• Current Applied Physics
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• 제18권11호
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• pp.1218-1224
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• 2018

Pressure-dependent structural and morphological changes of two amphibole minerals, tremolite and actinolite, were investigated up to 7.0 GPa using synchrotron X-ray powder diffraction underthree different pressure transmission media (PTM): water (W), $CO_2$ and silicone oil (SI). The elastic response of tremolite and actinolite are found to be dependent on the PTM used. When using water (W) as PTM, tremolite and actinolite show normal volume contractions with bulk moduli of 74(1) and 78(1) GPa, respectively. When using $CO_2$ as PTM, we observe the formation of calcite from tremolite above 3.8(1) GPa, whereas actinolite did not show any carbonation reaction. Under silicone oil PTM, we observe modulated volume contraction behaviors in both samples, compared to water and $CO_2$ PTM, with bulk moduli in the order of 90(1) and 94(4) GPa for tremolite and actinolite, respectively.

• 한국전산유체공학회지
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• 제21권2호
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• pp.90-98
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• 2016

A numerical study is conducted on thermal performance of a large-area hot plate specially designed as a heating and cooling tool for thermal nanoimprint lithography process. The hot plate has a dimension of $240mm{\times}240mm{\times}20mm$, in which a series of cartridge heaters and cooling holes are installed. The material is stainless steel selected for enduring the high molding pressure. A numerical model based on the ANSYS Fluent is employed to predict the thermal behavior of the hot plate both in heating and cooling phases. The PID thermal control of the device is modeled by adding user defined functions. The results of numerical computation demonstrate that the use of cartridge heaters provides sufficient heat-up performance and the active liquid cooling in the cooling holes provides the required cool-down performance. However, a crucial technical issue is raised that the proposed design poses a large temperature non-uniformity in the steady heating phase and in the transient cooling phase. As a remedy, a new hot plate in which heat pipes are installed in the cooling holes is considered. The numerical results show that the installation of heat pipes could enhance the temperature uniformity both in the heating and cooling phases.

• 한국전산유체공학회지
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• 제17권4호
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• pp.16-23
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• 2012

Current display manufacturing processes apply thermal treatment of glass backplanes widely for hydrogen degassing, crystallization of thin-films, tempering, forming, and precompaction. Estimation of the characteristics of transient heating stages and thermal non-uniformities on a single glass substrate or in a stack of glasses are extremely helpful to understand non-homogeneity of mechanical and electronic features of nano/micro structures of end products. Based on simple heat transfer models and using an electric muffle furnace, temperature variations in a glass stack were predicted and measured for glass backplanes of $1.5{\times}1.85m^2$ in size and 0.7 mm in thickness. Except for the period of putting glass backplanes into the furnace, thermal radiation was the major heating mechanism for the treatment and theoretical predictions agreed well to the experimental temperatures on the backplanes. Using the theoretical model, thermal fields for a glass stack of glass-size, $2.2{\times}2.5m^2$, and of the number of sheets, 1 to 12, were calculated for practical design and manufacturing of the muffle furnace for large-scale displays, e.g. up to $8^{th}$ generation.

• 대한기계학회논문집B
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• 제37권10호
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• pp.887-894
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• 2013

복합재의 물성치 해석에 일반적으로 사용되는 일반화된 자기일치모델(Generalized Self-Consistent Model)과 수정된 에쉘비모델(Modified Eshelby Model)을 이용하여 나노유체의 열전도계수를 예측할 수 있음을 보였다. 이 유체의 열전달효과를 대폭 향상시키는 대표적인 메카니즘 중 하나인 나노입자와 기본유체 사이에 존재하는 나노층의 영향을 고려하여 나노유체의 열전도계수를 예측하였다. 본 연구는 나노층의 열전도계수가 일정한 값을 가질 때 기존 대표적인 모델과 동일한 결과를 보였으며, 선형적으로 변할 때 역시 문헌에 있는 모델과 동등한 수준의 예측 값을 보였다. 알루미나와 산화구리를 나노입자로 물과 에틸렌글리콜을 기본유체로 한 나노유체의 열전도계수에 대한 실험결과와 본 모델의 예측결과를 비교함으로써 본 모델의 타당성을 입증하였다.

• 대한기계학회논문집B
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• 제35권2호
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• pp.113-120
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• 2011

본 논문은 나노유체의 열확산율을 측정하는 센서와 주변회로 그리고 데이터의 처리방법을 제시한 것이다. 기존 비정상열선법을 이용하면 이론상 유체의 열전도율과 열확산율을 동시에 측정할 수 있으나 열전도율과 비교하여 열확산율은 많은 오차가 발생한다. 본 연구에서 제시한 방법은 측정변수가 단순하고 복잡한 센서의 교정과정을 생략할 수 있는 실용적 측면의 장점이 있다. 먼저 열확산율이 잘 알려진 유체들에 대한 검증실험을 실시하였고 나노유체의 열확산율을 측정하여 기본유체와 비교하는 과정을 예시적으로 설명하였다. 본 연구는 기존 열전도율측정에 한정되어 왔던 나노유체 연구의 범위를 열확산율 또는 비열의 개념으로 확장하였다는 관점에서 중요성을 갖는다.

• 한국산학기술학회논문지
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• 제3권4호
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• pp.233-239
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• 2002

21세기에 가장 시급하게 확보되어야 하는 기술은 BT(Biotechonolgy)와 NT(Nano technology)를 접목시키는 기술이다. 특히, 이들을 종합한 MEMS 에 관한 연구는 가장 광범위한 분야에서 활발하게 이루어지고 있어 그 기술적 가치가 점차 중요시되고 있다. 본 연구는 Simulation을 통하여 Bio-MEMS 기술에서 사용되는 미세Pump 내에서의 유체흐름을 Fluent 프로그램을 사용하여 알아보고자 하였다. 즉, 미세Pump 내로 유체가 흐를 경우, 유체의 압력변화나 온도변화 및 Model에 따른 유동의 흐름을 관찰하여 미세Pump 내에서의 최적의 외부조건과 최적의 Pump Model을 알아보고자 실험하였다. 유동의 흐름을 조사해 본 결과 Chamber의 유무에 따라 압력과 온도의 변화를 관찰할 수 있었다. Chamber가 있는 경우 압력의 변화가 적었고 온도의 변화 또한 적었다. 따라서 Chamber가 있는 Pump가 유체의 흐름에 영향을 적게 줌을 알 수 있었으며 이는 Chamber가 있는 Pump를 설계하는 것이 필요하다고 할 수 있다.

• Korean Chemical Engineering Research
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• 제55권2호
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• pp.220-224
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• 2017

본 논문에서는 전기절연판이나 접착제로 널리 사용되는 페놀수지를 초임계 유체를 이용하여 카본입자로 재활용 하는방법을 연구 하였다. 폐페놀수지는 불융/불용 특성으로 대부분 매립하거나 소각처리하고 있으며, 환경오염 방지차원에서 페놀수지의 새로운 재활용 기술 개발이 매우 필요한 실정이다. 폐페놀수지를 재활용하기 위해 다양한 아/초임계 용매(에탄올, 아세톤, 물, 메탄올)를 선정하여 처리하였다. 그 결과 기존의 카본입자의 제조 방법들 보다 훨씬 낮은 온도 조건($350{\sim}380^{\circ}C$)에서 카본입자를 제조할 수 있었다. 본 연구에서는 재활용된 카본입자의 FT-IR, XRD, TGA, SEM, EDS 분석을 통하여 반응용매에 따른 카본입자의 특성을 고찰하였으며, 모든 용매에 대해 동일한 화학구조 및 비정질 구조를 가지는 카본입자를 제조 할 수 있었다.

• Journal of the Optical Society of Korea
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• 제10권3호
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• pp.130-142
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• 2006

Lab-on-a-chip technology is attracting great interest because the miniaturization of reaction systems offers practical advantages over classical bench-top chemical systems. Rapid mixing of the fluids flowing through a microchannel is very important for various applications of microfluidic systems. In addition, highly sensitive on-chip detection techniques are essential for the in situ monitoring of chemical reactions because the detection volume in a channel is extremely small. Recently, a confocal surface enhanced Raman spectroscopic (SERS) technique, for the highly sensitive biological analysis in a microfluidic sensor, has been developed in our research group. Here, a highly precise quantitative measurement can be obtained if continuous flow and homogeneous mixing condition between analytes and silver nano-colloids are maintained. Recently, we also reported a new analytical method of DNA hybridization involving a PDMS microfluidic sensor using fluorescence energy transfer (FRET). This method overcomes many of the drawbacks of microarray chips, such as long hybridization times and inconvenient immobilization procedures. In this paper, our recent applications of the confocal Raman/fluorescence microscopic technology to a highly sensitive lab-on-a-chip detection will be reviewed.

• 한국분무공학회지
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• 제8권1호
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• pp.16-22
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• 2003

Zeta potential measurements of colloid particles suspended in a liquid are performed by a Zeta Meter developed. There are many applications of colloid stability in spray technology, paints, wastewater treatment, and pharmaceuticalse. Zeta potentials of charged particles are obtained by measuring the electrophoretic velocities of the particles using video enhanced microscopy and image analysis program. The values of zeta potential of polystyrene latex(PSL), $silica(SiO_2)$M, polyvinylidence difluoride(PVDF), silicon nitride, and alumina particles in deionized (DI) water were measured to be -40.5, -31.9, -25.2, -15.1 and -10.1mV, respectively. The particles having high zeta potential less than -20 mV are stable in DI water, because the double layers of them have strong repulsive forces mutually, and the particles having low zeta potential over -20mV are unstable due to Van Der Waals forces. Silica(>20nm), PSL, aluminum and PVDF particles were found to be stable that would remain separate and well disperse, while silicon nitride and alumina particles were found to be unstable that would gradually agglomerate in DI water.

• 한국가시화정보학회지
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• 제3권1호
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• pp.3-19
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• 2005

Novel optical techniques are presented for three-dimensional tracking of nanoparticles; Optical Serial Sectioning Microscopy (OSSM) and Ratiometric Total Internal Reflection Fluorescent Microscopy (R-TIRFM). OSSM measures optically diffracted particle images, the so-called Point Spread Function (PSF), and dotermines the defocusing or line-of-sight location of the imaged particle measured from the focal plane. The line-of-sight Brownian motion detection using the OSSM technique is proposed in lieu of the more cumbersome two-dimensional Brownian motion tracking on the imaging plane as a potentially more effective tool to nonintrusively map the temperature fields for nanoparticle suspension fluids. On the other hand, R-TIRFM is presented to experimentally examine the classic theory on the near-wall hindered Brownian diffusive motion. An evanescent wave field from the total internal reflection of a 488-nm bandwidth of an argon-ion laser is used to provide a thin illumination field of an order of a few hundred nanometers from the wall. The experimental results show good agreement with the lateral hindrance theory, but show discrepancies from the normal hindrance theory. It is conjectured that the discrepancies can be attributed to the additional hindering effects, including electrostatic and electro-osmotic interactions between the negatively charged tracer particles and the glass surface.