• Journal of Electrochemical Science and Technology
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• 제2권3호
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• pp.157-162
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• 2011

We report a simple route for synthesizing multi-dimensional structured silicon anode materials from commercially available bulk silicon powders via metal-assisted chemical etching process. In the first step, silver catalyst was deposited onto the surface of bulk silicon via a galvanic displacement reaction. Next, the silver-decorated silicon particles were chemically etched in a mixture of hydrofluoric acid and hydrogen peroxide to make multi-dimensional silicon consisting of one-dimensional silicon nanowires and micro-scale silicon cores. As-synthesized silicon particles were coated with a carbon via thermal decomposition of acetylene gas. The carbon-coated multi-dimensional silicon anodes exhibited excellent electrochemical properties, including a high specific capacity (1800 mAh/g), a stable cycling retention (cycling retention of 89% after 20 cycles), and a high rate capability (71% at 3 C rate, compared to 0.1 C rate). This process is a simple and mass-productive (yield of 40-50%), thus opens up an effective route to make a high-performance silicon anode materials for lithiumion batteries.

• 한국기계가공학회지
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• 제12권6호
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• pp.117-124
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• 2013

Recently, the cell adhesion phenomenon that occurs in or between cells and other substances has become an important field of research in biology and biomedical engineering. Among the research, the foundational studies primarily experiment using biomedical materials (e.g. Glass Beads) attached to an AFM cantilever. For cell adhesion research, the mechanism where biomedical materials can be attached to the cantilever must be developed for this purpose; however, the mechanism remains an insufficient step. In this paper, a new stage where the Glass Bead can be attached to the cantilever is designed and fabricated;, the mm range movement in the stage is controlled using the stepping motor with a minimum displacement of $1{\mu}m$. The adhesive flow is also controlled using a PZT actuator. In addition, through the air suction, the cantilever holder can be fixed to the stage. The new stage including the bond inflows mechanism is evaluated and analyzed using theory and experiments.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1997년도 추계학술대회 논문집
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• pp.206-210
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• 1997

In the fields of the optics, precise machine, semiconductors, the micro-positioning actuators are required for the control of position in the submicron range. PNN-P2N-PZT ceramics were fabricated with various mole ratio of the PZT[Pb(Zr$_{1}$2//Ti$_{1}$2)O$_3$]. PNN (Pb(Ni$_{1}$3/Nb$_{2}$3/)O$_3$]and PZN[Pb(Zn$_{1}$3//Nb/sbu 2/3/)O$_3$] powders prepared by double calcination and PZT powders prepared by molten- salt synthesis method. The relative permittivity of specimen with PZT 0.3 mole ratio was shown 5,320 and appeared the relaxor ferroelectric feature. The maximum Piezoelectric coefficient d$_{31}$ to be used for evaluation the displacement of piezoceramics in PNN-PZN-PZT ceramics was 324$\times$10$^{-12}$ (C/V) at the vicinity of morphotropic phase boundary and was larger than that of solid PZT ceramics(120$\times$10$^{-12}$ C/V).

• Journal of Welding and Joining
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• 제2권2호
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• pp.54-61
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• 1984

Construction of welding structure is greatly dependent upon welding heat cycle. Fracture toughness is decreased remarkablely due to coarse grained HAZ and inequal residual stress of three dimensions to originate in welding. Post weld heat treatment(PWHT) is carried out to increase the fracture toughness of HAZ and to remove the residual stress. There occur some problem such as toughness decrement and stress relief cracking(SRC) in the coarse grained HAZ subject to the effect of tempering treatment. Therefore, in this paper, the effect of heat inputs affecting cooling rate and PWHT under the no stress on fracture toughness were evaluated by crack opening displacement (COD), SEM and micro-hardness test. Experimental results are as follows; 1. Fracture toughness of weld HAZ is dependent upon weld heat cycle and it is decreased with increment of heat input, but the degree of improvement of fracture toughness after PWHT was linearly increased with heat input. 2. Hardness of the parent metal is not changed, but the softening of coarse grained HAZ is remarkable due to PWHT. 3. Fracture surface of as-weld show the perfect brittle fracture with the cleavage fracture, but after PWHT they appear the ductile fracture surface with dimple.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2005년도 추계학술대회논문집
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• pp.731-734
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• 2005

Generally, characteristics of electromechanical actuators are coupled with the mechanical and the electrical properties. Important mechanical parameters of these actuators are the achievable force and displacement in the presence of electric field. These mechanical parameters are related to the stress and strain of the materials and the actuator geometry. This paper presents how to measure the blocked force by using the micro-balance. The blocked force is defined as the force produced by the transducer under an applied voltage when the tip is constrained to zero motion. Also, a theoretical force by using the cantilever beam model is calculated under elastic domain. From the sample of 4 cm $\times$ 1 cm $\times$ 20 $\mu$m, the blocked farce measured from the equipment is 20.3 $\mu$N at 8 V$_{DC}$. By comparing it with the theoretical value, 24.9 $\mu$N, the blocked force measurement is acceptable. The furce measurement is also investigated with different AC electric fields and the frequency.

• Steel and Composite Structures
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• 제32권5호
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• pp.671-686
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• 2019

Active control of solar panels with honeycomb core and carbon nanotube reinforced composite (CNTRC) facesheets for smart structures using piezoelectric patch sensor and actuator to reduce the amplitude of vibration is a lack of the previous study and it is the novelty of this research. Of active control elements are piezoelectric patches which act as sensors and actuators in many systems. Their low power consumption is worth mentioning. Thus, deriving a simple and efficient model of piezoelectric patch's elastic, electrical, and elastoelectric properties would be of much significance. In the present study, first, to reduce vibrations in composite plates reinforced by carbon nanotubes, motion equations were obtained by the extended rule of mixture. Second, to simulate the equations of the system, up to 36 mode shape vectors were considered so that the stress strain behavior of the panel and extent of displacement are thoroughly evaluated. Then, to have a more acceptable analysis, the effects of external disturbances (Aerodynamic forces) and lumped mass are investigated on the stability of the system. Finally, elastoelectric effects are examined in piezoelectric patches. The results of the present research can be used for micro-vibration suppression in satellites such as solar panels, space telescopes, and interferometers and also to optimize active control panel for various applications.

• Nuclear Engineering and Technology
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• 제51권4호
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• pp.1132-1141
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• 2019

Steel-concrete-steel (SCS) sandwich structures have important advantages over conventional concrete structures, however, bond-slip between the steel plate and concrete may lead to a loss of composite action, resulting in a reduction of stiffness and fatigue life of SCS sandwich structures. Due to the inaccessibility and invisibility of the interface, the interfacial performance monitoring and debonding detection using traditional measurement methods, such as relative displacement between the steel plate and core concrete, have proved challenging. In this work, two methods using piezoelectric transducers are proposed to detect the bond-slip between steel plate and core concrete during the test of the beam. The first one is acoustic emission (AE) method, which can detect the dynamic process of bond-slip. AE signals can be detected when initial micro cracks form and indicate the damage severity, types and locations. The second is electromechanical impedance (EMI) method, which can be used to evaluate the damage due to bond-slip through comparing with the reference data in static state, even if the bond-slip is invisible and suspends. In this work, the experiment is implemented to demonstrate the bond-slip monitoring using above methods. Experimental results and further analysis show the validity and unique advantage of the proposed methods.

• Advances in nano research
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• 제10권3호
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• pp.281-293
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• 2021

This paper presents a new nonlocal Hyperbolic Shear Deformation Beam Theory (HSDBT) for the free vibration of porous Functionally Graded (FG) nanobeams. A new displacement field containing integrals is proposed which involves only three variables. The present model incorporates the length scale parameter (nonlocal parameter) which can capture the small scale effect and its account for shear deformation by a hyperbolic variation of all displacements through the thickness without using the shear correction factor. It has been observed that during the manufacture of Functionally Graded Materials (FGMs), micro-voids and porosities can occur inside the material. Thus, in this work, the investigation of the free vibration analysis of FG beams taking into account the influence of these imperfections is established. Four different porosity types are considered for FG nanobeam. Material characteristics of the FG beam are supposed to vary continuously within thickness direction according to a power-law scheme which is modified to approximate material characteristics for considering the influence of porosities. Based on the nonlocal differential constitutive relations of Eringen, the equations of motion of the nanobeam are derived using Hamilton's principle. The effects of nonlocal parameter, aspect ratio, and the porosity types on the dynamic responses of the nanobeam are discussed.

• 한국안전학회지
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• 제37권5호
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• pp.7-13
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• 2022

Digital image correlation (DIC) is a method used to measure the displacement and strain of structures. It involves transforming and analyzing images before and after deformation using correlation coefficients from irregular light and shade on the surface of structures. In the present study, a microspeckle pattern was applied to the surface of a specimen to identify initial cracking. The test specimen constituted CFRP composites laminated on a curved Al liner The specimen was manufactured by stacking 100 ply of CFRP prepregs in the 0° and 90° directions in a three-point bending test. The equivalent strain was evaluated through DIC analysis after monitoring deformation using a CCD camera. Fracture shape was observed using a microscope. The equivalent strain contour distribution was checked until the maximum load fracture occurred at the center of the test specimen. Variations in the strain indicated the initial occurrence and progression of microcracks. These results can be used to improve the accuracy of detecting micro crack initiation and to achieve structural stability.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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• pp.143-146
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• 2002

Unsized AS-4 carbon fibers were etched by RF plasma and then coated via plasma polymerization in order to enhance adhesion to vinyl ester resin. The gases utilized for the plasma etching were Ar, $N_2 and O_2$, while the monomers used for the plasma polymerization coating were acetylene, butadiene and acrylonitrile. The conditions for the plasma etching and the plasma polymerization were optimized by measuring interfacial adhesion with vinyl ester resin via micro-droplet tests. Among the treatment conditions, the combination of Ar plasma etching and acetylene plasma polymerization provided greatly improved interfacial shear strength (IFSS) of 69MPa compared to 43MPa with as-received carbon fiber. Based on the SEM analysis of failure surface and load-displacement curve, it was assume that the failure might be occurred at the carbon fiber and plasma polymer coating. The plasma etched and plasma polymer coated carbon fibers were subjected to analysis with SEM, XPS, FT-IR or Alpha-Step, and dynamic contact angles and tensile strengths were also evaluated. Plasma polymer coatings did not change tensile strength and surface roughness of fibers, but decreased water contact angle except butadiene plasma polymer coating, possibly owing to the functional groups introduced, as evidenced by FT-IR and XPS.