• Title/Summary/Keyword: Micro-structure

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WETTABILITY AND DRUG DELIVERY OF FUNCTIONALLY GRADED NANO-MICRO POROUS TITANIUM SURFACE

  • Yun, Kwi-Dug;Vang, Mong-Sook;Yang, Hong-So;Park, Sang-Won;Park, Ha-Ok;Lim, Hyun-Pil
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.3
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    • pp.307-319
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    • 2008
  • STATEMENT OF PROBLEM: It is known that an anodic oxidation technique, one of the methods for the implant surface treatment, remarkably increased surface area, enhanced wettability and accelerated the initial bone healing. Purpose: This study was performed to evaluate the wettability of anodized titanium surface which has a nanotubular structure, to assess osseointegration after the placement of implant with nano-size tubes on tibia of rats and to analyze quantitatively transferable rhBMP-2 on each surface. MATERIAL AND METHOD: Four different kinds of surface-treated titanium discs (polished (machined surface) group, micro (blasting surface) group, nano (anodizedmachined surface) group, and nano-micro (anodized-blasting surface) group) were fabricated (n=10). Three different media were chosen to measure the surface contact angles; distilled water, plasma and rhBMP-2 solution. After a single drop (0.025 $m{\ell}$) of solution, the picture was taken with the image camera, and contact angle was measured by using image analysis system. For the test of osseointegration, 2 kinds of anodized surface (anodized-machined surface, anodized-blasting surface) implants having 2.0 mm in diameter and 5.0 mm in length inserted into the tibia of Wistar rats. After 3 weeks, tibia were harvested and the specimens were stained with hematoxylin and eosin for histological analysis. To test the possibility of drug delivery, after soaking sample groups in the concentration of 250 ng/$m{\ell}$l of rhBMP-2 for 48 hours, the excess solution of rhBMP-2 were removed. After that, they were lyophilized for 24 hours, and then the rhBMP-2 on the surface of titanium was resolved for 72 hours in PBS. All the extracted solution was analyzed by ELISA. One-way analysis of variance (ANOVA) was performed on the data. RESULTS: The wettability is improved by anodic oxidation. The best wettability was shown on the nano-micro group, and it was followed by nano group, micro group, and polished group. In the histological findings, all implants showed good healing and the new bone formation were observed along the implant surface. After 3 days, nano-micro group delivered the most amount of rhBMP-2, followed by nano group, micro group, and polished group. CONCLUSION: It indicated that anodic oxidation on blasting surface produce functionally graded nano-micro porous structure and enhance hydrophilicity of the surface and osseointegration. The findings suggest that the nano-micro porous structure could be a useful carrier of osteogenic molecules like rhBMP-2.

Processing Study for the Micro Pillar for Piezoelectric Energy Harvest (압전 에너지 하베스트를 위한 마이크로 필라 공정 연구)

  • Yun, Seok-Woo;Lee, Ku-Tak;Lee, Kyoung-Su;Jeong, Soon-Jong;Kim, Min-Soo;Cho, Kyoung-Ho;Koh, Jung-Hyuk
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.8
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    • pp.601-604
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    • 2010
  • In this study, the piezoelectric energy harvester was investigated employing the pillar structure with the diameter size of 50~500 um. Usually, the aspect ratio between the height and diameter was related with the piezoelectric performance. High aspect ratio was showed the low electric noise and high piezoelectric properties than low aspect ratio. Therefore, we have selected the Su-8 photo-resist and modified lithography process to manufacture the pillar structure with height above the 250 ${\mu}m$. In this presentation, we will report the process and properties of micro pillar structure based on the PMN-PZT (Pb$(Mg_{1/3}Nb_{2/3})O_3$-PbZrTiO$_3$) materials.

Strain gradient theory for vibration analysis of embedded CNT-reinforced micro Mindlin cylindrical shells considering agglomeration effects

  • Tohidi, H.;Hosseini-Hashemi, S.H.;Maghsoudpour, A.;Etemadi, S.
    • Structural Engineering and Mechanics
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    • v.62 no.5
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    • pp.551-565
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    • 2017
  • Based on the strain gradient theory (SGT), vibration analysis of an embedded micro cylindrical shell reinforced with agglomerated carbon nanotubes (CNTs) is investigated. The elastic medium is simulated by the orthotropic Pasternak foundation. The structure is subjected to magnetic field in the axial direction. For obtaining the equivalent material properties of structure and considering agglomeration effects, the Mori-Tanaka model is applied. The motion equations are derived on the basis of Mindlin cylindrical shell theory, energy method and Hamilton's principal. Differential quadrature method (DQM) is proposed to evaluate the frequency of system for different boundary conditions. The effects of different parameters such as CNTs volume percent, agglomeration of CNTs, elastic medium, magnetic field, boundary conditions, length to radius ratio and small scale parameter are shown on the frequency of the structure. The results indicate that the effect of CNTs agglomeration plays an important role in the frequency of system so that considering agglomeration leads to lower frequency. Furthermore, the frequency of structure increases with enhancing the small scale parameter.

Development of Nano-Stereolithography Process for Precise Fabrication of Three-Dimensional Micro-Devices (3차원 마이크로 디바이스 개발을 위한 나노 스테레오리소그래피 공정 개발에 관한 연구)

  • Park Sang-Hu;Lim Tae Woo;Yang Dong-Yol;Yi Shin Wook;Kong Hong-Jin;Lee Kwang-Sup
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.55 no.1
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    • pp.45-49
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    • 2006
  • A nano-stereolithography (NSL) process has been developed for the fabrication of three-dimensional (3D) micro-devices with high spatital resolution of approximately 100 nm. In the NSL process, a complicated 3D structure can be created by stacking layer-by-layer, so it does not require any sacrificial layer or any supporting structure. A laminated layer was fabricated by means of solidifying liquid-state monomers using two-photon absorption (TPA) which was induced by a femtosecond laser. When the fabrication of a 3D stacked structure was finished, unsolidified liquid resins were rinsed by ethanol to develop the fabricated structures; then, the polymerized structure was only left on the glass substrate. Through this work, several 3D microstructures such as a micro-channel, shell structures, and photonic crystals were fabricated to evaluate the possibility of the developed system.

The Manufacture of Calligraphy-Woodcarving Artwork Using Anatomical Micro Structure of Wood (목재의 미세조직구조를 이용한 서각작품 제작)

  • Ryu, Hyun-Soo;Chong, Song-Ho;Byeon, Hee-Seop
    • Journal of the Korea Furniture Society
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    • v.20 no.1
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    • pp.15-20
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    • 2009
  • Marvelous calligraphy-woodcarving artwork was made by using the mysterious beauty of anatomical structure of wood. The wooden artwork uses not only beautiful external appearance of wood, but it also uses the mysterious beauty of anatomical micro structure of wood which can only be observed through optical microscope or scanning electron microscope. The characteristics of anatomical structure of wood were presented through various carving techniques. The used wood species for the artwork include Quercus acutissima Carruth., Cinnamomum japonicum Sieb., Betula davurica PALL, Magnolia kobus A.P.DC, Populus maximowiczii HENRY, Betula schmidtii REGEL and Plerocaya stenoptera DC. These various types of woodcarving techniques are anticipated to be applied to the techart marketing for architecture as a field of environment art.

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Development of a 6 degrees-of-freedom micro stage for ultra precision positioning (초정밀작업을 위한 6자유도 마이크로 스테이지의 개발)

  • Kim, Kyung-Chan;Kim, Soo-Hyun;Kwak, Yoon-Keun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.22 no.2
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    • pp.372-379
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    • 1998
  • A new 6 degrees-of-freedom micro stage, based on parallel mechanisms and actuated by using piezoelectric elements, has been developed for the application of micro positioning such as semiconductor manufacturing devices, high precision optical measurement systems, and high accurate machining. The micro stage structure consists of a base platform and an upper platform(stage). The base platform can effectively generates planar motion with yaw motion, while the stage can do vertical motion with roll and pitch motions with respect to the base platform. This separated structure has an advantage of less interference among actuators. The forward and inverse kinematics of the micro stage are discussed. Also, through linearization of kinematic equations about an operating point on the assumption that the configuration of the micro stage remains essentially constant throughout a workspace is performed. To maximize the workspace of the stage relative to fixed frame, an optimal design procedure of geometric parameter is shown. Hardware description and a prototype are presented. The prototype is about 150mm in height and its base platform is approximately 94mm in diameter. The workspace of the prototype is obtained by computer simulation. Kinematic calibration procedure of the micro stage and its results are presented.

Structure Optimization of a Slot-Die Head with a Hydrophobic Micro-Patterns for Stripe Coatings (소수성 마이크로 패턴을 갖는 Stripe 코팅용 슬롯 다이 헤드 구조 최적화)

  • Yoo, Su-Ho;Lee, Jin-Young;Park, Jong-Woon
    • Journal of the Semiconductor & Display Technology
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    • v.18 no.2
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    • pp.6-10
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    • 2019
  • In the presence of $\mu-tip$ for narrow stripe coating, there appears lateral capillary flow along the hydrophilic head lip because the $\mu-tip$ has some resistance to flow. It was known to be suppressed by increasing the contact angle of the head lip. In this paper, we have demonstrated by computational fluid dynamics(CFD) simulations that it can also be suppressed by the formation of micro-patterns on the shim and meniscus guide embedded into the slot-die head. To optimize the micro-patterned structure, we have performed simulations by varying the groove width, depth, and clearance. In the absence of micro-patterns, it is shown by experiment and simulation that the solution spreads to a distance of $1,300{\mu}m$ from the ${\mu}-tip$. In the presence of micro-patterns with the groove width and clearance of $50{\mu}m$, the distance the solution spreads is reduced to $260{\mu}m$. However, no further suppression in the capillary flow is observed with micro-patterns with the groove width of $40{\mu}m$ or less. It is also observed that the capillary flow is not affected by the groove depth if it is larger than $10{\mu}m$. We have shown that the distance the solution spreads can be reduced further to $204{\mu}m$ by coating a hydrophobic material (contact angle of $104^{\circ}$) on the surface of micro-patterns having the groove width and clearance of $50{\mu}m$.

Veering Phenomena and Dynamic Characteristics in Lateral Micro-Gyroscope (수평형 마이크로 자이로스코프의 비어링 현상 및 동특성)

  • 정호섭;박규연
    • Journal of KSNVE
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    • v.11 no.1
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    • pp.132-140
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    • 2001
  • The vibratory gyroscope can effectively measure the angular velocity as the oscillating and position-sensing mode are exactly tuned. The veering Phenomenon impedes the exact tuning, which is caused by the mode coupling of two modes. In this paper, the gyroscope's structure with two frames is introduced to minimize the veering phenomenon that destabilizes the tuning process of oscillating and position-sensing mode. Experimental results show that the Proposed structure can achieve the mode intersection without veering phenomenon.

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A study on the prediction of micro-deformation in laser welding of small structure (소형구조물의 레이저-용접시 미세 변형 예측에 관한 연구)

  • 장원석;나석주
    • Proceedings of the KWS Conference
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    • 2000.10a
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    • pp.170-172
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    • 2000
  • In this research, newly proposed heat source equations were calculated to predict micro distortion of small structure in laser welding and compared with experimental results which were measured using laser speckle metrology. A finite element code, ABAQUS is used for the heat transfer analysis with a three-dimensional plane assumption. The results suggest that weld distortion is varied according to the heat source of the. laser beam.

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Pore Structure of Cement Matrix Exposed to High Temperatures (고온하의 시멘트 경화체의 공극구조)

  • 송훈;도정윤;소승영;소양섭
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.509-512
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    • 2003
  • Dehydration and micro crack thermal expansion occur in cement hydrates of concrete structure heated by fire for a long time. The characteristic of concrete exposed to high temperature can be analyzed from distribution of porosity and pore size. Porosity showed a tendency to increase irrespective of specimen types. This is due to both the outbreak of collapse of gel comprising the cement and a micro crack by heating. Porosity did not affect the variety of specimen and increased with the same tendency throughout every specimen. In addition, the deteriorate of compressive strength resulted from increase in porosity

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