• Title/Summary/Keyword: Microstructure properties

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Effect of Cr2O3 Content on Densification and Microstructural Evolution of the Al2O3-Polycrystalline and Its Correlation with Toughness

  • Seo, Mi-Young;Kim, Hee-Seung;Kim, Ik-Jin
    • Journal of the Korean Ceramic Society
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    • v.43 no.8 s.291
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    • pp.469-471
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    • 2006
  • The effects of $Cr_2O_3$ on the microstructural evolution and mechanical properties of $Al_2O_3$ polycrystalline were investigated. The microstructure of $Al_2O_3-Cr_2O_3$ composites (ruby) was carefully controlled in order to obtain dense and fine-grained ceramics, thereby improving their properties and reliability with respect to numerous applications related to semiconductor bonding technology. Ruby composites were produced by Ceramic Injection Molding (CIM) technology. Room temperature strength, hardness, Young's modulus and toughness were determined, as well as surface strengthening induced by thermal treatment and production of a fine-grained homogenous microstructure.

Effects of Niobium Microalloying on Microstructure and Properties of Hot-Dip Galvanized Sheet

  • Mohrbacher, Hardy
    • Corrosion Science and Technology
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    • v.9 no.2
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    • pp.67-73
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    • 2010
  • Niobium microalloying is effective in hot-rolled and cold-rolled steels by providing a fine-grained microstructure resulting in increased strength. To optimize the strengthening effect, alloy design and hot-rolling conditions have to be adapted. As a key issue the dissolution and precipitation characteristics of Nb are discussed in particular with regard to the run-out table conditions. It is then considered how the hot-rolled microstructure and the solute state of Nb interact with the hot-dip galvanizing cycle. The adjusted conditions allow controlling the morphology and distribution of phases in the cold-rolled annealed material. Additional precipitation hardening can be achieved as well. The derived options can be readily applied to produce conventional HSLA and IF high strength steels as well as to modern multiphase steels. It will be explained how important application properties such as strength, elongation, bendability, weldability and delayed cracking resistance can be influenced in a controlled and favorable way. Examples of practical relevance and experience are given.

Bending Strength and Microstructure of Cement Paste Containing SWCNT Dispersion Solution (SWCNT 분산용액을 혼입한 시멘트 페이스트의 휨강도 및 미세구조)

  • Choi, Ik-Je;Kim, Ji-Hyun;Lee, Soo-Yong;Chung, Chul-Woo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.11a
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    • pp.149-150
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    • 2017
  • It is known that physical and chemical changes of cement hydrates cause problems in the volume stability of concrete. In order to overcome these problems, there is a growing interest in research on mixing technology of cement-based materials and nanomaterials. Among the nanomaterials, carbon nanotubes (CNTs) are attracting attention due to their excellent mechanical properties. The CNTs are made of cylindrically shaped graphene sheets. According to the number of sheets, single-walled carbon nanotubes (SWCNTs) and multi-walled carbon nanotubes (MWCNTs) are classified. Although the SWCNT has superior mechanical properties, the research using MWCNT is vigorous due to the difficulty of marketability and manufacturing, but the research using SWCNT is insufficient. In this study, we investigate the effect of SWCNT on the formation of hydrate of cement paste by observing the microstructure of broken cement paste after measuring the flexural strength of cement paste with SWCNT dispersion.

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Effects of Patenting Temperature on the Bending Fatigue Resistance of the Steel Filaments used for Automotive Tire (열처리 조건에 따른 미세 강선의 굽힘 피로 특성 변화)

  • Yang, Y.S.;Bae, J.G.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.454-457
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    • 2008
  • Effects of patenting temperature on bending fatigue resistance of pearlitic steel filaments were investigated experimentally. The fatigue resistance of steel filaments was carried out by using hunter machine, specially designed for ultra fine-sized steel wires, in the controlled conditions. The transmission electron microscopy (TEM) was used for observing the overall microstructure. It revealed that the fatigue resistance as well as tensile strength increased together with increase of patenting temperature from 510 to $600^{\circ}C$, while the endurance ratio ($\sigma_e/\sigma_{TS}$) of filaments decreased. It is believed that this variation of mechanical properties with change of patenting temperature should be strongly influenced by the change of microstructure. The bending fatigue properties of steel filaments were discussed based on microstructural parameters.

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The Expectation for Material Properties of Microstructure by Application of Dynamic Response Characteristics (동적 응답 특성을 활용한 미세구조의 물성 분포에 대한 예측)

  • Lee, Jeong-Ick;Yeo, Moon-Su
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.3
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    • pp.580-586
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    • 2008
  • This paper addresses the prediction of the material property continuities of a microstructure. Prediction was made by measuring the dynamic responses distribution of the fabricated materials used in the microstructures. When these distributional material properties were used in estimating the mechanical performances of microstructures, the differences between the computer simulation and the experimental result of microstructures could be reduced and their reliability design could be made.

Effect of Fe Addition on Mechanical Properties and Microstructure of As-Extruded Hypereutectic Al-Si-Fe Alloy (Fe가 첨가된 과공정 Al-Si-Fe합금 압출재의 기계적특성 및 미세조직에 관한 연구)

  • Lee, S.D.;Kim, D.H.;Beck, A.R.;Lim, S.G.
    • Transactions of Materials Processing
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    • v.28 no.3
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    • pp.123-129
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    • 2019
  • Hypereutectic Al-Si alloys have been widely utilized for wear-resistant components in the automotive industry. In order to expand the application of Hypereutectic Al-Si alloys, the addition of alloying elements forming a stable precipitate at high temperature is required. Thermally stable inter metallic compounds can be formed through the addition of transition elements such as Fe, Ni to Al alloys. However, the amount of transition element to be added to Al alloys is limited due to their low solid solubility. Also, hypereutectic Al-Si-Fe alloys form coarse primary Si phases and needle-shaped intermetallic compounds during solidification in the general casting processes. In this study, the effects of the destruction of Intermetallic compound and Si phase are investigated via hot extrusion. Both the microstructure and mechanical properties are discussed under different extrusion conditions.

Influence of Al, Cu and Ni Additions on Mechanical Properties of Hot-Rolled Fe-9Mn-0.2C Medium-Manganese Steels

  • Young-Chul Yoon;Sang-Gyu Kim;Sang-Hyeok Lee;Byoungchul Hwang
    • Archives of Metallurgy and Materials
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    • v.66 no.4
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    • pp.1007-1011
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    • 2021
  • The microstructure and mechanical properties of hot-rolled Fe-9Mn-0.2C medium-manganese steels with different Al, Cu, and Ni contents were investigated in this study. Based on the SEM, XRD, and EBSD analysis results, the microstructure was composed of martensite, band-type delta ferrite, and retained austenite phases depending on the Al, Cu, and Ni additions. The tensile and Charpy impact test results showed that the sole addition of Al reduced significantly impact toughness by the presence of delta-ferrite and the decrease of austenite stability although it increased yield strength. However, the combined addition of Al and Cu or Ni provided the best combination of high yield strength and good impact toughness because of solid solution strengthening and increased austenite stability.

Effects of Tempering Treatment on Microstructure and Mechanical Properties of Cu-Bearing High-Strength Steels (템퍼링에 따른 Cu 첨가 고강도강의 미세조직과 기계적 특성)

  • Lee, Sang-In;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.24 no.10
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    • pp.550-555
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    • 2014
  • The present study deals with the effects of tempering treatment on the microstructure and mechanical properties of Cu-bearing high-strength steels. Three kinds of steel specimens with different levels of Cu content were fabricated by controlled rolling and accelerated cooling, ; some of these steel specimen were tempered at temperatures ranging from $350^{\circ}C$ to $650^{\circ}C$ for 30 min. Hardness, tensile, and Charpy impact tests were conducted in order to investigate the relationship of microstructure and mechanical properties. The hardness of the Cu-added specimens is much higher than that of Cu-free specimen, presumably due to the enhanced solid solution hardening and precipitation hardening, result from the formation of very-fine Cu precipitates. Tensile test results indicated that the yield strength increased and then slightly decreased, while the tensile strength gradually decreased with increasing tempering temperature. On the other hand, the energy absorbed at room and lower temperatures remarkably increased after tempering at $350^{\circ}C$; and after this, the energy absorbed then did not change much. Suitable tempering treatment remarkably improved both the strength and the impact toughness. In the 1.5 Cu steel specimen tempered at $550^{\circ}C$, the yield strength reached 1.2 GPa and the absorbed energy at $-20^{\circ}C$ showed a level above 200 J, which was the best combination of high strength and good toughness.

Effect of Sintering Temperature and Sb/Bi Ratio on Microstructure and Grain Boundary Properties of ZnO-Bi2O3-Sb2O3-Co3O4 Varistor (소결온도와 Sb/Bi 비가 ZnO-Bi2O3-Sb2O3-Co3O4 바리스터의 미세구조와 입계 특성에 미치는 영향)

  • Hong, Youn-Woo;Shin, Hyo-Soon;Yeo, Dong-Hun;Kim, Jin-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.12
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    • pp.969-976
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    • 2011
  • In this study we aims to evaluate the effects of 1/3 mol% $Co_3O_4$ addition on the reaction, microstructure development, resultant electrical properties, and especially the bulk trap and grain boundary properties of $ZnO-Bi_2O_3-Sb_2O_3$ (Sb/Bi=2.0, 1.0, and 0.5) system (ZBS). The samples were prepared by conventional ceramic process, and characterized by XRD, density, SEM, I-V, impedance and modulus spectroscopy (IS & MS) measurement. In addition of $Co_3O_4$ in $ZnO-Bi_2O_3-Sb_2O_3$ (ZBSCo), the phase development, density, and microstructure were controlled by Sb/Bi ratio. Pyrochlore on cooling was reproduced in all systems. The more homogeneous microstructure was obtained in ZBSCo (Sb/Bi=1.0) system. In ZBSCo, the varistor characteristics were improved drastically (non-linear coefficient ${\alpha}$=23~50) compared to ZBS. Doping of $Co_3O_4$ to ZBS seemed to form $V^{\cdot}_o$(0.33 eV) as dominant defect. From IS & MS, especially the grain boundary of Sb/Bi=0.5 system is composed of electrically single barrier (0.93 eV) and somewhat sensitive to ambient oxygen with temperature.