    • 2013
  • Nowadays, terms such as 'Smart Textile', 'Intelligent Textile' and 'Wearable Computing' are commonly used in everyday contexts. And radio-frequency identification (RFID) is the use of a wireless non-contact system that uses radio-frequency electromagnetic fields to transfer data from a tag attached to an object, for the purposes of automatic identification and tracking. These products are required technologies which are textile treatments, printing, ink, etc. Durability of textile substrates is an essential marker for conductive ink printing process. Especially, heat stability is important, since conductive ink should be processable (annealing, curing) at temperatures below $150^{\circ}C$. This study was application of RFID on textiles. The textile pre-treatment processes should be carried out to use RFID antenna on textiles.

Effects of Pre-salting on the Components Changes in the Preparation of Salted Anchovy (Engraulis japonica)

  • Cho Young-Je;Shim Kil-Bo;Kim Tae-Jin;Ju Jung-Mi;Choi Yeung-Joon
    • Fisheries and Aquatic Sciences
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    • v.3 no.3_4
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    • pp.200-204
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    • 2000
  • To investigate pre-salting conditions in the preparation of salted anchovy from large anchovy, anchovy were salted with various salt concentration and stored at $5^{\circ}C$ and $20^{\circ}C$ for 10 days. Moisture content decreased with the increase of salt and the salinity increased in proportion to salt concentration at $20^{\circ}C$. Total nitrogen decreased slightly as the increase of salt concentration during pre-salting at $20^{\circ}C$. The nitrogenous components such as amino nitrogen and extractable nitrogen were invariable or decreased until 7 days in salt concentration over $25\%$ during pre-salting at $5^{\circ}C$. These results imply that soluble nitrogen with moisture run out of anchovy body in high salt concentration and the hydrolysis was inhibited by salt over $25\%$ at $5^{\circ}C$. VBN content were constant in salt concentration over $25\%$ until 7 days, regardless of curing temperature. The POV were under the influence of salt concentration and temperatures. We concluded that the optimal condition for preparation of salted anchovy were pre-salting with salt over $25\%$ at $5^{\circ}C$ for 7 days.

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Effect of Formability of Physical Properties of Polyester/Melamine Cured Coating Using Polycarbonate Diol with Various Molecular Weight (폴리카보네이트 분자량이 폴리에스터/멜라민 경화형도료의 도막 성형성 및 물성에 미치는 영향)

  • Lee, Yong-Hee;Moon, Je-Ik;Kim, Hyun-Joong;Lee, Jae-Young;Noh, Seung Man;Nam, Joon Hyun
    • Journal of Adhesion and Interface
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    • v.12 no.4
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    • pp.105-110
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    • 2011
  • Polyester/melamine cured coatings had been used for pre-primed coatings and pre-coated metal coatings, because it has good mechanical,chemical properties, and mar resistance. But it has weak points such as stiffness and low formability for making automotive components. Polyester had been synthesized using polycarbonate diol of long alkyl chain which can improve flexibility and formability which is one of the important factors for pre-coated steel sheets (PCM). In this study, strain and tensile strength were examined by the tensile test and formability was examined by the drawing test. Also, Those polyester resins were also measured by DMA to verify flexibility of cured coatings.

Effect of Fermented Spinach as Sources of Pre-Converted Nitrite on Color Development of Cured Pork Loin

  • Kim, Tae-Kyung;Kim, Young-Boong;Jeon, Ki-Hong;Park, Jong-Dae;Sung, Jung-Min;Choi, Hyun-Wook;Hwang, Ko-Eun;Choi, Yun-Sang
    • Food Science of Animal Resources
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    • v.37 no.1
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    • pp.105-113
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    • 2017
  • The effect of fermented spinach extracts on color development in cured meats was investigated in this study. The pH values of raw cured meats without addition of fermented spinach extract or nitrite (negative control) were higher (p<0.05) than those added with fermented spinach extract. The pH values of raw and cooked cured meats in treatment groups were decreased with increasing addition levels of fermented spinach extract. The lightness and yellowness values of raw cured meats formulated with fermented spinach extract were higher (p<0.05) than those of the control groups (both positive and negative controls). The redness values of cooked cured meats were increased with increasing fermented spinach extract levels, whereas the yellowness values of cooked cured meats were decreased with increasing levels of fermented spinach extract. The lowest volatile basic nitrogen (VBN) and thiobarbituric acid reactive substances (TBARS) values were observed in the positive control group with addition of nitrite. TBARS values of cured meats added with fermented spinach extract were decreased with increasing levels of fermented spinach extract and VBN values of curing meat with 30% fermented spinach extract was lower than the other treatments. Total viable bacterial counts in cured meats added with fermented spinach extract ranged from 0.34-1.01 Log CFU/g. E. coli and coliform bacteria were not observed in any of the cured meats treated with fermented spinach extracts or nitrite. Residual nitrite contents in treatment groups were increased with increasing levels of fermented spinach extract added. These results demonstrated that fermented spinach could be added to meat products to improve own curing characteristics.

Optimal Mix Design Model of Recycled Aggregate Concrete for Artificial fishing Reefs (인공어초용 재생골재 콘크리트의 최적 배합설계 모델)

  • 홍종현;김문훈;우광성;고성현
    • Journal of Ocean Engineering and Technology
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    • v.18 no.1
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    • pp.53-62
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    • 2004
  • The Purpose of this study is to recycle the waste concrete, which is generated in huge quantities, from construction works. in order to achieve this goal, it is important to determine the compressive strength, workability, slump, and ultrasonic velocity of recycled aggregate concrete. Thus, several experiment parameters are considered, such as water-cement ratios, sand percentage, and fine aggregate composition ratios, in order to apply the recycled aggregate concrete to pre-cast artificial fishing reefs. From the results, it has been shown that the proper mix designs for reef concrete are W/C=45%, S/a=50%, SR50:SN50 in recycled sand and natural sand mix combination case, W/C=45%, S/a=50%, SC50:SN50 in crushed sand and natural sand mix combination case, W/C=45%, S/a=50%, SR50:SC50 in recycled sand and crushd sand mix combination case. Also, this study shows that the shape and surface roughness of fine aggregate particles have an effect on the strength, slump, ultrasonic velocity of tested concrete, and the compressive strength ratios of 7days' and 90days' curing ages of recycled aggregate concrete are about 70% and 110% of 28days' curing age.

Thermal Curing and Electrical Properties of Epoxy/Graphite/Expanded Graphite Composite for Bipolar Plate of Pemfc (PEMFC 바이폴라 플레이트 제조용 EPOXY/GRAPHITE/EXPANDED GRAPHITE 복합재료의 열경화 및 전기적 성질)

  • Lee, Jae-Young;Lee, Hong-Ki
    • Transactions of the Korean hydrogen and new energy society
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    • v.22 no.6
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    • pp.827-834
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    • 2011
  • Epoxy/graphite/expanded graphite composites have been prepared in various weight ratios and thermal degradation and electrical properties were estimated in order to use for the bipolar plate materials in PEMFC. Thermogravimetric analysis (TGA) showed that the epoxy/graphite system cured by a curing agent GX-533 was most proper because its weight loss until $80^{\circ}C$ at which PEMFC would be operated was 0.3 wt%, and differential scanning calorimetry (DSC) analysis showed its cure temperature would be sufficient at $80^{\circ}C$. The activation energy for the cure reaction was 132.0 kJ/mol and the pre-exponential factor was $1.76{\times}10^{17}min^{-1}$. Electrical conductivity on the surface of the bipolar plate prepared under a pressure of 200 $kgf/cm^2$ was increased from 4 to 25 $S/cm^2$ by increasing expanded graphite (EG) content from 50 phr to 90 phr. The percolation threshold was initiated around 75 phr and the corrosion rate at 80 phr was 1.903 $uA/cm^2$.