• Title/Summary/Keyword: Micro-tensile test

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The Effect of Hydrogen on Mechanical Properties of Gas Pipeline Material: I Tensile property (가스배관 재료의 기계적특성에 미치는 수소의 영향: I 인장특성)

  • Kim, Woo-Sik;Jang, Jae-Il
    • Journal of the Korean Institute of Gas
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    • v.15 no.3
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    • pp.67-73
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    • 2011
  • One of the important topics to prepare the up-coming era of so-called ‘hydrogen economy’ is hydrogen transmission. Pipeline is conceivably the most economic way to consistently and safely transport a large amount of hydrogen over a long distance, which may be strongly requested in hydrogen economy era. As a good starting point for the purpose, one might wonder whether conventional API pipeline steels as designed for natural gas transmission can be used as the hydrogen pipeline materials or not. To answer the question, here we performed a series of micro-/nano-indentations together with tensile tests on the hydrogen-charged API X65, X70 and X100 steels having different strength level. In this paper, from the results of tensile tests, the hydrogen effects on the mechanical behavior in the API steels are systematically evaluated.

Biocompatibility of 13-93 Bioactive Glass-SiC Fabric Composites

  • Park, Jewon;Na, Hyein;Choi, Sung-Churl;Kim, Hyeong-Jun
    • Journal of the Korean Ceramic Society
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    • v.56 no.2
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    • pp.205-210
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    • 2019
  • Bioactive glass (BG) finds limited use as a bone replacement material owing to its low mechanical properties. In order to solve this problem, the micro-sized 13-93 BG was prepared as a fabric composite with SiC microfibers, and its mechanical properties and biocompatibility were investigated in this study. The tensile strengths of BG-SiC fiber-bundle composites increased in proportion to the number of SiC fibers. In particular, even when only one SiC fiber was substituted, the tensile strength increased by 81% to 1428 MPa. In the early stage of the in-vitro test, a silica-rich layer was formed on the surface of the 13-93 BG fibers. With time, calcium phosphate grew on the silica-rich layer and the BG fibers were delaminated. On the other hand, no products were observed on the SiC fibers for 7 days, therefore, SiC fibers are expected to maintain their strength even after transplantation in the body.

A Study on Degradation Characteristic of High Strength Fire Resistance Steel for Frame Structure by Acoustic Emission (음향방출법에 의한 고강도 구조요 내화강의 열화특성에 관한 연구)

  • 김현수;남기우;강창룡
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2000.04a
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    • pp.51-56
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    • 2000
  • Demand for new nondestructive evaluations is growing to detect tensile crack growth behavior to predict long term performance of materials and structure in aggressive environments, especially when they are in non-visible area. Acoustic emission technique is well suited to these problems and has drawn a keen interests because of its dynamic detection ability, extreme sensitivity and location of growing defects. In this study, we analysed acoustic emission signals obtained in tensile test of high strength fire resistance steel for frame structure with time frequency analysis methods. The results obtained are summaries as follows ; In the T and TN specimen consisting of ferrite and pearlite grains, most of acoustic emission events were produced near yield point, mainly due to the dislocation activities during the deformation. However, B specimen under $600^{\circ}C$ - 10min had a two peak which was attribute to the presence of martensite phase. The first peak is before yield point the second is after yield point. The sources of second acoustic emission peak were the debonding of martensite-martensite interface and the micro-cracking of brittle martensite phase. In $600^{\circ}C$-30min to $700^{\circ}C$-60min specimens, many signals were observed from area before yield point and counts were decreased after yield point.

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Sensing and Interfacial Evaluation of Ni Nanowire Strands/Polymer Composites using Electro-micromechanical Technique (Electro-Micromechanical 시험법을 이용한 Ni Nanowire Strands 강화 고분자 복합재료의 Sensing과 계면 물성 평가)

  • Kim, Sung-Ju;Jung, Jin-Gyu;Park, Joung-Man
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.141-144
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    • 2005
  • Sensing and interfacial evaluation of Ni nanowire strands/polymer composites were investigated using Electro-micromechanical technique. Electro-micromechanical techniques can be used as sensing method for micro damage, loading, temperature of interfacial properties. Using Ni nanowire strands/silicone composites with different content, load sensing response of electrical contact resistivity was investigated under tensile and compression condition. The mechanical properties of Ni nanowire strands with different type/epoxy composites were measured using uniformed cyclic loading and tensile test. Ni nanowire strands/epoxy composites showed humidity and temperature sensing within limited ranges, 20 vol% reinforcement. Some new information on temperature and humidity sensing plus loading sensing of Ni nanowire strands/polymer composites could be obtained from the electrical resistance measurement as a new concept of the nondestructive interfacial evaluation.

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A study on electromechanical properties of CNT conductive film deposited on flexible substrate (유연 모재 위에 증착된 CNT 전도성 필름의 전기-기계적 특성에 대한 연구)

  • Song, Sun-Ah;Kim, Jae-Hyun;Lee, Hak-Joo;Song, Jin-Woo;Chang, Won-Seok;Han, Chang-Soo
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.35-39
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    • 2008
  • In this study, electromechanical properties of carbon nanotube (CNT) thin film on flexible substrates were measured using a micro-tensile machine with functionality of simultaneous measurements of displacement, load and electrical resistance. The CNT thin film of about 100 nm thick was deposited on flexible substrates, polyethylene terephthalate (PET) using spraying and ink-jetting techniques. To investigate the effect of process condition on the electromechanical properties of CNT thin film, sets of CNT samples were fabricated under various heat treatments and microwave process. The microstructures of the CNT thin film before and after tensile test were investigated using Scanning Electron Microscope (SEM), and the failure modes of the CNT thin films were identified to understand their electromechanical behaviors and interaction with the flexible substrates. Based on the experimental results, the use of CNT thin film as flexible electrodes and strain gages is discussed.

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Squeeze Casting of SiC Whisker Reinforced Magnesium Composites (용탕단조를 이용한 SiC 휘스카 강화 마그네슘복합재료의 제조)

  • Chang, Si-Young;Shin, Dong-Hyuk;Hong, Sung-Kil;Choi, Jung-Chul
    • Journal of Korea Foundry Society
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    • v.20 no.3
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    • pp.167-172
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    • 2000
  • Squeeze casting was performed to fabricate the SiC whisker reinforced magnesium matrix composites, and the suitability of the squeeze casting for the production of the sound composites was determined by micro/macro-structures observations and tensile test. The two-directional infiltration of the melt and the removal of air during infiltration using the devised mold were necessary to produce the composites. The pressure of 100 MPa was effective for the production of composites with the SiC whisker volume fraction of 30%, but the pressure should be lower than 50 MPa in case of below 20% in the volume fraction. The SiC whiskers in the squeeze cast composites were randomly and densely aligned, and the SiC whiskers/magnesium interfaces were continuously well-bonded. The elastic modulus, 0.2% proof stress and tensile strength in the composite were about 2.5times, l0times and 4times as large as those of magnesium, respectively, indicating that the squeeze casting sufficiently provides the high strength magnesium composites reinforced with SiC whiskers.

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Mechanical Properties of Austempered Fe-2.0wt.%Si-0.3wt.%Mn Steel with various Carbon Contents (탄소함량 변화에 따른 오스템퍼드 Fe-2.0wt.%Si-0.3wt.%Mn 강의 기계적 성질)

  • Ha, Jong-Gyu;Shin, Sang-Yun;Lee, Do-Hoon;Ye, Byung-Joon
    • Journal of Korea Foundry Society
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    • v.35 no.1
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    • pp.1-7
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    • 2015
  • In this study, we investigated the effect of carbon on mechanical properties with different austempering conditions of high carbon(0.7~1.3wt.%C)-2.0wt.%Si steels. The specimens were austenitized at 850, 925 and $1020^{\circ}C$, and austempered at 260, 320 and $380^{\circ}C$ for the various period of time from 3 min to 300 min. After heat treatment, the evolution of stage I and stage II was identified with optical microscope, XRD and hardness test. When the austempering temperature was $260^{\circ}C$, the microstructure consisted of the lower ausferrite while the upper ausferrite micro-structure was formed at $380^{\circ}C$. As the austempering temperature increases from 260 to $380^{\circ}C$, the tensile strength decreases and elongation increases. In addition, when carbon content increases, tensile strength and elongation decrease.

Carbonation Behavior Evaluation of OPC Concrete Considering Effect of Aging and Loading Conditions (재령 및 하중효과를 고려한 OPC 콘크리트의 탄산화 거동 평가)

  • Hwang, Sang-Hyeon;Yoon, Yong-Sik;Kwon, Seung-Jun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.1
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    • pp.122-129
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    • 2019
  • The movement of deterioration agents such as a chloride ion, etc. in concrete varies with loading conditions and micro-structure developed by age effect. In this paper, the carbonation behavior by accelerated carbonation test is evaluated considering curing periods(28 days, 91 days, and 365 days) and loading conditions. Carbonation velocity coefficients are obtained referred to KS F 2584. In the control case without loading condition, carbonation velocity coefficient of 91 days decreases to 50.0 % level and that of 365 days decreases to 44.8 % level than that of 28 days curing condition. In 28 curing days, carbonation velocity coefficients changed level of 103.9 ~ 108.8 % in tensile region and 91.9~104.6 % in compressive region by loading conditions. Carbonation velocity coefficients in the 30 % and 60 % tensile loading case at 28 days decreases to 47.3 % and 52.5 % level compared to control case after 1 year. Furthermore, 45.8 % and 44.9 % level of carbonation velocity coefficients are evaluated for 30 % and 60 % compressive loading conditions compared to control case after 1 year. Carbonation velocity coefficient decreases in the 30 % compressive loading level due to effective pore compaction and it increases afterwards due to micro-cracking. In the tensile loading condition, unlike the behavior of compressive region, it linearly increases with increasing loading level.

Change of Mechanical Properties of Clad Steel According to the Welding Process Design (용접 공정 디자인에 따른 클래드강의 기계적 성질 변화)

  • Lee, Jung-Hyun;Park, Jaw-Won
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.3
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    • pp.372-379
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    • 2013
  • In this study, we investigated the traits of the clad metals used in hot-rolled clad steel plates. We examined the sensitization and mechanical properties of STS 316 steel plate and carbon steel (A516) under the specific circumstances of post heat treatment and whether a weld was multilayered and thick or repeated because of repairs. The test conditions were as follows. The clad steel plates were butt-welded using FCAW/SAW, and the heat treatment was conducted at $625^{\circ}C$, for 80, 160, 320, 640, or 1280 min. The change in the corrosion resistance was evaluated in these specimens. In the case of the carbon steel (A516), as the heat treatment time increased, the annealing effect caused the tensile strength to decrease. The micro- hardness gradually increased and then decreased after 640 min. The elongation and contraction of the area increased gradually. An oxalic acid etch test and EPR test on STS316, a clad metal, showed a STEP structure and no sensitization. From the test results for the multi-layered and repair welds, it could be concluded that there is no effect on the corrosion resistance of clad metals. In summary, the purpose of this study was to suggest some considerations when developing on-site techniques and evaluate the sensitization of stainless steels.

Mechanical and wear properties evaluation of Al/Al2O3 composites fabricated by combined compo-casting and WARB process

  • Vini, Mohamad Heydari;Daneshmand, Saeed
    • Advances in Computational Design
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    • v.7 no.2
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    • pp.129-137
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    • 2022
  • Compo-casting method is one of the popular technique to produce metal based matrix composites. But, one of the main challenges in this process is un-uniform spreading of reinforced subdivisions (particles) inside the metallic matrix and the lack of desirable mechanical properties of the final produced composites due to the low bonding strength among the metal matrix and reinforcement particles. To remove these difficulties and to promote the mechanical properties of these kind of composites, the WARM ARB technique was utilized as supplementary technique to heighten the mechanical and microstructural evolution of the casted Al/Al2O3 composite strips. The microstructure evolution and mechanical properties of these composites have been considered versus different WARM ARB cycles by tensile test, average Vickers micro hardness test, wear test and scanning electron microscopy (SEM). The SEM results revealed that during the higher warm- ARB cycles, big alumina clusters are broken and make a uniform distribution of alumina particles. It was shown that cumulating the forming cycles improved the mechanical properties of composites. In general, combined compo-casting and ARB process would consent making Al/Al2O3 composites with high consistency, good microstructural and mechanical properties.