• Toxicological Research
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• 제24권3호
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• pp.227-233
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• 2008

To detect lead ions using electrochemical voltammetric analysis, Infrared Photo-Diode Electrode(IPDE) was applied via cyclic and square wave stripping voltammetry. Lead ions were deposited at 0.5 V(versus Ag/AgCl) accumulation potential. Instrumental measurements systems were made based on a simple and compact detection system. The stripping voltammetric and cyclic voltammetric optimal parameters were searched. The results yielded a cyclic range of $40{\sim}240mgl^{-1}$ Pb(II) and a square wave stripping working range of $0.5{\sim}5.00mgl^{-1}$ Pb(II). The relative standard deviation at 2 and 4 $mgl^{-1}$ Pb(II) was 0.04% and 0.02%(n=15), respectively, using the stripping voltammetric conditions. The detection limit was found to be 0.05 $mgl^{-1}$ with a 40 sec preconcentration time. Analytical interference ions were also evaluated. The proposed method was applied to determine lead ions in various samples.

• 한국가스학회지
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• 제5권3호
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• pp.63-72
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• 2001

천연가스 공급용 고압 지하 매설배관에 교류가 유도될 때 쿠폰과 전기저항형 박막센서를 이용하여 교류에 의한 부식속도를 평가하고 주요한 인자를 규명하고자 하였다. 전국에 걸쳐 조사된 교류전압 측정결과를 바탕으로 쿠폰과 전기저항형 박막센서를 설치하고, 주요인자를 고찰하기 위하여 다양한 인자들 (교류전압, 교류전류, 토양 비저항, 주파수, 방식전위)을 정기적으로 기록하였다. 황산동 전극기준 -850mV의 방식전위를 충분히 만족하는 상황에서도 교류에 의한 부식이 진행하였으며, 교류에 의한 부식속도는 교류전압과는 관계없이 교류전류밀도와 주파수에 의존하는 것으로 나타났다. 교류에 의한 부식속도는 유효교류전류밀도에 따라 직선적으로 증가하였으며, 쿠폰에 의한 평가결과 직선의 기울기는 0.619, 전기저항형 센서에 의한 직선의 기울기는 0.885로 나타났다.

• Asian-Australasian Journal of Animal Sciences
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• 제14권8호
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• pp.1144-1148
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• 2001

The implications of incorporating deoiled rice bran (DORB) in diet on the utilization of certain nutrients had been examined through balance studies made with 6- and 10- week-old Japanese quails. The stuffs evaluated in this study had their origin from two different types of processes- a batch extraction (DORB-B) and another continuous process (DORB-C), and each included at 10, 20 or 30% level in an iso-nitrogenous and iso-caloric diet. On chemical analyses, the DORB-B was found to contain crude protein, 19.0; ether extract, 0.79; total ash, 17.05; Ca, 0.11; P, 1.92; glucose, 2.35 and starch 11.22 g/100 g day matter. Corresponding values for DORB-C were 15.02, 1.56, 13.0, 0.40, 2.76, 2.16 and 19.0, respectively. The data on nutrient balances with quails fed diets containing the two-types of DORB suggested no significant (p>0.05) differences in per cent retention of diet dry matter (DM), organic matter (OM), ether extract (EE), gross energy (GE), nitrogen (N), crude fiber (CF), calcium (Ca) or phosphorus (P) content attributable to the extraction process. The age of the birds also appeared to have no significant (p>0.05) effect on nutrient utilization by them. However, the level of inclusion of DORB had a significant (p<0.05) effect on nutrient utilization by quails in that the retention of dietary N, EE, CF, Ca and P was better at lower than at higher levels. It is concluded that the DORB, irrespective of extraction process, can safely be employed upto 20% level in diet of adult Japanese quails without noticeable interference in utilizing the major dietary nutrients.

• 한국정보통신학회:학술대회논문집
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• 한국해양정보통신학회 2001년도 춘계종합학술대회
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• pp.512-515
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• 2001

홀터 심전계는 휴대용 소형 심전도 기록기로서 신체에 부착한 후 일상생활을 계속하면서 심장의 운동 및 전위변화를 기록, 분석하여 심장질환의 유무를 판단하는데 유용하게 쓸 수 있으므로 연구가 활발하게 진행되고 있다. 깨끗한 심전도를 얻기 위해서는 심전도(ECG) 신호에 섞여있는 60Hz 전원 잡음, 기저선 변동, 근 잡음을 제거해야 된다. 홀터 심전계에서 심전도 신호를 기록하는데 있어서 가장 큰 문제를 야기하는 부문이 기저선 변동인데 전극을 부착한 부위의 근육수축과 호흡의 리듬에 따라서 발생하게된다. 그러한 기저선은 상하로 심하게 불규칙한 변동을 하면서 흔들리게 되어 심전도 신호를 진단하는데 어려움이 있으므로 기저선 변동을 제거하는 부분이 매우 중요하다. 본 연구에서는 아날로그 단에서 기저선 변동을 안정화하고 실시간으로 신호 처리할 수 있는 디지털 필터를 구현함으로써 기저선 변동을 제거하는 시스템을 설계하여 환자의 심장질환을 분석하는데 응용할 수 있도록 하였다.

• 대한전기학회논문지:시스템및제어부문D
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• 제54권11호
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• pp.680-688
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• 2005

The electrical current generated by heart creates not only electric potential but also a magnetic field. We have observed electrophysiological phenomena of the heart by measuring components of magnetocardiogram(MCG) using 61 channel superconducting quantum interference device(SQUD) system. We have analyzed the possibility and characteristics of MCG parameters for diagnosis of ischemic heart disease. A technique for automatic analysis of MCG signals in time domain was developed. The methods for detecting the position, the interval, the amplitude ratio, and the direction of single current dipole were examined in the MCG wave. The position and interval parameters were obtained by calculating the gradients of a envelope curve which could be formed by the difference between the maximum and minimum envelope of multi-channel MCG signals. We show some differences of the frequency contour map between the normal MCG and the abnormal (ischemic heart disease) MCG. The direction of single current dipole can be defined by rotating the magnetic field according to Biot-Savart's law at each point of MCG signals. In this study, we have examined the direction of single current dipole from searching for the centroids of positive and negative magnetic fields. The amplitude ratio parameters for measuring 57 deviation consisted of A$_{T}$/A$_{R}$ and other ratios. and We developed a new analysis method, which is based on the frequency contour map of electromagnetic field. Using theses parameters, we founded significant differences between normal subjects and ischemic patients in some parameters.

• 스마트미디어저널
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• 제9권3호
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• pp.71-79
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• 2020

이동통신망은 통화, 메시지, 데이터 전송 등의 서비스를 위하여 많은 사용자들이 전 세계적으로 사용하고 있는 네트워크이다. 이동통신망은 긴급재난망으로도 사용되고 있는 국가적으로 중요한 공공자산이며 이동통신망에서 사이버 공격이나 통신 방해를 이용한 서비스거부공격이 발생할 경우 다양한 피해를 초래할 수 있다. 그러므로 이러한 이동통신망에 대한 안전성 검증이 필수적이나 정해진 몇몇 이동통신사업자들이 망을 구축하여 폐쇄적으로 서비스하고 있고 망의 안전성 검증을 위한 테스트 망이 따로 존재하지 않아 실제로 이동통신망의 코어네트워크를 분석하기는 쉽지 않다. 따라서 본 논문에서는 3GPP 표준을 기반으로 구현하여 오픈소스로 제공되는 OpenAirInterface를 이용하여 가상의 이동통신망을 구축하고 이를 기반으로 코어네트워크 구조와 프로토콜을 분석한다. 특히 단말기에서 전송되는 메시지가 코어네트워크에 미치는 영향을 분석하기 위하여 기지국인 eNodeB와 단말기를 관리하는 MME 사이의 인터페이스인 S1-MME에서의 S1AP 프로토콜 메시지를 분석하여 보안 위협의 실현 가능성을 확인한다.

• 분석과학
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• 제8권1호
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• pp.17-23
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• 1995

$5.0{\times}10^{-2}M$ $LiClO_4$ 용액 중에서 펄스차이 폴라그래피로 2-mercapto-1-methyl-imidazole(MMI)의 정량방법을 조사하였다. 분석의 최적 조건은 초기전위 -0.9 volt vs. Ag/AgCl, 펄스높이 80mV, 주사속도 2mV/sec, 중간 크기 수은방울이었다. 검정곡선은 $1.0{\times}10^{-7}M$에서 $8.0{\times}10^{-5}M$ 범위까지 좋은 직선성을 보여 주었으며, 검출한계는 $2.2{\times}10^{-9}M$이었다. 이 방법은 다른 첨가제의 방해 없이 항갑상선 치료제 중의 MMI 정량에 응용할 수 있었다.

• Asian Journal of Atmospheric Environment
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• 제11권1호
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• pp.1-14
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• 2017

For the quantitative analysis of volatile organic compounds (VOC), the use of a proper solvent is crucial to reduce the chance of biased results or effect of interference either in direct analysis by a gas chromatograph (GC) or with thermal desorption analysis due to matrix effects, e.g., the existence of a broad solvent peak tailing that overlaps early eluters. In this work, the relative performance of different solvents has been evaluated using standards containing 19 VOCs in three different solvents (methanol, pentane, and hexane). Comparison of the response factor of the detected VOCs confirms their means for methanol and hexane higher than that of pentane by 84% and 27%, respectively. In light of the solvent vapor pressure at the initial GC column temperature ($35^{\circ}C$), the enhanced sensitivity in methanol suggests the potential role of solvent vapor expansion in the hot injector (split ON) which leads to solvent trapping on the column. In contrast, if the recurrent relationships between homologues were evaluated using an effective carbon number (ECN) additivity approach, the comparability assessed in terms of percent difference improved on the order of methanol (26.5%), hexane (6.73%), and pentane (5.24%). As such, the relative performance of GC can be affected considerably in the direct injection-based analysis of VOC due to the selection of solvent.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
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• pp.183-183
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• 2011

Multiferroic materials have been widely studied in recent years, because of their abundant physics and potential applications in the sensors, data storage, and spintronics. $BiFeO_3$ is one of the well-known single-phase multiferroic materials with $ABO_3$ structure and G-type antiferromagnetic behavior below the Neel temperature $T_N$ ~ 643 K, but the ferroelectric behavior below the Curie temperature $T_c$~1,103 K. In this study, the $BiFe_{1-x}Ni_xO_3$ (x=0 and 0.05) bulk ceramics were prepared by solid-state reaction and rapid sintering with high-purity $Bi_2O_32$, $Fe_3O_4$ and NiO powders. The powders of stoichiometric proportions were mixed, as in the previous investigations, and calcined at 450$^{\circ}C$ for $BiFe_{1-x}Ni_xO_3$ for 24 h. The obtained powders were grinded, and pressed into 5-mm-thick disks of 1/2-inch diameter. The disks were directly put into the oven, which has been heated up to 800$^{\circ}C$ and sintered in air for 20 min. The sintered disks were taken out from the oven and cooled to room temperature within several min. The phase of samples was checked at room temperature by powder x-ray diffraction using a Rigaku Miniflex diffractometer with Cu K${\alpha}$ radiation. The Raman measurements were carried out by employing a hand-made Raman spectrometer with 514.5-nm-excitation $Ar^+$ laser source under air ambient condition on a focused area of 1-${\mu}m$ diameter. The field-dependent magnetization measurements were performed with a superconducting quantum-interference-device magnetometer.

• 한국미생물학회:학술대회논문집
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• 한국미생물학회 2008년도 International Meeting of the Microbiological Society of Korea
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• pp.62-64
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• 2008

A major hurdle to the development of RNA interference as therapy for HIV infection is the delivery of siRNA to T lymphocytes which are difficult cells to transfect even in vitro. We have employed a single chain antibody to the pan T cell surface antigen CD7 was conjugated to an oligo-9-arginine peptide (scFvCD7-9R) for T cell-specific siRNA delivery in NOD/SCIDIL2${\gamma}$-/- mice reconstituted with human peripheral blood lymphocytes (Hu-PBL). Using a novel delivery, we first show that scFvCD7-9R efficiently delivered CD4 siRNA into human T cells in vitro. In vivo administration to Hu-PBL mice resulted in reduced levels of surface CD4 expression on T cells. Mice infected with HIV-1 and treated on a weekly basis with scFvCD7-9R-siRNA complexes targeting a combination of viral genes and the host coreceptor molecule CCR5 successfully maintained CD4/CD3 T cell ratios up to 4 weeks after infection in contrast to control mice that displayed a marked reduction in CD4 T cell numbers. p24 antigen levels were undetectable in 3 of the 4 protected mice. scFvCD7-9R/antiviral siRNA treatment also helped maintain CD4 T cell numbers with reduced plasma viral loads in Hu-PBL mice reconstituted with PBMC from donors seropositive for HIV, indicating that this method can contain viral replication even in established HIV infections. Our results show that scFvCD7-9R could be further developed as a potential therapeutic for HIV-1 infection.