• 한국재료학회지
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• 제11권9호
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• pp.745-750
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• 2001

Ni-33.3at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ni and Si) were observed for the 15 min mechanically alloyed (MA 15 min) powder. but $Ni_2$Si and elemental phases were observed to coexist for the 30 min mechanically alloyed (MA 30 min) powder. Elemental Ni and $Ni_2$Si phases were observed for the HIPed compact of MA 15 min powder at 100 and 150 MPa for 2 hr at $800^{\circ}C$. Only the $Ni_2$Si phase was, however, observed for the HIPed compacts of MA 30 min powder. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1100^{\circ}C$ at 150MPa for 2hr. The hardness values of the HIPed $Ni_2$Si compacts at $1100^{\circ}C$ at 100/150 MPa for 2 hr were higher than HRC 66. The densification and mechanical property of HIPed $Ni_2$Si compacts were found to depend on more HIP temperature than HIP pressure.

• 한국분말재료학회지
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• 제8권4호
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• pp.223-230
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• 2001

Ti-37.5at%Si elemental powder mixtures were mechanically alloyed by a high-energy ball mill, followed by CIP (cold isostatic pressing) and HIP (hot isostatic pressing) for different processing conditions. Only elemental phases (Ti and Si) were observed for the 5 min mechanically alloyed (MA 5 min) powder, but only $Ti_5Si_3$phase was observed for the 30 min mechanically alloyed (MA 30 min) powder. $Ti_5Si_3$phase was observed for the HIPed compact of MA 5 min and 30 min powders at 150 and 190 MPa for 3 hr at $1000^{\circ}C$. For the HIPed compacts, the highest sintered density was obtained to be 99.5% of theoretical density by a HIP step at $1350^{\circ}C$ at 190MPa for 3hr. The hardness values of the HIPed $Ti_5Si_3$compacts at $1350^{\circ}C$ at 150/190 MPa for 3hr were higher than HRC 76. The densification and mechanical property of HIPed $Ti_5Si_3$compacts was found to depend on more HIP temperature than HIP pressure.

• 한국분말재료학회지
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• 제9권1호
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• pp.11-18
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• 2002

The 6061 Al alloy based composites reinforced with 10 vol% SiC whiskers were prepared by powder metallurgy with the powders having the different sizes, i.e. < $30{\mu}m$ and > $30{\mu}m$ The composites were subjected to equal channel angular pressing (ECAP) at various conditions and the microstructural changes during ECAP were examined In the composites SiC whiskers were clustered and randomly aligned. The clusters were relatively well distributed in the composite with the smaller initial powder size. After ECAP, the clusters were aligned parallel to flow direction and became smaller. In addition, the shape of clusters was changed from irregular to round. The microstructure of the ECAPed samples were compared with those of the conventionally hot-extruded composites. The uniform microstructure and enhanced microhardness could be obtained by using the powders having the smaller size, decreasing ECAP temperature and repeating ECAP.

• 대한기계학회논문집A
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• 제30권10호
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• pp.1242-1248
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• 2006

Densification behavior of nanocrystalline titania powder was investigated under cold compaction. Experimental data were obtained under triaxial compression with various loading conditions. Lee and Kim proposed the Cap model by developing the parameters involved in the yield function of general Cap model and volumetric strain evolution under cold isostatic pressing. The parameters in the Drucker/Prager Cap model and the proposed model were obtained from experimental data under triaxial compression. Finite element results from the models were compared with experimental data for densification behavior of nanocystalline ceramic powder under cold isostatic pressing and die compaction. The proposed model agreed well with experimental data under cold compaction, but the Drucker/Prager Cap model underestimated at the low density range. Finite element results, also, show the relative density distribution of nanocystalline ceramic powder compacts is severe compared to conventional micron powder compacts with the same averaged relative density.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.841-843
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• 2006

In high-performance cold work applications, tool failure depends on the predominating loading conditions. Typical failure mechanisms are a combination of abrasive wear, adhesive wear, plastic deformation, cracking and edge crumbling. In this paper we demonstrate how the microstructure of tool steels can be positively influenced by modifying the alloying system and the production route to meet the demands of the different loading situations which occur during operation. The investigation was focused on ductility, fatigue strength and wear resistance. Theoretical considerations were confirmed by practical tests.

• 한국세라믹학회지
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• 제31권4호
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• pp.347-358
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• 1994

Creep densification and grain growth of alumina powder compacts during high temperature processing were investigated. The creep densification and grain growth of alumina powder compacts during various sintering processes were analyzed by employing the consitutive model by Kwon and Kim. Theoretical results from the constitutive model were compared with various experimental data of alumina powder compacts in the literature including pressureless sintering, sinter forging and hot pressing. The proposed constitutive equations were implemented into finite element analysis program (ABAQUS) to simulate densification for more complicated geometry and loading conditions. The effects of friction between die and powder compact or punch and powder compact during sinter forging and hot pressing are investigated by using the finite element method. Also, high temperature forming processing of alumina compact with complicated shape was simulated.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.529-530
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• 2006

This paper concerned with SPS (spark plasma sintering), hot pressing of sinter nanometer WC-Co powder and discussed the density, hardness, microstructures and grain sizes of the alloys sintered. The results showed that the two sintered techniques could produce high density alloys and play well on the grain growth, but SPS could lower the sintering temperature and shorten sintering time. Besides, the hardness of the sintered cemented alloys that was dependent on the grain size and densification could also be improved.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.22-23
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• 2006

High velocity compaction (HVC) is a production technique with capacity to significantly improve the mechanical properties of powder metallurgy (PM) parts. Investigated here are green body data such as density, tensile strength, radial springback, ejection force and surface flatness. Comparisons are performed with conventional compaction using the same pressing conditions. Cylindrical samples of a pre-alloyed water atomized iron powder are used in this experimental investigation. The HVC process in this study resulted in a better compressibility curve and lower ejection force compared to conventional quasi static pressing. Vertical scanning interferometry measurements show that the HVC process gives flatter sample surfaces.

• 한국자기학회:학술대회 개요집
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• 한국자기학회 2003년도 하계학술연구발표회 및 한.일 공동심포지엄
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• pp.214-215
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• 2003

• 한국분말재료학회지
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• 제3권1호
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• pp.1-12
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• 1996