• Journal of the Korean Society of Manufacturing Technology Engineers
• /
• v.6 no.3
• /
• pp.73-81
• /
• 1997

This study was to find the best adhesive condition comparing mechanical property in case of hot-melt adhesion using glue-gun, ultrasonic welding with adhesion and only ultrasonic welding in order to adhere thermoplastic resin of polyethylene (PE) in which reliable adhesion was resulted in case of ultrasonic welding with same materials of PE. The best welding condition were acquired at welding time 1 second, welding pressure 250kPa for PE-PE where welding time and welding pressure were increased in accordance with the increase of material strength. At the best ultrasonic welding conditions, bonding strength of PE-PE welding was about 21MPa of which material have tensile strength of 24MPa. Through the analysis of microscophic test for ultrasonic welding structure, it was distinguished between well welded structure with higher intermolecule flow and bad welded structure with lower flow, of which result is mostly correspond with the result of tensile strength test.

• Food Science and Biotechnology
• /
• v.14 no.3
• /
• pp.317-322
• /
• 2005

A simple and convenient method of immobilizing dextransucrase via an affinity interaction is described, along with the use of this system to synthesize leucrose. Dextransucrase was produced in sucrose-free medium by fermenting a constitutive mutant of Leuconostoc mesenteroides NRRL B-512F and was separated using an ultrafiltration membrane. The purified enzyme was free of dextran polymer, which previously was always found with the sucrose-induced enzyme. Therefore, it was possible to immobilize the enzyme on dextran-based resins using an affinity interaction. Sephadex G-200 was the best resin for immobilizing the dextransucrase and gave a fast flow rate through the packed column. The immobilized dextransucrase retained more than 80% of its specific activity after immobilization ($K_m\;=\;18.1\;mM$ and $k_{cat}\;=\;450\;sec^{-1}$ vs. 13.1 mM and $640\;sec^{-1}$, respectively, for the free enzyme). The immobilized dextransucrase showed improved stability over a pH range of 4.0 to 6.5 and at moderately high temperatures over $40^{\circ}C$. When immobilized dextransucrase was used to synthesize leucrose via the transfer reaction with sucrose and fructose, about 74% of the sucrose was converted into leucrose after one day, and the half-life of the enzyme activity was 15 days. Regeneration of the resin by supplementation with dextransucrase enabled the recovery of the initial activity of the system, but both the reaction and the flow rate were lower, probably owing to the accumulation of dextran inside the resin.

• ETRI Journal
• /
• v.35 no.6
• /
• pp.1152-1155
• /
• 2013

A cost-effective and simple solder on pad (SoP) process is proposed for a fine-pitch microbump interconnection. A novel solder bump maker (SBM) material is applied to form a 60-${\mu}m$ pitch SoP. SBM, which is composed of ternary Sn3.0Ag0.5Cu (SAC305) solder powder and a polymer resin, is a paste material used to perform a fine-pitch SoP through a screen printing method. By optimizing the volumetric ratio of the resin, deoxidizing agent, and SAC305 solder powder, the oxide layers on the solder powder and Cu pads are successfully removed during the bumping process without additional treatment or equipment. Test vehicles with a daisy chain pattern are fabricated to develop the fine-pitch SoP process and evaluate the fine-pitch interconnection. The fabricated Si chip has 6,724 bumps with a 45-${\mu}m$ diameter and 60-${\mu}m$ pitch. The chip is flip chip bonded with a Si substrate using an underfill material with fluxing features. Using the fluxing underfill material is advantageous since it eliminates the flux cleaning process and capillary flow process of the underfill. The optimized bonding process is validated through an electrical characterization of the daisy chain pattern. This work is the first report on a successful operation of a fine-pitch SoP and microbump interconnection using a screen printing process.

• Journal of the Korea Concrete Institute
• /
• v.15 no.5
• /
• pp.739-746
• /
• 2003

Various researches on the application of polymer dispersions to the cement mortar and concrete have been carried out in many countries like America, Japan and Germany and so on due to their high performance and good modification effect. PAE of polymer dispersion widely used in situ was employed that the high flowability may be induced in the cement mortar. In order to investigate the modification of cement mortar with high flowability by PAE and fracture mode of adhesive strength properties in tension of that, experimental parameters were set as PAE solid-cement ratio(P/C) and cement: fine aggregate(C:F) and the experiments such as unit weight, flow, consistency change, crack resistance and segregation that inform on the general properties have been done. Adhesion in tension is measured with a view to comprehending the properties and fracture mode in tensile load. Consistency change of cement mortar modified by PAE did grow better as the ratio of PAE solid-cement increased and was much superior to that of resin based flooring such as polyurethane and epoxy which recorded the loss of consistency in 90 min. after mixing. Adhesive strength in tension increased with continuity during curing period and showed the maximum in case of C:F=1:1 and P/C=20%.

• Membrane Journal
• /
• v.15 no.2
• /
• pp.141-146
• /
• 2005

In this study, carbon composites were prepared using carbon graphite, thermoset resin, and carbon black. Oxygen permeability was measured using the continuous flow gas permeation analyzer as a function of composition and processing conditions. The experimental results showed that the oxygen permeability increased as the carbon black content increased, whereas the oxygen permeability decreased as the pressing time increased. The oxygen permeability was not affected by the processing pressure.

• Polymer(Korea)
• /
• v.28 no.3
• /
• pp.263-272
• /
• 2004

Using computer simulation, the processibility and properties of the inst겨ment panel of automobile produced by gas injection molding were predicted and evaluated. The P-V-T data of ABS, resin were used in the gas injection molding process in order to estimate the mold filling phenomena. The optimum process conditions were found by adjusting the process parameters including pressure, filling time, the positions of gas channel and runner. The process was simplified and the final instrument panel produced by the gas injection molding was found to have improved dimension stability compared to the one produced by conventional injection molding.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2005.06a
• /
• pp.1997-2000
• /
• 2005

In this work, the effects of orthogonal ribs on warpage of plastic structure through injection molding process were investigated. Three kinds of injection molds were prepared to perform injection molding experiments of orthogonal stiffened plastic plate. The warpage of each injection molded specimen was measured using 3D CMM. And plastic injection molding analysis with commercial code was performed for the presented model. Numerical results of injection molding analysis were compared with those of experiments. It was shown that orthogonal ribs have a significant effect on the warpage of the structure in both cases of experiment and numerical analysis.

• Journal of the Korean Society for Precision Engineering
• /
• v.12 no.3
• /
• pp.110-118
• /
• 1995

The filling phase analysis of the injection molding process for thermoplastics was applied to predict pressure, themperature and shear stress in the test mold, and the results were compared with the experiment using 30% glass fiber added ABS resin. The finite difference method was used in the analysis considering the effects of heat transfer between molten polymer and mold wall, and also frictional heating by shear flow. The analysis results were considered as a method to improve the quality and the productivity of injection molding process. Using the analysis results, the molding factors such as mold-ability of polymers, performance of injection molding machine, positioning of gate and dimendsioning of runner in the injection molding process can be estimated at the design stage of mold for good quality and productivity.

• Proceedings of the KSME Conference
• /
• 2004.04a
• /
• pp.983-988
• /
• 2004

In the present study, the effects of orthogonal ribs on structural warpage during injection molding process were investigated. Basic ribbed models for the evaluation of degree of warpage were introduced and designed. Injection molds for these models are manufactured based on the full 3D CAD/CAM technology and specimens are prepared for experiment. Numerical analysis using commercial plastic injection molding analysis software was also performed to compare the results with experimental ones. The variations of materials and parameters such as injection time, mold temperature, melt temperature, holding time were considered in the present work. It was shown that orthogonal ribs have significant effect on the reduction of warpage during the injection molding process.

• Composites Research
• /
• v.20 no.1
• /
• pp.23-31
• /
• 2007

In order to improve the mechanical properties of jute fiber/polypropylene(PP) composites, the property change with the addition of a coupling agent, maleic anhydride polypropylene(MAPP) was examined experimentally. The maleated coupler acts as an intermediate to chemically connect the polar nature of the fiber and non-polar nature of the polyolefin polymer resin. Furthermore, the decrease in viscosity of the resin which results from the melting point reduction by the MAPP, leads to an increase of contact area with the fiber interface. We discussed the improvement of the PP composite blend of the maleated coupler with the 80mm jute long fiber mat in conjunction with the change of physical parameters in the thermoplastic resin. We confirmed the extent of contribution to the mechanical physical enhancement by using the following parameters: melting flow index(MI) and viscosity, contact angle, thickness of the composite, interfacial shear strength and morphology observation etc. Especially it was observed that the MI and viscosity, MAPP mixture had a very strong relationship with the tensile and flexural strength and modulus, and interfacial shear strength(IFSS).