• 한국초전도ㆍ저온공학회논문지
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• 제14권4호
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• pp.28-31
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• 2012

We report the solid-liquid phase equilibria on the $GdBa_2Cu_3O_{7-{\delta}}$ (GdBCO) stability phase diagram in low oxygen pressures ($PO_2$) ranging from 1 to 100 mTorr. On the basis of the GdBCO stability phase diagram experimentally determined in low oxygen pressures, the isothermal sections of three different phase fields on log $PO_2$ vs. 1/T diagram were schematically constructed within the $Gd_2O_3-Ba_2CuO_y-Cu_2O$ ternary system, and the solid-liquid phase equilibria in each phase field were described. The invariant points on the phase boundaries include the following three reactions; a pseudobinary peritectic reaction of $GdBCO{\leftrightarrow}Gd_2O_3$ + liquid ($L_1$), a ternary peritectic reaction of $GdBCO{\leftrightarrow}Gd_2O_3+GdBa_6Cu_3O_y$ + liquid ($L_2$), and a monotectic reaction of $L_1{\leftrightarrow}GdBa_6Cu_3O_y+L_2$. A conspicuous feature of the solid-liquid phase equilibria in low $PO_2$ regime (1 - 100 mTorr) is that the GdBCO phase is decomposed into $Gd_2O_3+L_1$ or $Gd_2O_3+GdBa_6Cu_3O_y+L_2$ rather than $Gd_2BaCuO_5+L$ well-known in high $PO_2$ like air.

• ETRI Journal
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• 제25권1호
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• pp.19-24
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• 2003

This paper describes the performance of a Ku-band 5-bit monolithic phase shifter with metal semiconductor field effect transistor (MESFET) switches and the implementation of a ceramic packaged phase shifter for phase array antennas. Using compensation resistors reduced the insertion loss variation of the phase shifter. Measurement of the 5-bit phase shifter with a monolithic microwave integrated circuit demonstrated a phase error of less than $7.5{\circ}$ root-mean-square (RMS) and an insertion loss variation of less than 0.9 dB RMS for 13 to 15 GHz. For all 32 states of the developed 5-bit phase shifter, the insertion losses were $8.2{\pm}1.4$dB, the input return losses were higher than 7.7 dB, and the output return losses were higher than 6.8 dB for 13 to 15 GHz. The chip size of the 5- bit monolithic phase shifter with a digital circuit for controlling all five bits was 2.35 mm ${\times}$1.65 mm. The packaged phase shifter demonstrated a phase error of less than $11.3{\circ}$ RMS, measured insertion losses of 12.2 ${\pm}$2.2 dB, and an insertion loss variation of 1.0 dB RMS for 13 to 15 GHz. For all 32 states, the input return losses were higher than 5.0 dB and the output return losses were higher than 6.2 dB for 13 to 15 GHz. The size of the packaged phase shifter was 7.20 mm${\times}$ 6.20 mm.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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• pp.222.2-222.2
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• 2015

A $Ge_2Sb_2Te_5$ nanowire (GST NW) phase change memory device is investigated with Joule heating electrodes. GST is the most promising phase change materials, thus has been studied for decades but atomic structure transition in the phase-change area of single crystalline phase-change material has not been clearly investigated. We fabricated a phase change memory (PCM) device consisting of GST NWs connected with WN electrodes. The GST NW has switching performance with the reset/set resistance ratio above $10^3$. We directly observed the changes in atomic structure between the ordered hexagonal close packed (HCP) structure and disordered amorphous phase of a reset-stop GST NW with cross-sectional STEM analysis. Amorphous areas are detected at the center of NW and side areas adjacent to heating electrodes. Direct imaging of phase change area verified the atomic structure transition from the migration and disordering of Ge and Sb atoms. Even with the repeated phase transitions, periodic arrangement of Te atoms is not significantly changed, thus acting as a template for recrystallization. This result provides a novel understanding on the phase-change mechanism in single crystalline phase-change materials.

• Journal of Microbiology and Biotechnology
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• 제2권2호
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• pp.135-140
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• 1992

The partitioning of recombinant human interleukin-2(rhII-2) in PEG 8000-dextran 38800 aqueous two-phase system has been investigated using three different sources of rhIL-2. In the case of pure rhIL-2, the solubility in a PEG-dextran two-phase system was low and most of rhIL-2 was partitioned into the bottom phase. For the recovery of rhIL-2 from insoluble protein aggregates, the inclusion bodies of recombinant E. coli were solubilized by the treatment with sodium dodecyl sulfate (SDS). The addition of SDS significantly enhanced not only the solubility of rhIL-2 but also the partitioning of rhIL-2 to the top phase. When the ratio of SDS to rhIL-2 was 2.0, the partition coefficient(K) and the recovery yield(Y) at the top phase were 4.5 and 88%, respectively, at pH 6.8. In order to reduce the recovery steps further, SDS was directly added to the intact recombinant E. coli cells and then partitioned into the PEG/dextran aqueous two-phase system. The observed partition coefficient ($K{\cong{3.0$) and recovery yield ($Y{\geq}80%$ )of this method were comparable to the rhIL-2 recovery from insoluble protein aggregates. The results obtained in this work indicate that PEG-dextran two-phase partitioning might provide a simple way for the recovery and partial purification of recombinant proteins which are produced as inclusion bodies.

• 한국세라믹학회지
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• 제36권11호
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• pp.1198-1204
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• 1999

The effect of sintering atmosphere on the grain sizes and phase distributions in 3Y-ZrO2 and 8Y-ZrO2 was investigated O2 and N2 were used as sintering atmospheres. In the case of 3Y-ZrO2 the sintered density was higher in N2 than in O2 while in the case of 8Y-ZrO2 contrary results were obtained. The observation can be explained by the nitrogen solubility into the zirconia lattice. That is nitrogen gas can behave as a diffusive gas contrary to the behavior in other oxides depending on the amount of Y2O3. In 3Y-ZrO2 tetragonal phase was retained at room temperature irrespective of sintering atmospheres. Grain sizes of two specimens were below 2㎛ and larger in O2 thin in N2 Under a given stress the transformability of tetragonal phase into monoclinic phase was higher in O2 than N2. The results are discussed on the basis of an effect of the grain size and non-transformable ttragonal(t') phase.

• 대한금속재료학회지
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• 제49권3호
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• pp.197-202
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• 2011

This study was carried out to investigate the precipitation behavior of ${\chi}$ phase and effect of ${\chi}-phase$ which precipitated at the initial stage of aging on mechanical properties of 25%Cr-7%Ni-4%Mo-0.2%N super duplex stainless steel. ${\chi}-phase$ was precipitated mainly at the interface of ferrite / austenite phases and inside of the ferrite phase at the initial stage of aging, and it was transformed into ${\sigma}-phase$ with an increase of aging time. The ferrite phase was decomposed into new $austenite({\gamma}_2)phase$ and ${\sigma}-phase$ by aging treatment. The hardness and tensile strength of the initial stage of aging when ${\chi}-phase$ was precipitated did not changed considerably, while elongation rapidly decreased. Accordingly, it is considered that ${\chi}-phase$ didn't affect the hardness and strength significantly, but it affected the elongation.

• 대한의용생체공학회:의공학회지
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• 제2권1호
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• pp.39-46
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• 1981

Microstructural phases of the dental amalgams have been studied by optical microscope, scanning electron microprobe and X-ray diffractometer. r1 ($Ag_2Hg_3$) phase and r2 ($Sn_{7-8}Hg$) phase are found on conventional compositioned alloys. On high copper single compositioned alloy, rl ($Ag_2Hg_3$) phase and V ($Cu_6Sn_5$) phase are found but brittle r2 ($Sn_(7-8)Hg$) phase.

• 한국세라믹학회지
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• 제32권8호
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• pp.915-921
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• 1995

The morphotropic phase boundary and phase transitions of the solid solutiion system, (1-x)(Na1/2Bi1/2)TiO3-PbTiO3＋xPbTiO3 were studied by investigating changes in crystal structure, variations in permittivity with temperature, and calorimetric behavior. It was observed that the morphotropic phase boundary (MPB) of this solid solutiion system was at near 14 mol% of PbTiO3. Compositions containing less than 10mol% PbTiO3 (x<0.1) exhibited a phase transition, i.e. ferroelectric rhombohedrallongrightarrowparaelectric paraelectric cubic, with increasing temperature. Composition containing more than 14 mol% PbTiO3 (x 0.14) showed a phase transition from ferroelectric tetragonal to paraelectric cubic. In the composition range of 0.1$\varepsilon$ (T) curve, which coincided with a phase transition from ferroelectric rhombohedral to an intermediate phase, was also found.

• 한국정밀공학회지
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• 제15권3호
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• pp.107-118
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• 1998

Two-phase neuro-system identification method is presented. The 1$^{st}$-phase identification uses conventional neural network mapping for modeling an input-output system. The 2$^{nd}$ -phase modeling is also performed sequentially using the 1$^{st}$-phase modeling errors. In the 2$^{nd}$ a phase modeling, newly generated input signals, which are obtained by summing the 1st-phase modeling error and artificially generated uniform series, are utilized as system's I-O mapping elements. The 1$^{st}$-phase identification is interpreted as a “Real Model” system identification because it uses system's real data(i.e., observations and control inputs) while the 2$^{nd}$ -phase identification as a “Artificial Model” identification because of using artificial data. Experimental results are given to verify that the two-phase neuro-system identification could reduce the overall modeling errors.rrors.

• JSTS:Journal of Semiconductor Technology and Science
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• 제16권3호
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• pp.352-358
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• 2016

A 5-phase phase-locked loop (PLL) for USB2.0 applications was implemented by using an all-synthesis technique. The length of the time-to-digital converter for the fine phase detector was halved by the operation of a coarse phase detector that uses 5-phase clocks. The maximum time difference between the rising edges of two adjacent-phase clocks was 6 ps at 480 MHz. The PLL chip in a 65-nm process occupies $0.038mm^2$, consumes 4.8 mW at 1.2 V. The measured rms and peak-to-peak output jitters are 8.6 ps and 45 ps, respectively.