• Title/Summary/Keyword: Micro chemical analysis

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Failure Analysis of Circulating Water Pump Shaft in Power Plant (발전 계획에서 순환 물 펌프 고장 분석)

  • Lee, Jaehong;Jung, Nam-gun
    • KEPCO Journal on Electric Power and Energy
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    • v.7 no.1
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    • pp.125-128
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    • 2021
  • This paper presents the root cause failure analysis of the circulating water pump in the 560 MW thermal power plant. A fractured austenitic stainless-steel shaft operated for 24 years was examined. Fracture morphology was investigated by micro and macro-fractographic analysis. The metallurgical analyses including chemical analysis, metallography and hardness testing were performed. The analysis reveals that the pump shaft was fractured due to the reverse bending load with combination of rotating bending load. Corrective actions for plant operator was recommended based on the analysis.

엑사이머 레이져를 이용한 실리콘웨이퍼의 미세가공

  • 윤경구;이성국;황경현
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.04a
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    • pp.1058-1062
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    • 1997
  • Development of laser induced chemical etching technologt with KrF laser are carried out in this study for micromachining of silicon wafer. The paper is devoted to experimental identification of excimer laser induced mechanism of silicon under chlorine pressures(0.02~500torr). Experimental results on pulsed KrF excimer laser etching of silicon in chorine atmosphere are presented. Etching rate dependency on laser fluence and chlorine pressure are discussed on the basis of experimental analysis, it is concluded that accurate digital micro machining process of silicon wafer can achieved by KrF laser induced chemical etching technology.

A study on the characteristics of Ti frame using filler metal at brazed joints (납재를 이용한 티타늄(Ti) 안경테의 땜질 접합부의 특성에 관한 연구)

  • Kim, Dae-Nyoun;Kim, Ki-Hong;Kim, Hye-Dong;Jang, Woo-Yeong
    • Journal of Korean Ophthalmic Optics Society
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    • v.8 no.1
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    • pp.47-52
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    • 2003
  • The metallurgical and mechanical experiments of Titanium frame were conducted to investigate the optimum brazing and the improved brazed joints by filler metals has been developed by using other filler metals at brazing process. The filler metal is used in form of a metallic glass. The optimum brazing conditions were obtained from microstructural observation of brazed joints chemical analysis by means of X-ray micro-analysis and heating method.

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The Fabrication of Pt Micro Heater Using Aluminum Oxide as Medium Layer and Its Thermal Characteristics (알루미늄산화막을 매개층으로 이용한 백금 미세발열체의 제작과 발열특성)

  • 노상수;정귀상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.11a
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    • pp.331-334
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    • 1997
  • The electrical and physical charateristics of aluminum oxide and Pt thin films on it, deposited by reactive sputtering and DC magnetron sputtering, respectively, were analysed with increasing annealing temperature(400~80$0^{\circ}C$) by four point probe, SEM and XRD. Under $600^{\circ}C$ of annealing temperature, aluminum oxide had the properties of improving Pt adhesion to SiO$_2$and insulation without chemical reaction to Pt thin films and the resistivity of Pt thin finns was improved. But these properties of aluminum oxide and Pt thin finns on it were degraded over $700^{\circ}C$ of annealing temperature because aluminum oxide was changed into metal aluminum and then reacted to Pt thin films deposited on it. The thermal characteristics of Pt micro heater were analysed with Pt-RTD integrated on the same substrate. In the analysis of properties of Pt micro heater. active area was smaller size, Pt micro heater had better thermal characteristics. Temperature of Pt micro heater fabricated on membrane was up to 34$0^{\circ}C$ with 1.2watts of the heating power due to reduction of the external thermal loss.

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Preparation and Characterization of Metal-containing Activated Carbon Derived from Phenolic Resin

  • Oh, Won-Chun
    • Carbon letters
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    • v.4 no.2
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    • pp.86-92
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    • 2003
  • A series of micro- and mesoporous activated carbons were prepared from two kinds of phenolic resin using a metal treated chemical activation methodology. $N_2$-adsorption data were used to characterize the surface properties of the produced activated carbons. Results of the surface properties and pore distribution analysis showed that phenolic resin can be successfully converted to micro- and mesoporous activated carbons with specific surface areas higher than 973 $m^2/g$. Activated carbons with porous structure were produced by controlling the amount of metal chlorides ($CuCl_2$). Pore evolvement depends on the amount of additional metal chloride and precursors used. From the SEM and EDX data, copper contents were shown to be most effected by the incremental addition of metal chloride.

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A Pilot study of poroelastic modulus measurement in micro-bone tissue (미세 골조직의 공극탄성계수 측정을 위한 예비 연구)

  • 박영환;홍정화
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.1038-1041
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    • 2004
  • In this study, developed a micro-level experimental setup to measure pore pressure and poroelastic modulus in various strain and strain rate about a stress in micro-structure of bone tissue. It is essential device in the development of the model to analysis the interstitial bone fluid flow of the lacuno-canalicular system to be known that would effect on the bone remodeling. The constitution of the experimental setup is as follows, microscopic image processing system; actuator control unit; load measurement system. A pilot study was used an artificial chemical wood to have similar poroelastic property of bone matrix and conducted to validate the suitability of the measurement system.

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The Fabrication of Micro-Heater MgO Medium Layer and It`s Characteristics (산화마그네슘을 매개층으로 이용한 백금박막 미세발열체의 제작과 그 특성)

  • 홍석우;노상수;장영석;정쉬상
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1999.05a
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    • pp.150-153
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    • 1999
  • The electrical and physical characteristics of MgO and Pt thin-films on Si wafers deposited by r.f magnetron sputtering, were analyzed with annealing condition(100$0^{\circ}C$, 120 min) by four point probe, SEM and XRD. Until annealing temperature of 100$0^{\circ}C$, MgO had the properties of improving Pt adhesion to SiO$_2$ and insulation without chemical reaction to Pt thin-films and the resistivity of Pt thin-films was improved. The thermal characteristics of Pt micro-heater were analyed with Pt-RTD integrated on the same substrate, In the analysis of properties of Pt-RTD, TCR value had 3927 ppm/$^{\circ}C$ and liner in the temperature range of 25~40$0^{\circ}C$ temperature of Pt micro-heater had up to 40$0^{\circ}C$ with 1.5 watts of the heating power.

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Fabrication of the temperature controllable microreactor for trypsin treatment (온도 조절이 가능한 트립신 전처리 반응침의 제작)

  • Sim, Tae-Seok;Lee, Kook-Nyung;Joo, Hwang-Soo;Kim, Dae-Weon;Kim, Byung-Gee;Kim, Yong-Hyup;Kim, Yong-Kweon
    • Proceedings of the KIEE Conference
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    • 2003.10a
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    • pp.45-48
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    • 2003
  • In the research of proteomics, mass spectrometry analysis is the essential method for identification of the unknown proteins. Trypsin treatment for the sample preparation of mass spectrometry is the inevitable procedure[1]. However, sample preparation procedure is cumbersome and time consuming. To resolve these problems, Temperature controllable microreactor was designed and fabricated. It consists of metering chamber, micro channel, reaction chamber, platinum (Pt) thin film heater and a temperature sensor so that micro metering and mixture of reagent with temperature control can be done on the same chip. The total size of the fabricated microreactor was $37{\times}30{\times}1\;mm^3$ and the size of channel cross section was $200{\times}100{\mu}m^2$. PID temperature controller was realized using NI DAQ, PCI-MIO-l6E-1 board and LabVIEW program.

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Electrochemical characterization of activated carbon-sulfur composite electrode in organic electrolyte solution

  • Kim, Dongyoung;Park, Soo-Jin;Jung, Yongju;Kim, Seok
    • Carbon letters
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    • v.14 no.2
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    • pp.126-130
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    • 2013
  • In this study, we present a more electrochemically enhanced electrode using activated carbon (AC)-sulfur (S) composite materials, which have high current density. The morphological and micro-structure properties were investigated by transmission electron microscopy. Quantity of sulfur was measured by thermogravimetric analysis analysis. The electrochemical behaviors were investigated by cyclic voltammetry. As a trapping carbon structure, AC could provide a porous structure for containing sulfur. We were able to confirm that the AC-S composite electrode had superior electrochemical activity.