• 제목/요약/키워드: Phase variation

검색결과 2,038건 처리시간 0.027초

플라즈마 질탄화처리된 SCM435강의 미세조직에 미치는 가스 조성의 영향 (Influence of Ambient Gas Composition on the Microstructure of Plasma Nitrocarburised SCM435 steel)

  • 이인섭
    • 한국재료학회지
    • /
    • 제12권6호
    • /
    • pp.427-430
    • /
    • 2002
  • Plasma nitrocarburizing treatment was performed for SCM 435 steel by using a plasma ion nitriding system. The effects of the variation of nitrogen and methan contents upon the hardened layer was investigated. Both the thickness of the compound layer and the amount of $\varepsilon$ phase in the compound layer increased with increasing nitrogen content. However, the thickness of the compound layer decreased due to unstable plasma for an atmosphere containing 90% $N_2$ gas content in the gas mixture. The amount of $\varepsilon$phase in the compound layer increased with increasing $CH_4$ gas content. For $CH_4$ gas content more than 2% in the gas mixture, the thickness of the compound layer decreased due to the formation of $\theta$ phase.

Vapor Phase Mercury Removal by Sulfur Impregnated Activated Carbons and Sulfur Impregnation Protocol

  • Lee, Si-Hyun;Cha, Sun-Young;Park, Yeong-Seong
    • Carbon letters
    • /
    • 제2권1호
    • /
    • pp.37-43
    • /
    • 2001
  • Mercury has been identified as a potential health and environmental hazardous material. Activated carbon adsorption offers promising potential for the control of mercury emissions, and sulfur impregnated (sulfurized) activated carbons has been shown to be an effective sorbent for the removal of vapor phase $Hg{\circ}$ from sources. In this work, vapor phase mercury adsorption by sulfur impregnated activated carbons were investigated. Sulfur impregnated activated carbons were made by variation of impregnation temperature, and the comparison of adsorption characteristics with commercial virgin and sulfurized carbons were made. Factors affecting the adsorption capacity of virgin and sulfurized activated carbons such as pore characteristics, functional groups and sulfur impregnation conditions were discussed. It was found that the sulfur allotropes plays a critical role in adsorption of mercury vapor by sulfurized activated carbons.

  • PDF

On-line Trace Enrichment for the Determination of Insulin in Biological Samples Using Reversed-Phase High Performance Liquid Chromatography with Column Switching

  • Lee, Jung-Sook;Lee, Heeyong;Lee, Hye-Suk;Lee, Kang-Choon
    • Archives of Pharmacal Research
    • /
    • 제17권5호
    • /
    • pp.360-363
    • /
    • 1994
  • Column--swtiching technique with a reversed-phase high performance liquid chromatographic method has been developed for the routine analysis of radioiodinated insulin and its degadation products in biological fluids. The diluted biological samples were loaded onto a precolumn packed with LiChrosorb RP-8 $(25-40{\;}{\mu}m)$ using 0.1% trifuoroacetic acid (TFA) in water as a washing solvent. After valve switching, the concentrated insulins were eluted in the back-flush mode and separated by a W-Porex $C_{18}$ column with a gradient of 0.1% TFA in water and 0.1% TFA in acetonitrile as the mobile phase. The method showed good precision, accuracy and speed with the detection limit of 20 pg/ml. Total analysis time per sample was about 40 min and the coefficients of variation were less than 8, 2%.

  • PDF

Pyrochlore상의 부피분율에 따른 PMN-Pyrochlore 2상 혼합체의 유전율변화;General Effective Media식의 적용 (Variation of Dielectric Constant with the Volume Fraction of Pyrochlore Phae in the PMN-Polychlore Diphasic System ; Application of General Effective Media Equation)

  • 허강일;김정주;김남경;김진호;조상희
    • 한국세라믹학회지
    • /
    • 제30권1호
    • /
    • pp.78-84
    • /
    • 1993
  • In PMN-pyrochlore phase mixtures, dielectric constant was measured as a function of the volume fraction of pyrochlore phase and considered with general effective media(GEM) equation. For the application of GEM equation to this system, the critical volume fraction(Vc) where connectivity between the perovskite PMN and pyrochlore phase changed from 0-3 to 3-3, was determined based on the each particle size ratio of two phases with microstructural observation. And then the t value was determined from modified percolation powder-law dependence ( K-Kc (V-Vc)t). In the case of applying such values of t and Vc to the GEM equation, which provided a reasonable fit to the measured dielectric constant within the experimental error range.

  • PDF

Phase-Locked Loop with Leakage and Power/Ground Noise Compensation in 32nm Technology

  • Kim, Kyung-Ki;Kim, Yong-Bin;Lee, Young-Jun
    • JSTS:Journal of Semiconductor Technology and Science
    • /
    • 제7권4호
    • /
    • pp.241-246
    • /
    • 2007
  • This paper presents two novel compensation circuits for leakage current and power supply noise (PSN) in phase locked loop (PLL) using a nanometer CMOS technology. The leakage compensation circuit reduces the leakage current of the charge pump circuit and the PSN compensation circuit decreases the effect of power supply variation on the output frequency of VCO. The PLL design is based on a 32nm predictive CMOS technology and uses a 0.9 V power supply voltage. The simulation results show that the proposed PLL achieves 88% jitter reduction at 440 MHz output frequency compared to the PLL without leakage compensator and its output frequency drift is little to 20% power supply voltage variations. The PLL has an output frequency range of 40 $M{\sim}725$ MHz with a multiplication range of 1-1023, and the RMS and peak-to-peak jitter are 5psec and 42.7 psec, respectively.

DP-PLL의 Holdover 모드에 대한 OCXO의 주파수 모델 (A Frequency Model of OCXO for Holdover Mode of DP-PLL)

  • 한욱;황진권;김영권
    • 전기전자학회논문지
    • /
    • 제4권2호
    • /
    • pp.266-273
    • /
    • 2000
  • OCXO (Oven Controlled X-tal Oscillator)의 주파수 모델이 holdover 알고리즘을 DP-PLL (Digital Processing-Phase Locked Loop) 시스템에 적용하기 위해 제안되었다. 이 모델은 온도와 OCXO의 노화에 따라 2차 다항식으로 간단하게 표현된다. 모델 변수들은 LSM (Least Squared Method)을 적용한 실험 데이터로부터 얻어진다. holdover 알고리즘은 다른 실험 데이터를 사용한 동일한 모델로 모의실험 할 수 있다.

  • PDF

단상 유도전동기의 고정자 동손 최소화를 위한 설계 방법 (Design Methodology for Minimal Stator Copper Loss in A Single-phase Induction Motor)

  • 백수황;김병택;권병일
    • 전기학회논문지
    • /
    • 제57권9호
    • /
    • pp.1536-1545
    • /
    • 2008
  • In this paper, we research a new method for efficiency improvement of a single-phase Induction motor by minimization of the stator loss. To make this, we perform winding design which is based on balanced and quasi-balanced operation condition. It gives efficiency improvement greatly but poor starting torque simultaneously. To obtain the best efficiency improvement maintaining the maximum and starting torque, the optimal winding specification and rotor dimension is determined with variation of secondary resistance, running capacitor and turn ratio. Finally, this paper gives the comparison between the simulation results and experimental results.

Control Method for Reducing the THD of Grid Current of Three-Phase Grid-Connected Inverters Under Distorted Grid Voltages

  • Tran, Thanh-Vu;Chun, Tae-Won;Lee, Hong-Hee;Kim, Heung-Geun;Nho, Eui-Cheol
    • Journal of Power Electronics
    • /
    • 제13권4호
    • /
    • pp.712-718
    • /
    • 2013
  • This paper proposes a control method for reducing the total harmonic distortion (THD) of the grid current of three-phase grid-connected inverter systems when the grid voltage is distorted. The THD of the grid current caused by grid voltage harmonics is derived by considering the phase delay and magnitude attenuation due to the hardware low-pass filter (LPF). The Cauchy-Schwarz inequality theory is used in order to search more easily for the minimum point of the THD. Both the gain and angle of the compensation voltage at the minimum point of the THD of the grid current are derived with the variation of cut-off frequencies of the hardware LPF. Simulation and experimental results show the validity of the proposed control methods.

반응표면법과 유한요소법을 이용한 단상 스위치드 릴럭턴스 전동기의 최적 설계 (Single Phase Switched Reluctance Motor Optimum Design Using Response Surface Methodology and Finite Element Method)

  • 임승빈;최재학;박재범;손영규;이주
    • 대한전기학회논문지:전기기기및에너지변환시스템부문B
    • /
    • 제55권12호
    • /
    • pp.596-607
    • /
    • 2006
  • This paper presents Single Phase Switched Reluctance Motor (SPSRM) optimum design for vacuum cleaners using Response Surface Methodology (RSM) to determine geometric parameters, and the 2-D Finite Element Method (FEM) has been coupled with the circuit equations of the driving converter. Additionally, an optimum process for SPSRM has been proposed and peformed with geometric and electric parameters thereby influencing the inductance variation and effective torque generation as design variables. SPSRM performances have also been analyzed to determine an optimal design model for maximized efficiency at high power factor. In order to confirm the propriety of the Finite Element Method and motor performance calculation, simulation waveform and experiment waveform for motor voltage and current were compared.

동시 증착으로 제작한 BSCCO 박막의 초전도 특성 (Superconducting Characteristics of BSCCO Thin Film Fabricated by Co-deposition)

  • 이희갑;이준웅;박용필
    • 대한전기학회:학술대회논문집
    • /
    • 대한전기학회 1999년도 추계학술대회 논문집 학회본부 C
    • /
    • pp.929-931
    • /
    • 1999
  • BSCCO thin films have been fabricated by co-deposition at an ultralow growth rate using ion beam sputtering(IBS) method. Bi 2212 phase appeared in the temperature range of 750 and $795^{\circ}C$ and single phase of Bi 2201 existed in the lower region than $785^{\circ}C$. Whereas, ozone gas pressure dependance on structural formation was scarcely observed regardless of the pressure variation. And high quality of c-axis oriented Bi 2212 thin film with $T_c$(onset) of about 90 K and $T_c$(zero) of about 45 K is obtained. Only a small amount of CuO in some films was observed as impurity, and no impurity phase such as $CaCuO_2$ was observed in all of the obtained films.

  • PDF