• Title/Summary/Keyword: Particle size measurement

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Age-Hardening Behavior of SiCp Reinforced 6061 Aluminum Alloy Composites (SiCp/6061Al합금복합재료의 시효거동)

  • An, Haeng-Geun;Yu, Jeong-Hui;Kim, Seok-Won;U, Gi-Do
    • Korean Journal of Materials Research
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    • v.10 no.12
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    • pp.793-798
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    • 2000
  • The age-hardening behavior of unreinforced 6061 Al alloy and SiCp/6061 Al alloy composites reinforced with different size of SiC particle (average diameter ; 0.7$\mu\textrm{m}$ and 7.0$\mu\textrm{m}$) was investigated by hardness measurement, calorimetric technique and transmission electron microscopy. At 17$0^{\circ}C$ isothermal aging treatment, the peak aging time of 0.7$\mu\textrm{m}$SiCp/6061Al alloy composite and 7.0$\mu\textrm{m}$SiCp/6061Al alloy composite is shorter than that of unreinforced 6061Al alloy, and the aging of 7.0$\mu\textrm{m}$SiCp/6061Al alloy composite is accelerated more than that of 0.7$\mu\textrm{m}$SiCp/6061Al alloy composite. This acceleration is due to the increase of dislocation density by the compositeness with SiCp and the SiC particle size. In the peak aged condition, the major strengthening phase of these materials is intermediate $\beta$ phase(Mg$_2$Si), and the activation energy for the formation of $\beta$ phase is considerably decreased by the compositeness with SiCp and the increasing of SiC Particle site.

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A study on the characteristics of fuel performance according to the oxygenated additive type for gasoline fuel Part 2. Exhaust and Non-regulated, PM emission characteristics (휘발유 연료용 함산소 첨가제 종류에 따른 성능 특성 연구 Part 2. 배출가스 및 미규제 물질, 입자상 물질 특성)

  • Lee, Min-Ho;Kim, Ki-Ho;Ha, Jong-Han
    • Journal of the Korean Applied Science and Technology
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    • v.33 no.2
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    • pp.374-384
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    • 2016
  • Concern about air pollution is gradually rising up in domestic and foreign, automotive and fuel researchers are trying to reduce vehicle exhaust emissions, through a lot of approaches, which consist of new engine design and innovative after-treatment systems, using clean (eco-friendly alternative) fuels and fuel quality improvement. This research is proceeding by two main issues : exhaust emissions and PM particle emissions of gasoline vehicle. Exhaust emissions, non-regulated emissions and PM (particulate matter) particles of automotive are causing many problems which ambient pollution and harmful effects on the human body. The main particulate fraction of automotive exhaust emissions consists of small particles. Because of their small size, inhaled particles can easily penetrate deep into the lungs. The rough surfaces of these particles make it easier for them to combine with other toxins in the environment. Thus, the hazards of particle inhalation are increased. Based on the oxygenated fuel additive types (MTBE, Bio-ETBE, Bio-ethanol, Bio-butanol), this paper discussed the influence of oxygen contents on gasoline vehicle exhaust emissions, non-regulated emissions and nano-particle emissions. Also, this paper assessed exhaust emission characteristics at 2 type test modes. The test modes were FTP-75 and HWFET. All measurement items be verified less than the value of regulated emissions. It could be known difference increase and decrease by each measurement item depending on increase the oxygen contents.

Screen-printed carbonaceous matrrials for photocapacitor electrode (스크린 프린터에 의한 광캐패시터용 카본 전극 제작)

  • Choi, Woo-Jin;Kwak, Dong-Joo;Sung, Youl-Moon;Ha, Soon-Ho
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2009.10a
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    • pp.411-414
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    • 2009
  • Photo-capacitor electrodes are attracting great attention because of their high capacitance and potential applications in electronic devices. Carbon capacitor, active carbon capacitor and its combination will be fabricated using simple sandwich capacitor electrode method as carbonaceous material on each type of capacitor electrodes with 20 ${\times}$ 15 mm cell size. Carbon/active carbon cell was fabricated using sol-gel process with 120oC dry temperature in l hour and using sintering process with 500oC in 2 hour. The effect of sintering temperature on carbon properties was also investigated with X-ray diffraction technique to get the best sintering temperature. The detail of fabrication process will be explained. Elemental composition in electrode material can be measured using quantitative spectroscopic as and a cyclic voltammetric technique was used to study the combined effects of electrode material and effect of annealing temperature and also time on the capacitance of thermally treated in capacitor electrode. In this work, characterization impedance technique is used to measurement of capacitance and giving complementary results. Active carbon as carbonaceous material has a better capacitance in charge/discharge process with mean thickness $32{\mu}m$ and with particle size $1{\mu}m$ to $4.5{\mu}m$ in 20 ${\times}$ 15 mm sample size of capacitor electrode.

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The Preparation of Copper Powder Using Solvothermal Process and Its Application as EMI Shielding Agent (솔보써말 방법을 이용한 구리분말 제조 및 전자파 차폐제로의 응용)

  • Lee, Hyo-Won;Kim, Soo-Ryong;Kwon, Woo-Teck;Choi, Duck-Kyun;Kim, Young-Hee
    • Korean Journal of Materials Research
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    • v.16 no.5
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    • pp.285-291
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    • 2006
  • Copper powders have been widely used in electrically conductive coatings, electrode materials et al. and are very prospective since they are cheaper than noble metal powders such as silver or palladium. In this study, copper powders for metal filler of EMI shielding have been prepared using a solvothermal process from $CuSO_4$, NaOH, Glucose, mixed solvent ($H_2O$: Ethanol) and hydrazine which was used as a reducing agent at various reaction conditions. The prepared copper powders showed finely dispersed spherical shape without agglomerate, uniform morphology, narrow size distribution, high purity and were about 400-700 nm in size. The prepared powders were characterized using XRD, SEM, TGA, XPS, particle size measurement and EMI shielding efficiency.

Influence of Precursor on the Electrochemical Properties of Li(Ni0.5Co0.2Mn0.3)O2 Cathode for the Lithium Secondary Battery (전구체의 물성에 따른 리튬 2차전지용 Li(Ni0.5Co0.2Mn0.3)O2의 전기화학적 특성 변화)

  • Kang, Donghyun;Arailym, Nurpeissova;Chae, Jeong Eun;Kim, Sung-Soo
    • Journal of the Korean Electrochemical Society
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    • v.16 no.4
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    • pp.191-197
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    • 2013
  • The one of the cathode material, $Li(Ni_{0.5}Co_{0.2}Mn_{0.3})O_2$, was synthesized by the precursor, $Ni_{0.5}Co_{0.2}Mn_{0.3}(OH)_2$, from the co-precipitation method and the morphologies of the primary particle of precursors were flake and needle-shape by controlling the precipitation parameters. Identical powder properties, such as particle size, tap density, chemical composition, were obtained by same process of lithiation and heat-treatment. The relation between electrochemical performances of $Li(Ni_{0.5}Co_{0.2}Mn_{0.3})O_2$ and the primary particle morphology of precursors was analyzed by SEM, XRD and EELS. In the $Li(Ni_{0.5}Co_{0.2}Mn_{0.3})O_2$ cathode from the needle-shape precursor, the primary particle size was smaller than that from flake-shape precursor and high Li concentration at grain edge comparing grain center. The cycle and rate performances of the cathode from needle-shape precursor shows superior to those from flake-shape precursor, which might be attributed to low charge-transfer resistance by impedance measurement.

Stabilization of Nanoemulsion Using PEG-free Surfactant (PEG-free 계면활성제를 사용한 Nanoemulsion의 안정화)

  • Kim, Huiju;Jung, Taek Kyu;Kim, Ja Young;Yoon, Kyung-Sup
    • Journal of the Korean Applied Science and Technology
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    • v.36 no.2
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    • pp.434-447
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    • 2019
  • Polyethylene glycol (PEG) is widely used in cosmetics as a surfactant, detergent and emulsifier. During the manufacturing process, 1,4-dioxane, which is toxic to humans, can be produced as a by-product by dimerization of ethylene oxide. As consumers' interest in cosmetic ingredients has increased, the need for safe emulsion research without PEG ingredients in the personal care market has increased. With increasing consumer interest in cosmetic ingredients, the need for safer emulsion research without the PEG ingredient in the personal care market has increased. In this study, we aimed to develop and stabilize nanoemulsion formulation without PEG. Response Surface Methodology (RSM) was used to develop optimized nanoemulsion formulations. Surfactant content (2~4%), oil content (4~8%) and polyol content (12~24%) were set as independent variables as a result of preliminary experiments for determining independent variables and ranges. The particle size, zeta potential, turbidity, and polydispersity index of the formulation were measured as response variables. As a result of measurement of the prepared nanoemulsion by FIB (Focused ion beam), spherical particles were found to have a size distribution of 100 to 200 nm. The stability of each formulation was evaluated for 30 days at each temperature ($4^{\circ}C$, $25^{\circ}C$, and $45^{\circ}C$). The optimal formulation considering the optimum particle size, turbidity, polydispersity index and zeta potential was found to be surfactant (2%), oil (8%) and polyol (24%).

A Study on the Statistical Analysis of the Flow Characteristics of Droplet in the Cross Region of Twin Spray (이중분무 교차지역에서의 액적유동특성의 통계학적 분석에 관한 연구)

  • 조대진;윤석주;최태민
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.3
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    • pp.635-644
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    • 1994
  • This study investigated mainly on the flow characteristics of a droplet in the cross region of twin spray. The velocities of the droplet were measured along the axial and radial direction, and the flow characteristics of the droplet were statistically analyzed. For the statistical analysis, the probability density of the turbulent components has been studied, and then the Reynolds shear stress, the skewness and the flatness factors were calculated, and compared with the Gaussian value. Two pressure swirl stomizers were used for the twin spray system and kerosene was employed as the working liquid. 2-D PDA(particle dynamic analyzer) was used for the purpose of the measurement of droplet size and velocities. As a result, it was found that (1) the droplets collision was taken place strongly in the cross region. So, a large momentum loss of droplets due to the loss of natural movement direction was occurred, and momentum loss of radial direction was greater than that of axial direction. (2) The axial direction skewness factor approached to zero like the Gaussian distribution in the cross region of twin spray. (3) In the cross region of twin spray, the fluctuation instability of droplet was increased because of the development of the turbulence characteristics due to the droplet collision.

CFD-DEM modeling of snowdrifts on stepped flat roofs

  • Zhao, Lei;Yu, Zhixiang;Zhu, Fu;Qi, Xin;Zhao, Shichun
    • Wind and Structures
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    • v.23 no.6
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    • pp.523-542
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    • 2016
  • Snowdrift formation on roofs should be considered in snowy and windy areas to ensure the safety of buildings. Presently, the prediction of snowdrifts on roofs relies heavily on field measurements, wind tunnel tests and numerical simulations. In this paper, a new snowdrift modeling method by using CFD (Computational Fluid Dynamics) coupled with DEM (Discrete Element Method) is presented, including material parameters and particle size, collision parameters, particle numbers and input modes, boundary conditions of CFD, simulation time and inlet velocity, and coupling calculation process. Not only is the two-way coupling between wind and snow particles which includes the transient changes in snow surface topography, but also the cohesion and collision between snow particles are taken into account. The numerical method is applied to simulate the snowdrift on a typical stepped flat roof. The feasibility of using coupled CFD with DEM to study snowdrift is verified by comparing the simulation results with field measurement results on the snow depth distribution of the lower roof.

Development of a High Resolution Digital Cinematic Particle Image Velocimetry (고해상도 Cinematic PIV의 개발)

  • Park, Gyeong-Hyeon;Kim, Gyeong-Cheon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.11
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    • pp.1535-1542
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    • 2001
  • A high resolution digital cinematic Particle Image Velocimetry(PIV) has been developed. The system consists of a high speed CCD camera, a continuous Ar-ion laser and a computer with camera controller. To improve the spatial resolution, we adopt a Recursive Technique for velocity interrogation. At first, we obtain a velocity vector fur a larger interrogation window size based on the conventional two-frame cross-correlation PIV analysis using the FFT algorithm. Based on the knowing velocity information, more spatially resolved velocity vectors are obtained in the next iteration step with smaller interrogation windows. When the correct velocity vector at the first step is found to be critical, a Multiple Correlation Validation(MCV) technique is applied to decrease the spurious vectors. The MCV technique turns out to improve SNR(Signal to Noise Ratio) of the correlation table. The developed cinematic PIV method has been applied to the measurement of the unsteady flow characteristics of a Rushton turbine mixer. A total of 3,245 instantaneous velocity vectors were successfully obtained with 4 ms time resolution. The acquired spatial resolution corresponds to the conventional high resolution digital PIV system using a 1K ${\times}$ 1K CCD camera.

Characteristics of Polycyclic Aromatic Hydrocarbons in Ambient Air in Jeonju between July and November in 2002 (2002년 6월부터 11월까지 전주지역 대기 중 다환방향족 탄화수소의 특성)

  • Kim Hyoung-Seop;Ghim Young-Sung;Kim Jong-Guk
    • Journal of Korean Society for Atmospheric Environment
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    • v.22 no.4
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    • pp.499-508
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    • 2006
  • Atmospheric concentrations of polycyclic aromatic hydrocarbons (PAHs) were measured at the Chonbuk National University located in Jeonju, four times between June and November 2002, each time for five days. Twenty-four compounds including five alkyl PAHs and byphenyl were analyzed. Average total concentration of 24 PAHs was 85 $\pm$ 15 ng/$m^3$ and about 94% of PAHs existed in the gas phase. On an average, naphthalene accounted for about 30% of the total PAHs concentration. The gas/particle partitioning was not much varied during the measurement period. High molecular weight PAHs with five and six rings were primarily associated with fine particles less than 1 $\mu$m. Lower molecular weight PAHs were evenly distributed in fine and coarse particles so that their distribution was similar to that of TSP.