• Title/Summary/Keyword: Microscopic interface

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Structural Analysis of Low Temperature Processed Schottky Contacts to n-InGaAs (저온공정 n-InGaAs Schottky 접합의 구조적 특성)

  • 이홍주
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.14 no.7
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    • pp.533-538
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    • 2001
  • The barrier height is found to increase from 0.25 to 0.690 eV for Schottky contacts on n-InGaAs using deposition of Ag on a substrate cooled to 77K(LT). Surface analysis leads to an interface model for the LT diode in which there are oxide compounds of In:O and As:O between the metal and semiconductor, leading to behavior as a metal-insulator-semiconductor diode. The metal film deposited t LT has a finer and more uniform structure, as revealed by scanning electron microscopy and in situ metal layer resistance measurement. This increased uniformity is an additional reason for the barrier height improvement. In contrast, the diodes formed at room temperature exhibit poorer performance due to an unpassivated surface and non-uniform metal coverage on a microscopic level.

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A study on characteristic adgesive condition at microscopic interfaces and notch shape strength of GFRP composites laminates under low-hot-wet environment (저온.고온고습 환경시험에 의한 GFRP의 미시계면 접착상태 및 노치형상강도 특성에 관한 연구)

  • 김옥만;박귀성;한길영;이동기;김이곤
    • Journal of Ocean Engineering and Technology
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    • v.10 no.4
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    • pp.58-66
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    • 1996
  • The purpose of this investigation is to estimate the strength with the variations of the notch shape and the adgesive condition at the fiber/matrix micro interface of E-glass/PP laminates. To promote the degradation of the adhesive condition at the fiber/matrix micro interface without matrix dissolution loss, low-, hot-wet and spiking tests were carried out. The absorpotion properties and the tensile properties were compared accrding to the fiber orientation and the content. The results show that, firstly, saturated moisture absorption was reached at 5cycles and their absorptions of RD-40, UD-42 and UD-50 are 0.68%, 0.63%, 0.60%, respectively. Secondly, all the specimens investigated were mostly degraded at 5cycle, whereas UD-50 having ellipse shaped notch the least decrement of strength.

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Interface between the Electroplated Copper-cobalt Thin Films and the Substrate

  • Kim, Jin-Gyu;Lee, Jung-ju;Bae, Jong-hak;Bang, Won-bae;Hong, Kim-in;Yoon, C. H.;Son, Derac;Jeong, Kee-ju
    • Journal of Magnetics
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    • v.11 no.3
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    • pp.119-122
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    • 2006
  • We electroplated copper-cobalt thin films on a silicon substrate, which had 150 nm thick copper seed layer. The adhesion between the two metallic layers could be increased by utilizing a proper organic additive, pulse plating technique, and high temperature annealing. The thin films exhibited columnar growth of the deposits and enhanced adhesion. This is attributed to the grain growth mechanism introduced by the additive and annealing.

Development of Solar Energy Concentration for Plastic Joining

  • Yarlagadda, P.;Kim, I.S.
    • International Journal of Korean Welding Society
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    • v.2 no.1
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    • pp.57-61
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    • 2002
  • This paper presents development of a SEC(Solar Energy Concentration) utilizing the concentrated solar beam radiation for joining engineering thermoplastics such as Acrylonitrile/Butadiene/Styrene(ABS), Polycarbonate(PC) and Polymethylmethacrylate (PMMA). In addition, to study the joining of the materials, necessary experimentation with applying primer was performed. Tensile tests were conducted to determine the bond strength achieved at the specimen Joint interface. Microscopic examinations of the fractured joints were performed in order to analyze the overall bond quality. Finally, the results in terms of bond strength achieved at the joint interface and energy consumed in the process was compared with those obtained with similar thermoplastic joining technique utilizing microwave energy.

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Effect of Slag Particle Size and Volume Fraction on Mechanical Properties of Slag Reinforced Composite (슬래그 입자의 크기 및 체적비에 따른 슬래그 입자강화 복합재료의 기계적 특성 연구)

  • Nam, Ji-Hoon;Chun, Heoung-Jae;Hong, Ik-Pyo
    • Composites Research
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    • v.26 no.4
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    • pp.218-222
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    • 2013
  • This study demonstrated that a slag, an industrial solid waste, can be used as a structural reinforcement. The mechanical properties(tensile strength and Elastic modulus) of slag reinforced composite(SRC) was investigated as functions of slag particle size (8~12 ${\mu}m$ and 12~16 ${\mu}m$) and volume fraction (0-40 vol.%). In order to investigate the interface and a degree of particle dispersion which have an effect on mechanical properties, optical microscopic images were taken. The results of tensile tests showed that the tensile strength decreased with an increase in slag volume fraction and particle size. The elastic modulus increased with an increase in slag volume fraction and particle size except for 30 vol.% SRC. The tensile strength decreased with an increase in slag particle size. The microscopic picture showed SRC has fine degree of particle dispersion at low slag volume fraction. SRC has a good interface at every volume fraction. However particle cluster was incorporated with an increase in slag volume fraction.

HISTOLOGIC COMPARATIVE STUDY ON THE BONE-IMPLANT INTERFACE OF HYDROXYLAPATITE AND TITANIUM PLASMA SPRAY COATED IMPLANTS (Hydroxylapatite 및 Titanium Plasma Spray 피복임프란트와 골조직 계면의 조직학적 비교 연구)

  • Cho, Ju-Oh;Song, Kwang-Yeob;Park, Charm-Woon
    • The Journal of Korean Academy of Prosthodontics
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    • v.33 no.3
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    • pp.492-516
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    • 1995
  • This study evaluated the responses of mandibular bones of mongrel dogs to loaded hydro xylapatite(HA) and titanium plasma spray(TPS) coated endosseous dental implants, using unloaded ones as the control group. after HA and TPS coated implants were implanted, their bone reactions with vital bones have been observed with light and scanning electron microscope(SEM) at the three periods of the 4th, 12th and 20th week. These reactions have been also compared in a histomorphometric method. The elemental distribution state of implants and the interface neighboring bone tissues have been measured with the energy dispersive analysis of X-rays(EDAX). The following results were obtained ; 1. The light microscopic analysis showed osseointegration in both the control group and the occlusal force loaded group ; Its degree was shown to be higher in the long-maintained and occlusal force groups. 2. The SEM analysis showed that both groups had osseointegration, In the case of TPS-coated implants, the coated layer was divided on the bone interface. In the case of HA-coated implants, there appeared a division between the metal and coated interface. 3. In the histomorphometric analysis, the measured ratio contaction bone of TPS-coated implants was $70{\pm}19$% in the case of no occlusal force ; it was $84{\pm}13$% in the case of occlusal force. The measured ratio contacting bone of HA-coated implants was $75{\pm}18$% in the case of no occlusal force ; it was $94{\pm}9$% in the case of occlusal force. However, there was no significant difference statistically(p>0.05). 4. Both groups showed that the ratio of calcium and phosphorous increased more in the bone tissues than on the bone to implant interface.

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Impact analysis of composite plate by multiscale modeling (멀티스케일 모델링에 의한 복합재료 평판의 충격해석)

  • Ji Kuk Hyun;Paik Seung Hoon;Kim Seung Jo
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.04a
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    • pp.67-70
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    • 2004
  • An investigation was performed to study the impact damage of the laminated composite plates caused by a low- velocity foreign object with multi-scale modeling based on the concepts of Direct Numerical Simulation (DNS)[4]. In the micro-scale part, we discretize the composite plates through separate modeling of fiber and matrix for the local microscopic analysis. A micro-scalemodel was developed for predicting the initiation of the damage and the extent of the final damage as a function of material properties, laminate configuration and the impactor's mass, etc. Anda macro-scale model was developed for description of global dynamic behavior. The connection betweenmicroscopic and macroscopic is implemented by the tied interface constraints of LS-DYNA contact card. A transient dynamic finite element analysis was adopted for calculating the contact force history and the stresses and strains inside the composites during impact resulting from a point-nose impactor. The low-velocity impact events such as contact force, deformation, etc. are simulated in the macroscopic sense and the impact damages, fiber-breakage, matrix cracking and delamination etc. are examined in the microscopic sense.

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Localized Corrosion Behavior of Inconel 718 in a Chloride-Containing Aqueous Solution (염수 환경에서 Inconel 718의 국부 부식 거동)

  • Lee, Jun-Seob;Lee, Yejin;Kwon, Soon il;Shin, Jungho;Lee, Je-Hyun
    • Corrosion Science and Technology
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    • v.20 no.6
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    • pp.361-366
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    • 2021
  • Localized corrosion behavior of Ni-based Inconel 718 alloy was investigated by electrochemical anodic polarization techniques in NACE TM 0177 A solution of 5 wt% NaCl + 0.5 wt% acetic acid at room temperature. After the solution heat treated at 1080 ℃ for 2.5 h, Inconel 718 was age-hardened at 780 ℃ for 8 h. The microstructure of the alloy surface was investigated by optical microscopic or scanning electron microscopic technique. The austenitic phase with the presence of metal carbides was observed on the surface of Inconel 718. Metal-carbides such as Nb-Mo and Ti-carbide with diameters of approximately 10 and 3 ㎛, respectively, were formed in Inconel 718. Anodic polarization results revealed that localized corrosion was observed at the interface between austenitic phase of a substrate and metal carbides. Difference in electrochemical property between a metal carbide and an austenitic substrate could provide an initiation site for localized corrosion of Inconel 718 surface.

A HISTOLOGIC STUDY OF THE OSSEOINTEGRATION PROCESS TO THE TITANIUM TOOTH ROOT IMPLANT (타이타늄 치근형 매식체에 대한 골유착 과정에 관한 조직학적 연구)

  • Ahn, Chang Young;Kim, Yung Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.2
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    • pp.1-28
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    • 1990
  • The severe atrophic edentulism with poor neuromuscular control militates against successful conventional denture therapy. To such situation, a prescribing of dental implant treatment has been considered with some probability. Implant materials used as a trial for dental implants includes metals, plastic polymers and ceramics. The purpose of this study was to observe histologic response in osseointegration process at titanium implant-tissue interface based on biocompatibility at specific period of sequential natures which were divided into a half month, one, month, two months, three months and immediate as a base line. In this study, unilateral lower left premolar and molar teeth were extraced in three dogs. After allowing to heal for 6 months, three kinds of osseointegrated implant, $Br{\aa}nemark$, Corevent and kimplant(a prototype of SNU implant study)were inserted in each dog respectively according to the above sequence from front to back. The specimens were taken from those dogs at the same time since implant were inserted quite reverse order of the specified periods, and decalcified and processed for histologic examination for the light microscopy and the electron microscopy. The microscopic histologic findings at the interface between titanium implants and tissue were interpretated as follows : A. Light microscopic findings : a. Immediate : Implant were surrounded by compact bone and spongy bone. Microcrak was observed in the superficial bone tissue. Osteocytes were disappeared and bone lacunae were observed as a vacant space in some parts. In the contacting with the spongy bone, bone trabeculae and bone marrow were in contact with the implant. b. A half Month : Osteoblasts exist as a monolayer in th inner bone trabeculae and do bone additiocn. Osteoblasts&inflammatory cells were observed in some parts. c. One Month : The presence of osteoclasts decreased. Osteoblasts did active bone fromation, and bone marrow was in contact with the implant in the many places. d. Two Months : Bone formation was advanced in comparison with the b and c. The presence of osteoclsts was not observed. e. Three Months : The superficial bone tissue contacted with the implants was entirely composed by the compact bone. B. Electron microscopic findings : a. A half month and one month group : In the parts of the active bone formation, osteoblasts with the well developed endoplasmic reticulum and Golgi apparatus were arranged in the monolayer. In the parts of the bone resorption, ruffled border was well developed and many osteoclasts with the well-developed golgi apparatus, mitochondria, vacuole, vesicle and lysosome were existed. b. Three months group : No osteoblasts were observed in the superficial bone tissue. Bone matrix with collaen fiber was observed. c. No significant dirrerence in the histologic findings was observed in $Br{\aa}nemark$, Core-vent and kimplant.

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Electron Microscopic Study of Osseointegration between Bone and Smooth Machined Implants (선반가공 임플란트와 골조직의 유착에 관한 전자현미경적 연구)

  • Chang, Byung-Soo
    • Applied Microscopy
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    • v.34 no.4
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    • pp.277-283
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    • 2004
  • This paper reports that the ultrastructural nature of the interface process between the implants and surrounding bone has been studied after in vivo 1, 4, 8, 12 weeks of implantation of smooth machined implants into rabbit tibias. There was no indication of the fibrous connective tissue formation around the implant that imply intolerance of the bone tissue towards the implant after 1 week of implantation. The regions showing direct bone tissue bonding to the smooth machined implant contained osteoblast activating across the interface in the direction after 4 weeks of implantation. The reaction of a smooth machined implant caused in the first instance formation of an amorphous woven bone, which transformed into a mineralized bone containing collagen fibers. After 8 weeks of implantation, the activities of osteoblast initiated osseointegration forming bone matrix at the interface. During this period, the osteoblast surrounded with a matrix consisting of collagen bundles running in various directions. In the interface area between newly formed bone tissue and implants which has been inserted in rabbit tibias for 12 weeks, the implant and mineralized bone was separated by an amorphous electron dense material layer about $1{\sim}1.5{\mu}m$ in thickness.