• Carbon letters
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• 제14권4호
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• pp.234-242
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• 2013

Potassium hydroxide-activated carbons (CK21, CK11, and CK12) were prepared from pistachio nutshells. Physicochemical properties of activated carbons were characterized by TGA, $pH_{pzc}$, Fourier transform infrared spectroscopy, scanning electron microscopy, and $N_2$-adsorption at $-196^{\circ}C$. The examinations showed that activated carbons have high surface area ranging between 695-1218 $m^2/g$, total pore volume ranging between 0.527-0.772 mL/g, and a pore radius around 1.4 nm. The presence of acidic and basic surface C-O groups was confirmed. Batch adsorption experiments were carried out to study the effects of adsorbent dosage, temperature, initial concentration of adsorbate, and contact time on deltamethrin adsorption by activated carbons. The kinetic studies showed that the adsorption data followed a pseudo-second order kinetic model. The Langmuir model showed a maximum adsorption capacity of 162.6 mg/g at $35^{\circ}C$ on CK12. Thermodynamic studies indicated that adsorption was spontaneous and increased with temperature, suggesting an endothermic process.

• Carbon letters
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• 제14권4호
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• pp.251-254
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• 2013

In this study, poly(amic acid) was prepared via a polycondensation reaction of 3,3'-dihydroxybenzidine and pyromellitic dianhydride in an N-methyl-2-pyrrolidone solution; reduced graphene oxide/polybenzoxazole (r-GO/PBO) composite films, which significantly increased the electrical conductivity, were successfully fabricated. GO was prepared from graphite using Brodie's method. The GO was used as nanofillers for the preparation of r-GO/PBO composites through an in situ polymerization. The addition of 50 wt% GO led to a significant increase in the electrical conductivity of the composite films by more than sixteen orders of magnitude compared with that of pure PBO films as a result of the electrical percolation networks in the r-GO during the thermal treatment at various temperatures within the films.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.2
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• pp.1033-1036
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• 2004

Si nanocrystallites thin films on p-type (100) Si substrate have been fabricated by pulsed laser deposition using a Nd:YAG laser. After deposition, samples were annealed at the temperatures of 400 to $800^{\circ}C$. Hydrogen passivation was then performed in the forming gas (95% $N_2$ + 5% $H_2$) for 1 hr. Strong violet-indigo photoluminescence has been observed at room temperature from nitrogen ambient-annealed Si nanocrystallites. The variation of photoluminescence (PL) Properties of Si nanocrystallites thin films has been investigated depending on annealing temperatures with hydrogen passivation. From the results of PL, Fourier transform infrared (FTIR), and high-resolution transmission electron microscopy (HRTEM) measurements, it is observed that the origin of violet-indigo PL from the nanocrystalline silicon in the silicon oxide film is related to the quantum size effect of Si nanocrystallites and oxygen vacancies in the SiOx(x : 1.6-1.8) matrix affects the emission intensity.

• 유체기계공업학회:학술대회논문집
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• 유체기계공업학회 2000년도 유체기계 연구개발 발표회 논문집
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• pp.200-210
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• 2000

본 연구에서는 고속의 원심압축기에서 스톨 발단에 관한 연구를 수행하였다. 스톨을 일으키는 요인과, 스톨이 발생하기 전에 이를 미리 경고할 수 있는 방법을 주된 연구 주제로 삼았다. 원주방향으로 균일하게 분포된 8개의 고속응답 압력변환기를 사용하여 순간압력을 측정하였으며, 이 신호를 공간 푸리에 변환(space Fourier transform)을 사용하여 스톨의 발단을 알리는 신호를 측정하였고, 회전하는 파의 에너지(Traveling Wave Energy) 방법을 사용하여 스톨을 미리 경고하는 방법에 대하여 연구하였다. 회전하는 파의 에너지 방법은 스톨을 경고하는 데 좋은 성능을 보였으며, 저속에서는 약 임펠러 100회전, 중간속도에서는 약 200회전, 그리고 고속에서는 약 임펠러 1000회전의 경고시간을 보였다. 그리고 스톨 발단 근처에서 공간 푸리에 계수의 위상이 임펠러 주파수의 속도로 선형적인 증가를 보이는 구간이 나타났으며, 또한 임펠러 주파수의 스펙트럼이 스톨로 접근하면서 증가하는 것으로부터, 임펠러 주파수가 스톨을 일으키는 중요한 요인으로 작용함을 알 수 있었다. 또한 임펠러의 회전속도에 관계없이 스톨로 접근하면서 임펠러 주파수의 스펙트럼이 증가하므로, 이 값이 스톨을 경고하는 방법으로 사용될 수 있음을 보였으며, 약 임펠러 2n회전의 경고시간을 얻을 수 있었고, 임펠러의 속도가 빠를수록 긴 경고시간을 얻었다. 이 방법의 개발로 하나의 센서의 측정만으로도 효과적으로 스톨을 경고할 수 있는 기반을 마련하였다.

• 한국전산유체공학회지
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• 제18권2호
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• pp.78-84
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• 2013

In this paper, numerical simulations of both low- and high-frequency buzz phenomena at the throttle ratios (T.R.) in Nagashima's experiment are performed. The dominant frequencies of the low-and high-frequency buzz in the experiment are about 109 Hz with T.R.=0.97 and 376 Hz with T.R.=0.55, respectively. An axisymmetric solver with the S-A turbulence model is used for the simulations, and DFT(Discrete Fourier Transform) on pressure histories is conducted for the buzz frequency analysis. In the present simulations, the free-stream Mach number and the Reynolds number based on the inlet diameter are 2 and $10^7$, respectively. Both the low- and high-frequency buzz phenomena are accomplished without the changes in the grid topology. The dominant frequency of the simulation is about 125 Hz with T.R.=0.97, while it is 399 Hz with T.R.=0.55.

• 대한기계학회논문집
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• 제18권4호
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• pp.1050-1056
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• 1994

When a vibration data for a rotating machine such as a pump or a compressor is concerned, the frequency fluctuation of the energy contents at an instant time may provide useful information on understanding the vibration characteristics of the rotating machinery, rather than the averaged energy distribution along the frequency axis. Especially, when a periodic signal has different spectral contents, the approach to use the averaged frequency distribution, called the normal frequency analysis, may not be appropriate to extract vibration source characteristics of the structure. This paper introduces a way to analyze the signal based on an instant time. In order to evaluate the performance of the various approach, the investigatation compares three different algorithms which are frequently implemented in the instantaneous frequency analysis. Also for the noise effect embodied in the true signal, various cases for different SN ratio have been examined. The result shows that the noise level is crucial to evalute the instantaneous frequency analysis. In order to implement the instantaneous frequency analysis, the extraction of the relevant information from the measured signal should have the high S/N ratio, i, e., 40 dB or above.

• 한국지진공학회:학술대회논문집
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• 한국지진공학회 2001년도 추계 학술발표회 논문집 Proceedings of EESK Conference-Fall 2001
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• pp.36-43
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• 2001

In Korea, we are absolutely short of earthquake data in good quality from moderate and large earthquakes, which are needed fur the study of strong ground motion characteristics. This means that the best use of the available data is needed far the time being. In this respect, several methods are suggested in this paper, which can be applied in the process of data selection and analysis. First, it is shown that the calibration status of seismic stations can be easily checked by comparing the spectra from accelerometer and velocity sensor both of which are located at the same location. Secondly, it is recommended that S/N ratio in the frequency domain should be checked before discarding the data by only look of the data in time domain. Thirdly, the saturated earthquake data caused by ground motion level exceeding the detection limit of a seismograph are considered to see if such data can be used for spectrum analysis by performing numerical simulation. The result reveals that the saturated data can still be used within the dominant frequency range according to the levels of saturation. Finally, a technique to minimize the window effect that distorts the low frequency spectrum is suggested. This technique involves detrending in displacement domain once the displacement data are obtained by integration of low frequency components of the original data in time domain. Especially, the low frequency component can be separated by using discrete wavelet transform among many alternatives. All of these methods mentioned above may increase the available earthquake data and frequency range.

• 한국전기전자재료학회논문지
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• 제27권1호
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• pp.39-44
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• 2014

Silicon nitride thin film deposited with Plasma Enhanced Chemical Vapor Deposition was treated by a nitrogen plasma generated by Inductively Coupled Plasma at room temperature. The treatment was investigated by Fourier Transform Infrared Spectroscopy and Atomic Force Microscopy on the surface at various RF source powers at two RF bias powers. The amount of hydrogen was reduced and the surface roughness of the films was decreased remarkably after the plasma treatment. In order to understand the causes, we analyzed the plasma diagnostics by Optical Emission Spectroscopy and Double Langmuir Probe. Based on these analysis results, we show that the nitrogen plasma treatment was effective in the improving of the properties silicon nitride thin film for flexible display.

• 한국멀티미디어학회논문지
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• 제18권7호
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• pp.818-826
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• 2015

With the rapid interest in Geographic Information System (GIS) contents, a large volume of valuable GIS dataset has been distributed illegally by pirates, hackers, or unauthorized users. Therefore the problem focus on how to protect the copyright of GIS vector map data for storage and transmission. But GIS vector map data is very large and current data encryption techniques often encrypt all components of data. That means we have encrypted large amount of data lead to the long encrypting time and high complexity computation. This paper presents the selective encryption scheme using hybrid transform for GIS vector map data protection to store, transmit or distribute to authorized users. In proposed scheme, polylines and polygons in vector map are targets of selective encryption. We select the significant objects in polyline/polygon layer, and then they are encrypted by the key sets generated by using Chaotic map before changing them in DWT, DFT domain. Experimental results verified the proposed algorithm effectively and error in decryption is approximately zero.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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• pp.167.2-167.2
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• 2014

In this work, ZnO shell on mesoporous $SiO_2$ ($ZnO/SiO_2$) was prepared by atomic layer deposition (ALD). Diethylzinc (DEZ) and $H_2O$ were used as precursor of ZnO shell. $ZnO/SiO_2$ sample was characterized by X-ray diffraction (XRD), N2 sorption isotherms, X-ray photoelectron spectroscopy (XPS), Scanning electron microscopy (SEM) and Fourier-transform infrared spectroscopy (FT-IR). $ZnO/SiO_2$ showed higher adsorption capacity of MB than that of bare mesoporous $SiO_2$ and the adsorption capacities of $ZnO/SiO_2$ could be regenerated by UV exposure through the photocatalytic degradation of the adsorbed MB. This system could be used for removing organic dye from water by adsorption and reused after saturation of adsorption due to its photocatalytic regeneration.