• Journal of the Korean institute of surface engineering
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• v.39 no.3
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• pp.110-114
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• 2006

In this work, comparative studies on microstructure and mechanical properties between $Mo_2N$ and Mo-Si-N coatings were conducted. Ternary Mo-Si-N coatings were deposited on AISI D2 steel substrates by a hybrid method, where AIP technique was combined with a magnetron sputtering technique. Instrumental analyses of XRD, HRTEM, and XPS revealed that the Mo-Si-N coatings must be a composite consisting of fine $Mo_2N$ crystallites and amorphous $Si_3N_4$. The hardness value of Mo-Si-N coatings significantly increased from 22 GPa of $Mo_2N$ coatings to about 37 GPa with Si content of 10 at.% due to the refinement of $Mo_2N$ crystallites and the composite microstructure characteristics. The average friction coefficient of the Mo-Si-N coatings gradually decreased from 0.65 to 0.4 with increasing Si content up to 15 at.%. The effects of Si content on microstructure and mechanical properties of Mo-N coatings were systematically investigated.

• Journal of Korea Foundry Society
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• v.39 no.5
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• pp.87-93
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• 2019

The effects of mold materials on the microstructure and tensile properties were investigated to develop a mass production technique of aluminum alloy parts with excellent mechanical properties using a lost foam casting method. The microstructures of the plate-shaped cast alloy showed a tendency to be finer in proportion to the thickness of the plate, and a remarkably fine structure was obtained by applying a steel chill or a ball as a mold material compared to general sand. When a steel ball was used, it was observed that the larger the ball, the finer the cast structure and the better the tensile properties. The microstructure and tensile properties of the cast parts with complex shapes were greatly affected by the gating system, but the positive effects of the steel chill and the steel ball as a mold material were clear.

• Journal of the Korean Society for Heat Treatment
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• v.37 no.1
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• pp.9-15
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• 2024

Nd-Fe-B permanent magnets have been utilized on various industrial fields such as electric vehicles, generator, robots with actuator, etc, due to their outstanding magnetic properties even 10 times better than conventional magnets. Recently, there are many researches that report magnetic properties improved by controlling microstructure through adjusting alloying elements or conducting various processing. Especially, post-sintering annealing (PSA) can significantly improve the coercivity by modifying the distribution and morphology of Nd-rich phase which formed at grain boundaries. In this study, Nd-Fe-B sintered magnets were subjected to primary heat treatment followed by secondary heat treatment at 460℃, 500℃, and 540℃ to investigate the changes in microstructure and magnetic properties with the secondary heat treatment temperature. EBSD analysis was conducted to compare anisotropic characteristics. Through the SEM and TEM observation for analyzing the morphology and distribution of Nd-rich phase, we investigated the relationship between microstructure and magnetic properties of sintered Nd-Fe-B magnets.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.5
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• pp.219-225
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• 2020

The objective of this study was to investigate the tensile properties and thermal conductivities of Mg9.3%Al alloy in as-cast state and heat-treated state consisting of fully discontinuous precipitates (DPs), respectively. The fully DPs microstructure was obtained by solution treatment at 405℃ for 24 h, followed by furnace cooling to RT. The as-cast alloy showed a partially divorced eutectic β(Mg₁₇Al₁₂) phase particles formed along the α-(Mg) cell boundaries. The DPs had various apparent (α+β) interlamellar spacings, which is related to different transformation temperatures during the furnace cooling. The DPs microstructure exhibited better tensile strength than the as-cast one, resulting from the higher value of elongation in response to its more homogeneous microstructure. It is noticeable that the DPs microstructure had 12.4% higher thermal conductivity in average than the as-cast one between RT and 200℃. The XRD analyses revealed that the lower Al concentration in the α-(Mg) matrix may well be responsible for the better thermal conductivity of the DPs microstructure.

• Journal of the Korean Chemical Society
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• v.55 no.5
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• pp.819-823
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• 2011

The relationship between the microstructure, mechanical properties, and oxidation behavior of pitch-, polyacrylonitrile (PAN)-, and Rayon-based carbon fibers (CFs) has been studied in detail. Three types of carbon fiber were exposed to isothermal oxidation in air and the weight change was measured by thermogravimetric analyzer (TGA) apparatus. After activation energy was gained according to the conversion at reacting temperature, the value of specific surface area and the surface morphology was compared, and the reaction mechanism of oxidation affecting development of pores of carbon fibers was examined. This study will lead to a new insight into the relationship between the microstructure and mechanical properties of carbon fibers.

• Journal of the Korean Ceramic Society
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• v.32 no.4
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• pp.436-440
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• 1995

Effects of microstructure of two Mg-ferrite specimens with the same starting composition and relative density but with different grain size on B-H hysteresis loop, natural resonance frequency, and ferromagnetic resonance line width are reported. Such properties as B-H hysteresis loop, saturation magnetization, natural resonance frequency, and ferromagnetic resonance line width were influenced by the microstructure development during sintering. Large grain size specimen showed high saturation magnetization, low coercive force, low natural resonance frequency, and low ferromagnetic resonance line width compared with the specimen of small grain size. The main reason for the changes in properties can be explained by the variation in anisotropic characteristics due to Fe+2 content generated during sintering process.

• Transactions on Electrical and Electronic Materials
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• v.11 no.5
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• pp.216-221
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• 2010

The microstructure, electrical properties, and DC-accelerated aging behavior of the Zn-Pr-Co-Cr-Y-Er (ZPCC-YE) varistors were investigated for different amounts of erbium oxide ($Er_2O_3$). The microstructure consisted of zinc oxide grain and an intergranular layer ($Pr_6O_{11}$, $Y_2O_3$, and $Er_2O_3$-rich phase) as a secondary phase. The increase of $Er_2O_3$ amount decreased the average grain size and increased the sintered density. As the $Er_2O_3$ amount increased, the breakdown field increased from 5094 V/cm to 6966 V/cm and the nonlinear coefficient increased from 27.8 to 45.1. The ZPCC-YE varistors added with 0.5 to 1.0 mol% $Er_2O_3$ are appropriate for high voltage, with high nonlinearity and stability against DC-accelerated aging stress.

• Journal of the Korean Ceramic Society
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• v.53 no.6
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• pp.575-580
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• 2016

Microstructural design of ceramics has generally focused on information gathered at the micro- and macro-scales and related this to how specific properties could be improved. Ceramic processing serves as the key to optimizes the final microstructure. However, the advent of nano-scale microstructures and highly advanced characterization tools are forcing us to develop new knowledge of what is occurring not just at the micro-scale but also at the atomic level. Thus we are now beginning to be able to address how microstructure is influenced by events at the atomic scale using atomic scale images and data. Theoreticians have joined us in interpreting the mechanisms involved in the "microstructural" evolution at multiple scales and how this can be used to enhance specific properties of ceramics. The focus here is on delving into the various layers the "microstructure" in order understand how atomic-scale events influence the structure and properties of ceramics.

• Metals and materials international
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• v.24 no.6
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• pp.1359-1368
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• 2018

The mechanical properties and microstructure evolution of Mg-8Li-3Al-1Y alloy undergoing different rolling processes were systematically investigated. X-ray diffraction, optical microscope, scanning electron microscopy, transmission electron microscopy as well as electron backscattered diffraction were used for tracking the microstructure evolution. Tensile testing was employed to characterize the mechanical properties. After hot rolling, the $MgLi_2Al$ precipitated in ${\beta}-Li$ matrix due to the transformation reaction: ${\beta}-Li{\rightarrow}{\beta}-Li+MgLi_2Al+{\alpha}-Mg$. As for the alloy subjected to annealed hot rolling, ${\beta}-Li$ phase was clearly recrystallized while recrystallization rarely occurred in ${\alpha}-Mg$ phase. With regard to the microstructure undergoing cold rolling, plenty of dislocations and dislocation walls were easily observed. In addition, the microstructure of alloys subjected to annealed cold rolling revealed the formation of new fresh ${\alpha}-Mg$ grains in ${\beta}-Li$ phase due to the precipitation reaction. The mechanical properties and fracture modes of Mg-8Li-3Al-1Y alloys can be effectively tuned by different rolling processes.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2003.10a
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• pp.60-63
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• 2003

Semi-solid forming is the process of stirring alloy during solidification, making the mixture of liquid and solid, solidifying it, reheating it to the solid-liquid coexistent temperature, and then injecting this semi solid slurry into dies. In the semi-solid die casting process, it is very important to find out the correlation of injection condition, microstructure and mechanical properties. Especially, an improper injection condition is the main cause of liquid segregation and non-homogeneous mechanical properties due to the difference of solid fraction according to the position of the products. To ensure the database requisite to the semi-solid die casting product, it is essential to acquire the mechanical properties considering liquid segregation to the injection condition. In this study, the effect of injection condition on liquid segregation, formability, microstructure and mechanical properties in a thin product was investigated.