• 제목/요약/키워드: Porous structure

검색결과 1,192건 처리시간 0.029초

수증기처리공정에 의한 다공성 코디어라이트의 제조 (Preparation of Porous Cordierite by Using Water-Vapour Treatment)

  • 문교태;서신석;노재성;조득희;김동표
    • 한국세라믹학회지
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    • 제34권9호
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    • pp.986-992
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    • 1997
  • Cordierite ceramic was prepared by sol-gel method. It was analyzed by Infrared spectroscopy and X-ray diffraction patterns that the ceramic was chemically mixed in molecular level and transformed to $\alpha$-cordierite at 125$0^{\circ}C$. Water vapour treatments for aging and drying process were conducted to get porous cordierite with thermally stable pore structure. It resulted in 220-410 $m^2$/g BET surface area and mesoporous structure with mean pore diameter, 40$\AA$. Compared to naturally dried ceramic, the ceramic showed superior thermal stability of surface area up to $700^{\circ}C$. Surfaces of porous cordierite ceramics were observed by SEM.

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Responses of Submerged Double Hull Pontoon/Membrane Breakwater

  • Kee S.T.
    • 한국해양공학회지
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    • 제19권2호
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    • pp.19-28
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    • 2005
  • The present paper outlines the numerical investigation of the incident wave interactions with fully submerged and floating dual double hull pontoon/vertical porous membrane breakwaters. Two dimensional five fluid-domains hydro-elastic formulation was carried out in the context of linear wave body interaction theory to study the wave interaction with the double hull of pontoon-membranes. The submerged circular pontoon is consisted of double hulls, which is filled with water in the void space between the outer structure and inner solid buoyant structure. Hydrodynamic characteristics of the proposed system with dual floating double-hull-pontoons filled with water have been studied numerically for the various incident waves. This study is a beginning stage research for the dual double hull porous pontoons/vertical porous membranes breakwaters which is ideally designed in order to suppress significantly the transmitted and reflected waves simultaneously.

다공성 세라믹스와 다공질층을 포함하는 적층체의 제조에 관한 연구;I. 기공구조 (Fabrication of Porous Ceramics and Multi-layered Ceramics Containing Porous Layers; I. Pore Structure)

  • 이해원;윤복규;송휴섭
    • 한국세라믹학회지
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    • 제31권9호
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    • pp.1044-1052
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    • 1994
  • Tape casting technique was successfully applied to produce porous ceramics and multi-layered ceramics containing porous layers, where spherical hollow polymer particles were introduced as pore precursors. In the presence of extreme differences in density and size between Al2O3 and pore precursor particles, hindered settling was effective in preventing segregation of component particles and packing behavior of mixed powders was improved through bimodal packing. There were two transitions in packing behavior of mixed powders. The first transition took place at 40~50 vol% pore precursor addition, where majority of pores changed from close to open pore state. The other transition occured at 60~70 vol% pore precursor addition, where pore precursor particles formed a continuous network structure.

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전류세기의 변화에 따른 DBR 다공성 실리콘의 광학적 특성 (Optical Characterization of DBR Porous Silicon by Changing of Applied Current Density)

  • 최태은;박재현
    • 통합자연과학논문집
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    • 제2권2호
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    • pp.82-85
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    • 2009
  • Distributed Bragg reflector (DBR) porous silicon (PSi) was generated by an electrochemical etching a bragg structure into a silicon wafer through electrode current in aqueous ethanolic HF solution. DBR PSi exhibiting unique reflectivity was successfully obtained by an electrochemical etching of silicon wafer using square current waveform. The multilayered photonic crystals of DBR PSi exhibited the reflection of a specific wavelength with high reflectivity in the optical reflectivity spectrum. In this work, we have developed a method to create refractive index in Si substrate through intensity of an electric current. The electrochemical process allows for precise control of the structural properties of DBR PSi such as thickness of the porous layer, porosity, and average pore diameter. The number of reflection peak of DBR PSi and its pore size increased as the intensity of electric current increased. This might be a demonstration for the fabrication of specific reflectors or filters.

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전기화학적 방법을 통한 금속 이중기공구조 형성 및 제어 (Formation and Control of Dual Porous Structures of Metal by an Electrochemical Method)

  • 하성혁;신헌철
    • 한국재료학회지
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    • 제29권2호
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    • pp.65-72
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    • 2019
  • Dual porous structures are observed for the first time on a metallic Cu surface underneath anodic Cu oxide by the application of an anodizing voltage to Cu in oxalic acid. The as-prepared porous Cu surface contains macropores of less than $1{\mu}m$ diameter and mesopores of about tens of nanometers diameter with circular shapes. The size and density (number of pores/area) of the macropores are dependent on the applied voltage. It is likely that the localized dissolution (corrosion) of Cu in oxalic acid under the anodizing voltages is responsible for the formation of the mesopores, and the combination of a number of the mesopores might create the macropores, especially under a relatively high anodizing voltages or a prolonged anodizing time. The variations of pore structure (especailly macropores) with applied voltage and time are reasonably explained on the basis of the proposed mechanism of pore formation.

변형에 의한 패턴변화를 활용한 음의 포아송비 다공성 구조 (Porous Structures with Negative Poisson's Ratio using Pattern Transformation Triggered by Deformation)

  • 오명훈;최명진;변태욱;조선호
    • 한국전산구조공학회논문집
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    • 제30권4호
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    • pp.275-282
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    • 2017
  • 본 논문에서는 변형에 의해 유발된 패턴변화(pattern transformation)에 기반하여 압축(compression)과 인장(tension) 하중 모두에서 음의 포아송 비(negative poisson's ratio)를 나타내는 다공성(porous) 구조를 제안한다. 기존에 개발된 원형 구멍을 이용한 구조는 연결선(ligament)의 회전 모멘트 부족으로 인해 인장 시 양의 포아송 비를 나타내는 한계점이 있었으며, 타원형 구멍을 이용한 구조는 응력집중 현상으로 인하여 내구성(durability)이 약한 문제점이 있었다. 이에 본 연구에서는 휘어진 연결선의 배열을 통하여 인장하중 하에서의 회전 모멘트를 증가시키는 동시에 응력집중 현상을 완화하고 변형에너지(strain energy)를 구조물 전반에서 고르게 흡수하도록 설계하였다. 이를 통해 10%의 공칭 변형률(nominal strain) 범위 내의 압축과 인장 모두에서 음의 포아송 비를 가지며, 기존 모델에 비하여 강성(stiffness)과 내구성이 개선된 구조를 개발하였다. 비선형 유한요소해석을 통하여 기존 타원형 구멍 모델과의 비교를 수행하였으며 제안된 모델이 구조의 강성과 내구성 측면에서 현저히 개선됨을 확인하였다.

반투명 전극으로 된 다공질 실리콘 알코올 가스 센서의 C-V 특성 (C-V Characteristics of Porous Silicon Alcohol Sensors with the Semi-transparent Electrode)

  • 김성진;이상훈
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2003년도 하계종합학술대회 논문집 II
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    • pp.1085-1088
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    • 2003
  • In this work, we fabricated a gas-sensing device based on porous silicon(PS), and its I-V and C-V properties were investigated for sensing alcohol vapor. The structure of the sensor consists of thin Au/Oxidized porous silicon/porous silicon/Silicon/Al, where the silicon substrate is etched anisotropically to be prepared into a membrane shape. As the result, I-V curves showed typical tunneling property, and C-V curves were shaped like those of a MIS (metal-insulator- semiconductor) capacitor, where the capacitance in accumulation was increased with alcohol vapor concentration.

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Wind loads for high-solidity open-frame structures

  • Amoroso, Samuel D.;Levitan, Marc L.
    • Wind and Structures
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    • 제14권1호
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    • pp.1-14
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    • 2011
  • Open frame structures, such as those commonly found in industrial process facilities, are often densely occupied with process related equipment. This paper presents a method for estimating wind loads for high-solidity open frame structures that differs from current approaches, which accumulate wind load contributions from various individual structure components. The method considers the structure as a porous block of arbitrary plan dimension that is subject to wind from any direction. The proposed method compares favorably with wind tunnel test results for similar structures. The possibility of defining an upper bound force coefficient is also discussed.

DBR 다공성 실리콘과 Host 다공성 실리콘으로 이루어진 이중 다공성 실리콘의 제조와 광학적 특성 (Preparation and Optical Characterization of DBR/Host Dual Porous Silicon Containing DBR and Host Structures)

  • 최태은;양진석;엄성용;진성훈;조보민;조성동;손홍래
    • 통합자연과학논문집
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    • 제3권2호
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    • pp.78-83
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    • 2010
  • DBR/Host dual porous silicons containing DBR and host structure were prepared and their optical properties were characterized using Ocean Optics spectrometer. In this dual porous silicon, single porous silicon layer was used as host layer for possible biomolecule and drug materials and DBR porous silicon layer was used for signal transduction due to the recognition of molecules. Optical reflection spectrum of dual porous silicon displayed only DBR reflection but Fabry-Perot fringe pattern. DBR reflection band of dual porous silicon shifted to the shorter wavelength as the etching time of host layer increased. Cross-sectional FE-SEM image of dual porous silicon displayed a thickness of about 20 micrometer for DBR porous silicon layer. Developed etching technology could be useful to prepare DBR porous silicon which exhibited specific reflection resonance at the required wavelength and to provide an label-free biosensors and drug delivery materials.

Fabrication and Characterization of Optically Encoded Porous Silicon Smart Particles

  • Sohn, Honglae
    • 통합자연과학논문집
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    • 제7권4호
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    • pp.221-226
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    • 2014
  • Optically encoded porous silicon smart particles were successfully fabricated from the free-standing porous silicon thin films using ultrasono-method. DBR PSi was prepared by an electrochemical etch of heavily doped $p^{{+}{+}}$-type silicon wafer. DBR PSi was prepared by using a periodic pseudo-square wave current. The surface-modified DBR PSi was prepared by either thermal oxidation or thermal hydrosilylation. Free-standing DBR PSi films were generated by lift-off from the silicon wafer substrate using an electropolishing current. Free-standing DBR PSi films were ultrasonicated to create DBR-structured porous smart particles. Optical characteristics of porous smart particles were measured by FT-IR spectroscopy. The surface morphology of porous smart particles was determined by FE-SEM.