• Title/Summary/Keyword: Nitrogen contents

Search Result 2,311, Processing Time 0.029 seconds

Comparison of the Total Nitrogen Determination Methods (총질소 분석방법의 비교)

  • Joung, Kwang-Wook;Yoon, Chun-Gyeong;Ham, Jong-Hwa
    • Proceedings of the Korean Society of Agricultural Engineers Conference
    • /
    • 2001.10a
    • /
    • pp.421-425
    • /
    • 2001
  • Among the many parameters describing water quality, total nitrogen content(TN) is regarded as important one in relation to water quality management of the waterbodies for its role in eutrophication process. This study evaluated for accuracy, convenience and promptness of nitrogen analysis methods : (1)UV spectrophotometric method, (2)summation method, (3)cadmium reduction method. And, the detection limit of each method was calculated using EPA method. The UV spectrophotometric method after oxidation appears to be more convenient and accurate in determination of the TN contents than the summation method and cadmium reduction method. The summation method is necessary to separate determinations of the organic nitrogen, ammonia, nitrite, and nitrate. And, because summation method has many other methods for each contents, it can be detected for wide range of concentration.

  • PDF

The Sheet Resistance Properties of Tungsten Nitride Thin films for Intergrated Circuit (IC소자용 질화 텅스텐 박막의 면저항 특성)

  • 이우선;정용호;김남오;정종상;유병수
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1997.11a
    • /
    • pp.94-97
    • /
    • 1997
  • We investigated the sheet resistance properties of tungsten nitride thin films deposited by RF and DC sputtering system. It deposited at various conditions that determine the sheet resistance. The properties of the sheet resistance of these films were measured under various conditions. Sheet resistance analysed under the flow rate of the argon gas and contents of nitrogen from nitrogen-argon gas mixtures. We found that these sheet resistance were largely depend on the temperature of substrate, gas flow rate and RF power. Very high and low sheet resistance of tungsten films obtained by DC sputtering. As the increase of contents of nitrogen gas obtained from nitrogen-argon gas mixture, tungsten nitride thin films deposited by the reactive DC sputtering and the sheet resistance of these films were increased.

  • PDF

Synthesis of Nitrogen-Doped Graphene by Thermal Annealing of Graphene Oxide with Melamine Compounds (멜라민 화합물을 이용한 산화 그래핀 도핑 및 특성 평가)

  • Kim, Sumin;Kim, Hyun;Kim, So Yang;Han, Jong Hun
    • Korean Journal of Materials Research
    • /
    • v.29 no.11
    • /
    • pp.677-683
    • /
    • 2019
  • In this paper, nitrogen-doped reduced graphene oxide(rGO) is obtained by thermal annealing of nitrogen-containing compounds and graphene oxide (GO) manufactured by modified Hummers' method. We use melamine as a nitrogen-containing compound and treat GO thermally with melamine at over $800{\sim}1,000^{\circ}C$ and 1 ~ 3 hr under Ar atmosphere. The electrical conductivity of doped rGO is measured by 4-point probe method. As a result, nitrogen contents on rGO are found to be in the range of 2.5 to 12.5 at% depending on the doping conditions after thermal annealing. The main doping site on graphene oxide is changed from pyridinic-N and pyrrolinic N to the graphitic site as the heat treatment temperature increases. The electrical conductivity of doped rGO increases as the N doping content increases. As the thermal treatment time increases, the change of both total doping contents and doping sites is slight and the surface resistance is remarkably reduced, which is caused by healing effects of doped graphene oxide at high temperature.

Effects of Nitrogen Level and Planting Density on Chemical Properties in Korean Native Tabacco Varieties (재래종연초의 화학특성에 미치는 질소시비량 및 재식밀도의 영향)

  • 정형진;김길웅;박수준
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.34 no.3
    • /
    • pp.288-295
    • /
    • 1989
  • This study was conducted to establish the most appropriate nitrogen levels and planting densities which can attribute to increase of aromatic substances in tobacco variety, Hyangcho, maintaining its original aroma. An increase of nitrogen fertilization from 3 to 12 kg per 10a increased total alkaloid content 2.0% to 3.3%, while an increased nitrogen fertilization decreased the contents of total sugar, starch, fatty acid etc., Which seem to be the positive components relating to tobacco aroma the contents of alkaloids were decreased and total fatty acids were increased as the planting densities increased. The higher contents of 2. 3-methylbutanoic and 3-methylpentanoic acid was obtained at the density of 3 plant per pit (12,498 plant/10a). The components determined in the neutural fraction such as solanone, furfural, furfurylalcohol and benzyl alcohol were presented in higher amount at the higher densities. The volatile acids such as 2. 3-methylbutanoic acid 3-methylpentanoic acid decreased and also the contents of butanol, furfutal, furfuryl alcohol, hexanol, cinnamil, acetophenone, benzyl acetate and solanone etc., were decreased as the nitrogen level increased from 3 to 12 kg per l0a.

  • PDF

Austenite Precipitation Behaviors with Solidification Rate and N Solubility in Cast Duplex Stainless Alloys (주조용 이상스테인리스강에서 응고속도 및 질소고용도에 따른 오스테나이트 석출 거동)

  • Lee, Jong-Yeop;Lee, Je-Hyun;Kim, Sang-Sik;Choi, Byung-Hak;Kim, Sung-Jun;Son, Hee-Young
    • Korean Journal of Materials Research
    • /
    • v.17 no.12
    • /
    • pp.654-659
    • /
    • 2007
  • Austenite precipitation behavior was studied with solidification rates and alloying contents, N and Cr, in duplex stainless steels by directional solidification. Directional solidification experiments were carried out with solidification rates, $1{\sim}100mm/s$, and N and Cr contents, $0{\sim}0.27wt.%,\;25{\sim}28wt.%$ respectively, in a duplex stainless steel, CD4MCU. As the solidification rate increases, the dendrite spacing reduced and the austenite phase in the ferrite matrix became finer. The volume fraction of austenite phase increased and its shape went to be round with increasing nitrogen contents in duplex stainless alloys. The Cr alloying element, even though it is a ferrite former, showed to enhance the nitrogen solubility in the alloy and caused the austenite round and finer. Also, Cr was supposed to decrease the austenite volume fraction, but it increased the austenite slightly due to increasing nitrogen solubility during solidification.

Nitrogen Characteristics in Poultry Manure Using Sea Urchin Shell Powder as Poultry Diets : A Field Study

  • Chung, Tae Ho;Choi, In-Hag
    • Journal of Environmental Science International
    • /
    • v.23 no.1
    • /
    • pp.153-156
    • /
    • 2014
  • This study was conducted to evaluate the effects of sea urchin shell powder on nitrogen characteristics in poultry litter by assigning ninety 1-d-old male broiler chicks (Arbor Acres) to one of 3 treatments (control, 1% sea urchin shell powder, and 1% feed additives) in 3 replicates of 10 birds each. For all treatments, the overall dry matter contents were decreased (P < 0.05) as time increased, except for at 1 week. When compared with controls, the dietary sea urchin shell powder and feed additives for 0 and 3 weeks did influence their TN contents, but not for 1, 2 and 4 weeks. The treatments with sea urchin shell powder and feed additives had a significant (P < 0.05) influence on $NH_3$-N in poultry litter compared with controls. However, at 4 weeks, no marked differences were observed in $NH_3$-N contents among treatments. Treatments with 1% sea urchin shell powder might enhance the value of poultry litter as N fertilizer.

A Study of Weld Fusion Zone Phenomena in Austenitic Stainless Steels(2) - Effects of Nitrogen on Microstructural Evolution and Hot Cracking Susceptibility GTA Welds in STS 304 - (오스테나이트계 스테인리스강 용접부의 금속학적 현상에 관한 연구(2) - STS 304 용접부 조직특성 및 고온균열 감수성에 미치는 질소의 영향 -)

  • 이종섭;김숙환
    • Journal of Welding and Joining
    • /
    • v.18 no.1
    • /
    • pp.59-69
    • /
    • 2000
  • The purpose of the present study was to investigate weld metallurgical phenomena such as primary solidification mode, microstructural evolution and hot cracking susceptibility in nitrogen-bearing austenitic stainless steel GTA welds. Eight experimental heats varying nitrogen content from 0.007 to 0.23 wt.% were used in this study. Autogenous GTA welding was performed on weld coupons and the primary solidification mode and their microstructural characteristics were investigated from the fusion welds. Varestraint test was employed to evaluate the solidification cracking susceptibility of the heats and TCL(Total Crack Length) was used as cracking susceptibility index. The solidification mode shifted from primary ferrite to primary austenite with an increase in nitrogen content. Retained delta ferrite exhibited a variety of morphology as nitrogen content varied. The weld fusion zone exhibited duplex structure(austenite+ferrite) at nitrogen contents less than 0.10 wt.% but fully austenitic structure at nitrogen contents more than 0.20 wt.%. The weld fusion zone in alloys with about 0.15 wt.% nitrogen experienced primary austenite + primary ferrite solidification (mode AF) and contained delta ferrite less than 1% at room temperature. Regarding to solidification cracking susceptibility, the welds with fully austenitic structure exhibited high cracking susceptibility while those with duplex structure low susceptibility. The cracking susceptibility increased slowly with an increase in nitrogen content up to 0.20 wt.% but sharply as nitrogen content exceeded 0.20 wt.%, which was attributed to solidification mode shift fro primary ferrite to primary austenite single phase solidification.

  • PDF

Relationship between some chemical components in the rice plants and varietal reaction to blast disease (도열병 품종저항성과 도체내 성분과의 관계)

  • Baek Soo Bong
    • Korean journal of applied entomology
    • /
    • v.9 no.1
    • /
    • pp.15-20
    • /
    • 1970
  • An investigation was carried out to know the relationship between resistance of rice varieties to blast disease and the chemical components, especially total nitrogen and total sugars, in the rice plants. The results sic summarized as follow: 1) The nitrogen contents in the resistant variety were less than those of susceptible one, and sugar contents were reversed. Accordingly, the C/N ratio in the resistant variety was higher than that obtained by susceptible one. 2) The free amino acids contents, especially, Glutamine, Valine, Leusine and Iso-leusine, in the resistant varieties were more than those of the susceptible varieties. 3) The starch synthetic activity of rice leaves in the resistant varieties was higher than that of susceptible one in fructose and glucose solutions, but it was reversed in sucrose solution. 4) When more nitrogen was dressed, the total nitrogen content of rice leaves was increased than the ordinary dressing. The rate of increase in nitrogen content in resistant variety was lower than those of the susceptible. The total sugar content of rice plants dressed more nitrogen was decreased at early tillering stage, but increased at maximum tillering stage. It seemed that the rate of increase of total sugar in the resistant variety was higher than those of the susceptible.

  • PDF

Seasonal biomass and carbon, nitrogen contents change of Schoenoplectus trigueter in Nakdong river estuary (낙동강 하구 갯벌에 생육하는 세모고랭이(Schoenoplectus triqueter)의 생체량 및 탄소, 질소 함량의 계절 변화)

  • An, Soonmo;Lee, Jiyoung;Jeong, Sinjae
    • Journal of Wetlands Research
    • /
    • v.8 no.3
    • /
    • pp.39-49
    • /
    • 2006
  • Seasonal biomass and carbon, nitrogen contents change of marsh club-rush (Schoenoplectus trigueter) was investigated in Nakdong river estuary, located near Busan, Korea. New shoot of S. trigueter sprouted from tuber in April and fast growth season was followed until mature in August. Mature lengths of shoot and root were 60 and 9.4 cm, respectively. The increase of biomass showed similar seasonal trends with length. Mature biomass were $3.5gind^{-1}$ in wet weight and $0.6gind^{-1}$ in dry weight. The biomass of S. trigueter in areal basis was also highest during July and August ($186gDWm^{-2}$). The shoot of S. trigueter was disappeared in October from the ground but the biomass of shoot was maintained as a form of detritus in sediment. The amount of S. trigueter detritus was about 30~50% of the biomass in August. During winter, the amount of detritus decreased with time but the biomass of root+tuber remained same, implying the root+tuber part is alive. The net productivity of S. trigueter estimated from biomass change were $538gDWm^{-2}yr^{-1}$, $240g-Cm^{-2}yr^{-1}$, $8.2g-Nm^{-2}yr^{-1}$ in dry weight, carbon and nitrogen equivalent respectively. During winter, carbon to nitrogen ratio in detritus increased implying the preferred remineralization of nitrogen during microbial degradation.

  • PDF

Studies on the Growth and Nutrient Uptake of Flag Leaf and Chaff of Rice Plant in Cold Injury Location II. Influence of Different Transplanting Date on Nutrient Uptake of Flag Leaf and Chaff of Rice Plant (냉해지대의 수도생육과 임,불임 인각의 양분흡수에 관한 연구 제2보 재배시기 이동이 수도지엽과 인각의 양분흡수에 미치는 영향)

  • Kim, Y.J.;Choi, S.I.;Ra, J.S.;Lee, J.H.
    • KOREAN JOURNAL OF CROP SCIENCE
    • /
    • v.27 no.3
    • /
    • pp.206-217
    • /
    • 1982
  • This experiment was conducted to study about nutrient absorption of flag leaf and chaff of rice plant different transplanting date with elevations. Heading stage was delayed by destructive cold temperature or late transplanting. Plant analyses revealed that above poor plants also had higher total nitrogen content, but ower silicate in the flag leaf and sterile chaff. Total nitrogen and silica contents to accumulated in flag leaf between yield was significant high correlation. The chaff of late transplanting and sterility was high total nitrogen. Relationship between silicate absorption and total nitrogen of chaff was significant high correlation. Ripening temperature after heading stage was influenced total nitrogen of chaff. Phosphate, potassium, calssium and silicate contents of chaff increased hight ripening temperature but total nitrogen decreased. Therefore, inorganic element contents of chaff was closely connected with grain sterility.

  • PDF