• 제목/요약/키워드: Pak1

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HPLC를 이용한 식품중 식용타르색소 8종의 동시분석 (Simultaneous Analytical Techniques for Determination of 8 Synthetic Food Colors in Foods by HPLC)

  • 박성관;이창희;박재석;윤혜정;김소희;홍연;이종옥;이철원
    • 분석과학
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    • 제13권3호
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    • pp.378-384
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    • 2000
  • 8종 합성착색료의 동시정성 정량법을 확립하기 위하여 고속액체크로마토그래프(HPLC)를 이용한 분석법에 관한 연구를 수행하였다. 식품에 첨가된 타르색소는 물 또는 에탄올의 혼합액으로 추출하여 진한염산으로 0.5% 염산농도가 되도록 조정하여 시료액으로 하였다. 이를 Sep-pak $C_{18}$으로 정제한 후 HPLC를 이용하여 254nm 및 각 색소별 최대흡수파장에서 정성 정량분석을 실시하였다. 식품별 회수율은 각각 청량음료 81.2-98.0%, 사탕 80.6-96.1%, 껌 79.8-96.3%, 과자 76.5-91.7%, 아이스크림 79.9-93.8%, 젤리 78.6-94.7% 이었다. 색소별 검출한계는 식용색소 청색제1호(B1) 청색제2호(B2), 녹색제3호(G3)는 $0.05{\mu}g/g$, 식용색소 황색제4호(Y4), 황색제5호(Y5), 적색제2호(R2), 적색제3호(R3), 적색제40호(R40)는 $0.10{\mu}g/g$이었다.

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동양의 율관에 관한 연구(II) -낙학궤범』소재 율장의 문제점 및 율산에 관한 연구- (Study on the ength of the Pitch Pipes Preserved in Korean Sources)

  • 남상숙
    • 한국수학사학회지
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    • 제5권1호
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    • pp.81-95
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    • 1988
  • In Akhakkyebom(낙학궤범), one of the greatest Korean Sources, a great mistake was found in the lengths of the pitch pipes. Whanjong(황종) from which the other eleven pitches are calculated, is nine inches by decimal system. But the rest are from 9inches by nonary system. To find out how such a contradictory combination could put into so great a book, all the sources available wereexamined. In the process of investigating the numeral change of the lengths of the pitchpipes, it was found that fixation of this contradictory combination was due to the tradiction of Confucianism, which is specialized by its adherence of the old. SongHyon(성현) couldn't understand well enough Tsai Yuan-ting's(몽원정) Account of the science of the pitch pipes in Lu-luhsin-shui(율여신서), Neither could Yi Hye-gu(이혜구) who translated Akhakkwebom(낙학궤범) into Korean. The parts they misunderstood were pointed out and explained as it should be in this thesis. Several other accounts of the science of the pitch pipes like Chu Tsai-yu's and Jing Farng's are also explained. The Pitch-pipes which were said to have been made by Pak Yon(박연) were found out to be of Chu Tsai-yu's. Those which Yi Sang dok(이상덕) wrote were one of Pak Yon's achievements turned out to be of Tsai Yuen-ting's(몽원정), And othe interesting mistakes were pointed out in thesis thesis. Most of these mistakes were made, I think, because of the lack of the study on the historical background. That's why I tried to examine all the sources available on pitch-pipes. In the lengths of the pitch-pipes preserved in Shih-chi(사기) by Ssu-ma Ch'ien(사마천), several letters were found to have been misprinted. Some 칠's should be “십” and the letter “일” in Hyopchong(황종) should be “칠”. I couldn't deal with all the lengths of the pitch-pipes in this thesis. Especially the real length of the old measure of Whangjong(황종) made by PakYon(박연) is remained still unknown. I believe a lot more study should be poured on this field to know our traditional music as it was.

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미국의 온라인 식료품 쇼핑에 관한 소고 (Online Grocery Shopping: Is there a Phoenix?)

  • 박명섭;박인섭
    • 수산경영론집
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    • 제37권1호
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    • pp.111-120
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    • 2006
  • 식품관련 시장조사 기관인 Food marketing Instittue에 따르면, 미국전체의 식료품체인 가운데 25%가 최소한 온라인 쇼핑을 운영하고 있다. Safeway, Albertsons 등 대형 수퍼마켓 체인들이 연이어 온라인 시장에 참가했고, Melon Seed, FreshDirect.com 등 신규업체도 참가했다. 2002년 5월 Safeway.cm을 설립한 Safeway는 동년 7월에 8번째 점포를 시애틀에 오픈하는 등, 온라인 비즈니스를 확대했다. 최근 할인매장, 드러그 스토어 둥에 일부 시장을 잠식당하고 있는 이들 전통적인 수퍼마켓 체인들은 고객의 이탈을 막기 위해 비록 소수이기는 하지만 고객의 온라인 수요에 대응할 필요성이 있다고 생각하기 때문이다. 본고의 목적은 미국의 식료품 온라인 쇼핑에서 발생하고 있는 여러 문제점을 지적하는 것이다. Webvan이 Dot Com의 실패를 예증하는데 사용되는 주요한 전자상거래 비즈니스이다. 오늘날 온라인 쇼핑 비즈니스의 도전을 보여주고 이익을 낳기 위해 취해야 할 조치를 논의하기 위해 온라인 쇼핑 밴더가 참조되고 있다. 또한 본고는 미국의 Vons.com, Peapod.com 그리고 Safeway.com과 같은 온라인 식료품 쇼핑 비즈니스에서 나타나고 있는 추세, 신규 영업자 및 잔존 영업자들의 특성과 온라인 식료품 쇼핑업자들의 성장에 필요한 요인들에 관해서도 논하였다.

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Development Process for Slit Mask Exchanger Mechanism Prototype (SMEM-P) of the Giant Magellan Telescope Multi-object Astronomical and cosmological Spectrograph (GMACS)

  • Lee, Hye-In;Cook, Erika;Ji, Tae-Geun;Byeon, Seoyeon;Pak, Suehee;Cynthia, Froning;Marshall, Jennifer;Depoy, Darren L.;Pak, Soojong
    • 천문학회보
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    • 제43권1호
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    • pp.68.4-69
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    • 2018
  • GMACS is one of the instruments for the Giant Magellan Telescope (GMT) which will provide wide field, multi-object, moderate resolution spectroscopy of faint targets. KHU (Kyung Hee University) is in charge of control software of GMACS. As a first step, the Slit Mask Exchange Mechanism Prototype (SMEM-P) will be used as a preliminary example to make development process between electronics and high level software. Recently, we have developed a sample program to communicate with low level devices via EtherCAT. It is expected to be a mockup design for software and control system of GMACS. In this poster, we show the development process and test operation results of control software for SMEM-P.

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고속액체크로마토그래피를 이용한 사람 혈장중 메비놀린 산의 정량 (Quantitation of Mevinolinic Acid in Human Plasma by HPLC)

  • 오한석;박동영;서성훈;김영관;홍선표;최영욱;이경태
    • Journal of Pharmaceutical Investigation
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    • 제30권4호
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    • pp.279-282
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    • 2000
  • Simple and precise high-performance liquid chromatographic (HPLC) assay was developed and validated for the determination of a HMG-CoA reductase inhibitor, $lovastatin^{TM}$ and its active metabolite (mevinolinic acid) in human plasma. The method involved solid phase extraction of mevinolinic acid and internal standard using Sep-Pak Cartridge. Samples were analyzed by reversed-phase HPLC using $Capcell-Pak\;C_{18}$ column with ultraviolet detection at 238 nm. The quantitation limit of mevinolinic acid was 2 ng/ml and the calibration curve was linear over the range of 2-50 ng/ml $(r^2>0.999)$ with human plasma. The analyses of quality control samples indicated that the normal values could be predicted with an accuracy >97%. The intra- and inter-day coefficients of variation for the analyses were <10%. The average recoveries were similar (79%) for mevinolinic acid and methylmevinolinic acid. The method described has been successfully applied to the quantification of mevinolinic acid in about 1,000 human plasma samples over six-month period.

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REAL HYPERSURFACES IN COMPLEX TWO-PLANE GRASSMANNIANS WHOSE SHAPE OPERATOR IS OF CODAZZI TYPE IN GENERALIZED TANAKA-WEBSTER CONNECTION

  • Cho, Kyusuk;Lee, Hyunjin;Pak, Eunmi
    • 대한수학회보
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    • 제52권1호
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    • pp.57-68
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    • 2015
  • In this paper, we give a non-existence theorem of Hopf hypersurfaces in complex two-plane Grassmannians $G_2(\mathbb{C}^{m+2})$, $m{\geq}3$, whose shape operator is of Codazzi type in generalized Tanaka-Webster connection $\hat{\nabla}^{(k)}$.

HOLOMORPHIC SECTIONAL CURVATURE OF THE TANGENT BUNDLE$^*$

  • Pak, Jin-Suk;Pahk, Yoi-Sook;Kwon, Jung-Hwan
    • 대한수학회보
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    • 제32권1호
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    • pp.13-18
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    • 1995
  • In order to investigate the differential structure of a Riemannian manifold (M, g), it seems a powerful tool to study the differential structure of its tangent bundle TM. In this point of view, K. Aso [1] studied, using the Sasaki metric $\tilde{g}$, the relation between the curvature tensor on (M, g) and that on (TM, $\tilde{g}$).

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전자현미경(電子顯微鏡) 건판(乾板)의 제작(製作) 및 그 특성(特性) 조사(調査) 연구(硏究) (Study on the emulsion and its physical properties)

  • 김현창;박규은
    • Applied Microscopy
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    • 제1권1호
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    • pp.3-10
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    • 1969
  • By the use of electron microscope, the study has beek made on the grain size in photo graphic emulsions, which are made at different temperature. It is found that ,the optimum temperature is $60^{\circ}C$, at which the average grain size obtained is the biggest. Also electron micrographs show NaCl-type crystal structure of AgBr and AgCl, as we expected.

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