• 분석과학
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• 제15권3호
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• pp.236-242
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• 2002

RF 글로우 방전 원자 방출 분광법을 사용하여 다층 도금강판 두께분석을 하였다. 일반적으로 gas jet boosted 글로우 방전은 플라스마 안정성과 스퍼터링 효율이 우수하여 기존의 두께 분석법에서 측정이 어려운 다층 두께분석이 가능하며, RF를 사용하여 비전도성 실리콘-수지계열의 다층 도금강판 두께분석이 가능하였다. RF gas-jet boosted 글로우 방전은 방전전원과 가스 흐름량 그리고 방전압력에 의해 스퍼터링을 조절할 수 있다. 그래서 스퍼터링 효율에 의해 다층 도금된 강판의 경우 소재에 따라 서로 다른 조건에서 측정할 수가 있었다. 본 연구에서 두께 $20{\mu}m$의 아연층을 가진 아연 도금강판의 두께 및 조성을 분석하기 위해서 최적조건에 대한 연구를 하였고, 두 가지 기준물질로 구성된 수지 도금강판을 이용해서 검량선을 측정하였다. 본 연구에 최적조건 및 검량을 하기 위해서 아연합금 도금강판 및 실리콘-수지 도금강판은 포항 산업 과학 기술원(RIST)에서 제공하였다.

• Journal of Pharmaceutical Investigation
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• 제31권4호
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• pp.241-256
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• 2001

Alginate microspheres, containing fluorescein isothiocyanate-bovine serum albumin (FITC-BSA) or green fluorescent protein (GFP) were prepared and used as a model drug to develop the oral vaccine delivery system. The alginate microspheres were coated with poly-L-lysine or chitosan. Two methods, w/o-emulsion and spray, were used to prepare alginate microspheres. To optimize preparation conditions, effects of several factors on the particle size and particle morphology of microsphere, and loading efficiency of model antigen were investigated. In both preparation methods, the particle size and the loading efficiency were enhanced when the concentration of sodium alginate increased. In the w/o-emulsion preparation method, as the concentration of Span 80 was increased from 0.5% to 2%, the particle size was decreased, but the loading efficiency was increased. The higher the emulsification speed was, the smaller the particle size and loading efficiency were. The concentration of calcium chloride did not show any effect on the particle size and loading efficiency. In the spray preparation method, the particle size was increased as the nozzle pressure $(from\;1\;kgf/m^2\;to\;3\;kgf/m^2)$ and spray rate was raised. Increasing calcium chloride concentration (<7%) decreased the particle size, in contrast to no effect of calcium chloride concentration on the w/o-emulsion preparation method. Alginate microspheres prepared by two methods were different in the particle size and loading efficiency, the particle size of microspheres prepared by the spray method was about $2-6\;{\mu}m$, larger than that prepared by the w/o emulsion method $(about\;2{\mu}m)$, and the loading efficiency was also higher with spray method. Furthermore, drying process for the microspheres prepared by the spray was simpler and easier, compared with the w/o emulsion preparation. Therefore, the spray method was chosen to prepare alginate microspheres for further experiments. Release pattern of FITC-BSA in alginate microspheres was evaluated in simulated intestinal fluid and PBS (phosphate buffered saline). Dissolution rate of FITC-BSA from alginate/chitosan microsphere was lower than that from alginate microsphere and alginate/poly-L-lysine microsphere. By confocal laser scanning microscope, it was revealed that alginate/FITC-poly-L-lysine microspheres were present in close apposition epithelium of the Peyer's patches of rabbits following inoculation into lumen of intestine, which proved that microspheres could be taken up by Peyer's patch. In conclusion, it is suggested that alginate microsphere prepared by spray method, showing a particle size of & $10\;{\mu}m$ and a high loading efficiency, can be used as a model drug for the development of oral vaccine delivery system.

• 대한소아치과학회지
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• 제24권4호
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• pp.763-770
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• 1997

The air abrasive technique is a non-mechanical method by which teeth are treated before restoration and stains and calculi are removed from tooth surfaces using the kinetic energy of small particles. The air abrasive technique in dentistry was first introduced in the 1950's with as instrument called 'Airdent'. But, as the main restorative materials of the period were amalgam and gold, and the instrument's inability to control the flow of particles caused the particles to be spread throughout the clinics, widespread use was not possible. In the 1990's, as these techincal problems were solved and more interest in new restorative materials rose in an effort to preserve sound tooth structure, new developements took place in instruments related to the air abrasive technique. The air abrasive technique produces less pressure, vibration and heat that might cause patient discomfort and facilitates the preservation of sound tooth structure. It also reduces the need for anesthesia and is less harmful to the pulp. Other advantages include increase in dentin bonding strength of composite resin, lower possibility of saliva contamination and maintenance of a dry field. But there is not direct contact between the nozzle and the tooth, the operator cannot use his or her tactile sense and must rely solely upon visual input. Other disadvantages are: the tooth preparation depends on the operator's ability; alpha-alumina particles, after bouncing off the tooth surface, cause damage to dental mirrors; the equipment is expensive and takes up a certain amount of space in the clinic. The author conducted case report using the air abrasive technique on patient visiting the Department of Pediatric Dentistry at Seoul National University Dental Hospital and arrived at the following conclusions. 1. The tooth preparation capability of different air abrasive devices varied widely among manufacturers. 2. It was more effective in treating early caries lesions and stains compared to lesions where caries had already progressed to produce soft dentin. 3. The cold stream and noise caused by the evacuation system was a major cause of discomfort to pediatric patients. 4. As there is no direct contact with tooth surface when using the air abrasive technique for tooth preparation, considerable experience and skill is required for proper tooth preparation.

• 한국재료학회지
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• 제29권11호
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• pp.720-726
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• 2019

Recently, research on cost reduction and efficiency improvement of crystalline silicon(c-Si) photovoltaic(PV) module has been conducted. In order to reduce costs, the thickness of solar cell wafers is becoming thinner. If the thickness of the wafer is reduced, cracking of wafer may occur in high temperature processes during the c-Si PV module manufacturing process. To solve this problem, a low temperature process has been proposed. Conductive paste(CP) is used for low temperature processing; it contains Sn57.6Bi0.4Ag component and can be electrically combined with solar cells and ribbons at a melting point of $150^{\circ}C$. Use of CP in the PV module manufacturing process can minimize cracks of solar cells. When CP is applied to solar cells, the output varies with the amount of CP, and so the optimum amount of CP must be found. In this paper, in order to find the optimal CP application amount, we manufactured several c-Si PV modules with different CP amounts. The amount control of CP is fixed at air pressure (500 kPa) and nozzle diameter 22G(outer diameter 0.72Ø, inner 0.42Ø) of dispenser; only speed is controlled. The c-Si PV module output is measured to analyze the difference according to the amount of CP and analyzed by optical microscope and Alpha-step. As the result, the optimum amount of CP is 0.452 ~ 0.544 g on solar cells.

• 한국추진공학회지
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• 제26권4호
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• pp.54-63
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• 2022

500 kg의 페이로드를 500 km 태양동기궤도에 이송가능한 소형발사체의 상단에 사용될 3톤급 액체로켓엔진을 설계하고 있다. 소형발사체의 1단에는 비행시험으로 검증된 75톤급 엔진을 사용한다. 상단용 엔진은 액체산소와 액체메탄을 연료로 사용되는데, 이 추진제 조합은 공통격벽탱크를 적용하여 무게 감소가 가능하고 비추력도 높다. 상단엔진의 사이클로는 저압으로 운용되어 신뢰성이 높은 팽창식 사이클을 채택했으며, 노즐 확대비 120이상에서 360초를 상회하는 비추력 성능을 보일 것으로 평가되었다. 엔진의 주요구성품인 연소기와 터보펌프는 목표 비용을 맞추기 위하여 적층제조된다. 엔진은 자가증기가압과 롤추력제어를 위하여 가열된 증기메탄을 제공하고, 이러한 기능을 가진 상단 추진기관시스템은 심우주탐사 등 다양한 임무에 확대 적용 가능할 것으로 기대된다.

• 생물환경조절학회지
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• 제22권2호
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• pp.138-145
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• 2013

최근 국내에 많이 보급되고 있는 이류체 포그 냉방시스템의 효율적인 제어알고리즘을 개발하기 위하여 다양한 조건의 분무사이클을 설정하여 토마토재배 온실에서 냉방실험을 실시하였다. 냉방효과는 평균 $1.2{\sim}4.0^{\circ}C$를 보였고, 냉방효율은 평균 8.2~32.9%로 나타났다. 분무간격에 따른 실험에서 90초 분무사이클의 냉방효율이 가장 높았고, 대체로 분무시간이 길수록, 정지시간이 짧을수록 냉방효율이 높게 나타났다. 이류체 포그시스템의 분무량이 증가할수록 냉방효율이 높아지는 경향을 찾을 수 있었다. 그러나 분무량을 증가시키더라도 내부공기가 포화상태에 가까워지면 더 이상 증발이 일어나지 않으므로 내부공기가 포화상태에 도달하기 전까지 분무량을 증대시키는 방법으로 냉방효율을 높일 수 있을 것으로 판단된다. 냉방효율이 증가함에 따라 실내공기의 포차는 감소하였고 실내외 절대습도 차이는 증가하는 경향을 보였다. 포그의 증발량이 증가할수록 실내와 실외의 절대습도 차이는 커지고, 이에 따라 환기에 의한 수증기 배출이 잘 되어 다시 증발효율을 상승시키므로 냉방효율이 높아지는 순환구조를 갖게 되는 것으로 판단된다. 분무시간과 정지시간에 따른 실내공기의 포차변화를 회귀분석한 결과 $10g{\cdot}kg^{-1}$의 포차 변화에 필요한 분무시간은 120초, 정지시간은 60초로 나타났다. 그러나 온도의 진동폭을 줄이고 냉방효율을 높이기 위해서는 포차의 변동범위를 $5g{\cdot}kg^{-1}$으로 설정하여 60초 분무, 30초 정지가 더 적당할 것으로 판단된다. 이류체 포그시스템의 제어방식을 컴퓨터 제어시스템과 현재 보급되고 있는 간편제어시스템으로 분류하여 제어알고리즘을 유도하였다. 자연환기 온실에서 간편 제어시스템을 사용한다면 분무사이클을 60초 on, 30초 off로 설정하고 온도하한은 30~$30{\sim}32^{\circ}C$, 습도상한은 85~90%로 설정할 것을 제안한다.