• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제52권7호
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• pp.288-292
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• 2003

AlM thin film has been deposited on A1$_2$O$_3$ substrate by reactive radio frequency(RF) magnetron sputtering method under various operating conditions such as working pressure, fraction of nitrogen partial pressure, and substrate temperature. Scanning Electron Microscope(SEM), X-ray Diffraction(XRD), and Atomic Force Microscope(AFM) have been measured to find out structural properties and preferred orientation of AlN thin films. SAW velocity of IDTs/AlN/Si structure was about 5038［㎧］ at the center frequency of 251.9［MHz］ and insertion loss was measured to be relatively low value of 35.6［dB］. SAW velocity of IDTs/AlN/A1$_2$O$_3$ structure was improved to be about 5960［㎧］ at the center frequency of 296.7［MHz］.

• Journal of applied mathematics & informatics
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• 제7권1호
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• pp.125-137
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• 2000

A solution of the findpath problem in which a moving object in required to avoid moving obstacles and move to the designated target in the plane is porcided via the second method of Lyapunov. This paper presents an new control designed by a family of piecewise Lyapunov functions to solve a findpath problem and gives some simultion results of that.

• 한국재료학회지
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• 제33권3호
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• pp.106-114
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• 2023

The carbon concentration in the carburized steels was measured by electron probe microanalysis (EPMA) for a range of soluted carbon content in austenite from 0.1 to 1.2 wt%. This study demonstrates the problems in carbon quantitative analysis using the existing calibration curve derived from pure iron (0.008 wt%C) and graphite (99.98 wt%C) as standard specimens. In order to derive an improved calibration curve, carbon homogenization treatment was performed to produce a uniform Kα intensity in selected standard samples (AISI 8620, AISI 4140, AISI 1065, AISI 52100 steel). The trend of detection intensity was identified according to the analysis condition, such as accelerating voltage (10, 15, 30 keV), and beam current (20, 50 nA). The appropriate analysis conditions (15 keV, 20 nA) were derived. When the carbon concentration depth profile of the carburized specimen was measured for a short carburizing time using the improved calibration curve, it proved to be a more reliable and accurate analysis method compared to the conventional analysis method.

• 대한화학회지
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• 제38권11호
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• pp.827-832
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• 1994

(N-methylphenazinium) bis(oxalato)palladate(II)$((C_{13}H_{11}N_2)_2[Pd(C_2O_4)_2])$의 착이온 및 결정의 구조는 X-선 회절법으로 연구하였다. 이 결정은 사방정계이고 공간군은 P1 (군번호 = 2)이다. 단위세포 길이는 a = 7.616(8), b = 9.842(3), c = $20.335(7)\AA$, $\alpha$ = 103.53(3), $\beta$ = 90.00(5), $\gamma$ = $112.38(5)^{\circ}이며$, $V = 1363(2){\AA}^3,\;F_w = 672.93,\;D_c = 1.639\;gcm^{-3},\;F(000) = 680.0,\;{\mu} = 7.3\;cm^{-1},\;Z = 2$이다. 회절반점들의 세기는 흑연 단색화 장치가 있는 자동 4축 회절기로 얻었으며 $Mo-K\alpha$ X - 선(${\lambda}$= 0.7107 $\AA)$을 사용하였다. 구조분석은 중금속법으로 풀었으며, 최소자승법으로 정밀화하였고, 최종 신뢰도 값들은 3120개의 회절반점에 대하여 $R = 0.069,\;R_w = 0.050,\;R_{all} = 0.069$ 및 S = 5.45였다. 착이온들은 근본적인 평면구조로써, 이들의 충진구조는 착음이온들을 두개의 양이온들이 거의 평행하게 둘러싸고 있는 삼중체들을 형성하고 있다. 양이온과 음이온들의 이면각들이 각각 6.3(6)과 $57.06(6)^{\circ}$인 삼중체들이 b축을 따라서 배열되어 있으나, 삼중체면의 배향은 두 가지 착음이온의 이면각이 $59.08(9)^{\circ}$을 이루는 방향이다. 삼중체내의 면간거리는 각각 3.328와 3.463 $\AA$이었다.

• 한국약용작물학회지
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• 제7권1호
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• pp.45-50
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• 1999

지모의 고품질 품종 육성 및 재배법 개선과 유통중인 생약으로서의 안전성을 위한 품질 평가 기준을 설정하기 위해 지모의 지표성분의 HPLC 분석법을 확립하고자 하였다. 먼저 지모의 유효성분을 분리하고 지표성분화 한 후 HPLC 분석 정량법을 검토하므로써 지모의 품질 분석법을 구명한 결과는 다음과 같다. 지모를 MeOH로 대량 추출하여 계통 추출법으로 용매분배 후 조사포닌 분획인 n-BuOH ext.를 얻었으며 이 n-BuOH ext. 을 silica gel 컬럼 크로마토그래피를 수행하여 화합물 1를 순수 분리 정제하였다. 화합물 1의 $^1H$, $^{13}C$ NMR spectra 등을 검토한 결과 화합물 1은 지모의 주요 약효성분인 timosaponin A III로 확인되었다. Timosaponin A III은 지모의 주요 성분이자 혈당 강하작용과 항암활성 등의 주요 약효를 보이는 성분으로 지모의 품질 평가 기준으로서 지모의 지표성분으로 하기에 적합하였다. Timosaponin A III의 HPLC 분석법 확립을 위해 ELSD 검출기 가 사용되었으며 ODS계 컬럼을 사용하고 60% acetonitrile를 이동상으로 하여 0.9ml/min의 유속으로 분석을 한 것이 가장 적절한 timosaponin AIII의 HPLC 분석 조건이었다. Timosaponin AIII의 HPLC 분석을 위한 지모 시료의 추출조건 검토에서는 1g 분말시료를 80% MeOH를 추출용매로 할 때 $80^{\circ}C$에서 총 2회 환류 추출하는 것이 성분의 총 회수율을 가장 높이는 추출조건이었다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2001년도 학술대회 논문집 전문대학교육위원
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• pp.35-39
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• 2001

The purpose of this paper is improvement the piezoelectric of Polyvinylidene fluoride(PVDF) organic thin films is fabricated by vapor deposition method. The piezoelectric of PVDF organic thin films attributed to dipole orientation in crystalline region. Also, the piezoelectric characteristic reduced that dipole moments orientation in crystalline region interfered with impurity carriers. Therefore, PVDF organic thin films fabricated with high substrate temperature condition for crystallinity improvement. The crystallinity of PVDF organic thin films fabricated by this condition increase from 47 to 67.8%. The ion density of PVDF organic thin films fabricated by substrate temperature variation from $30^{\circ}C$ to $105^{\circ}C$ decreased from $1.62{\times}10^{16}cm^3$ to $6.75{\times}10^{11}cm^3$ when temperature and frequency were $100^{\circ}C$, 10Hz, respectively. The $d_{33}$ and piezo-voltage coefficient of PVDF organic thin films increased from 20pPC/N to 33pC/N and $162.9{\times}10^{-3}V{\cdot}m/N$ to $283.2{\times}10^{-3}V{\cdot}m/N$, respectively. For the sake of the applications of piezoelectric sensor, we analyzed the output voltage characteristic as a function of the distance between an oscillator of 28kHz and PVDF organic thin film transducer. From this, we found that the output voltage is inversely proportional to the distance. At this time, the period was about $35.798{\mu}s$ and equal the oscillator frequency.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1997년도 하계학술대회 논문집 A
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• pp.303-305
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• 1997

The advantage of application polymer instead of conventional porcelain as the housing material for arrester is that light weight, shorter section length of arrester would be possible due to the use of an insulated hanger (mold compound). also, polymer arrester has very good characteristics in design versatility as well as excellent resistance to moist ingress and pollution performance. The finite element method is widely used to calculate for electromagnetic devices. In this paper, we perform the each conditional analysis of PC with an advanced graphical user interface(GUI) using the vector fields simulator. And we try to analyze electromagnetic fields through the conventional two dimensional analysis in case of high voltage contamination on the electrode of a arrester.

• 한국지반공학회:학술대회논문집
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• 한국지반공학회 2002년도 가을 학술발표회 논문집
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• pp.303-310
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• 2002

Overbreak occurred inevitably in a tunnel excavation, Is the main factor for increasing cost and time in tunnel projects. Furthermore the damage to the remained rock mass related to the overbreak can give rise to a serious safety problem in tunnels. As a rule of thumb, causes for the overbreak are inaccuracy in drilling, the wrong design of blasting and selection of explosives, and heterogeneity in rock mass. Specially, the geological features of the rock mass around periphery of an excavation are very important factors, so a lot of researches have been conducted to describe these phenomena. But the quantitative geological classification of the rock mass for the overbreak and the method for decreasing the amount of the overbreak have not been established. Besides, the technical improvement of the charge method is requested as explosives for the smooth blasting have not functioned efficiently. In this study, the working face around periphery of an excavation has been continuously sectionalized to 5∼6 parts, and the new Blastability Index for the overbreak based on 6 factors of RMD(Rock Mass Description), UCS(Uniaxial Compressive Strength) JPS(Joint Plane Spacing), JPO(Joint Plane Orientation), JPA(Joint Plane Aperture) and FM(Filling Material) is proposed to classify sections of the working face. On the basis of this classification, the distance between contour holes and the charging density are determined to minimize the overbreak. For controlling the charging density and improving the function of explosives, the New Deck Charge(N.D.C) method utilizing the deck charge method and detonation transmission in hole has been developed.

• 한국전기전자재료학회논문지
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• 제29권2호
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• pp.90-94
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• 2016

In this work, [$Pb(Mg_{1/2}W_{1/2})_{0.03}(Ni_{1/3}Nb_{2/3})_x(Zr_{0.5}Ti_{0.5})_{0.97-x}O_3-BiFeO_3$] (x=0.02 to 0.12) composition ceramics were fabricated by the conventional soild state reaction method and their microstructure and piezoelectric properties were investigated according to PNN substitution. The addition of small amount of $BiFeO_3$, $Li_2CO_3$, and $CaCO_3$ were used in order to decrease the sintering temperature of the ceramics. The XRD (x-ray diffraction patterns) of all ceramics exhibited a perovskite structure. The sinterability of PMW-PNN-PZT-BF ceramics was remarkably improved using liquid phase sintering of $CaCO_3$, $Li_2CO_3$. However, it was identified from of the X-ray diffraction patterns that the secondary phase formed in grain boundaries decreased the piezoelectric properties. According to the substitution of PNN, the crystal structure of ceramics is transformed gradually from a tetragonal to rhombohedral phase. The x=0.10 mol PNN-substituted PMW-PNN-PZT-BF ceramics sintered at $920^{\circ}C$ showed the optimum values of piezoelectric constant($d_{33}$), piezoelectric figure of merit($d_{33{\cdot}}g_{33}$), planar piezoelectric coupling coefficient($k_p$) and density : $d_{33}=566$ [pC/N], $g_{33}=29.28[10^{-3}mV/N]$, $d_{33{\cdot}}g_{33}=16.57[pm^2/N]$, $k_p=0.61$, density=7.82 [$g/cm^3$], suitable for duplex ultrasonic sensor application.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2001년도 기술교육위원회 창립총회 및 학술대회 의료기기전시회
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• pp.9-12
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• 2001

The $Sr_{0.8}Bi_{2.4}Ta_2O_9(SBT)$ thin films are deposited on Pt-coated electrode($Pt/TiO_2/SiO_2/Si$) using RF magnetron sputtering method. With increasing post-annealing temperature from $600[^{\circ}C]$ to $850[^{\circ}C]$, Bi-layered perovskite phase was crystallized above $650[^{\circ}C]$. The maximum remanent polarization and the coercive electric field is 11.60[${\mu}C/cm^{2}$] 48[kV/cm] respectively. The leakage current density of SBT capacitor at post-annealing temperature of $750[^{\circ}C]$ is $1.01{\times}10^{-8}A/cm^2$ at 100[kV/cm]