• Title/Summary/Keyword: Micro Material Property

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A Study on Thermal Properties for Epoxy Micro-and-Nano Mixture Composites(EMNC) (에폭시 마이크로-나노 입자가 혼합된 콤포지트의 열적특성에 관한연구)

  • Lee, Chang-Hoon;Kim, Kuk-Jin;Kim, Suk-Man;Kang, Do-Hoon;Yeon, Da-Som;Park, Jae-Jun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.83-83
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    • 2010
  • This study investigates the thermal and mechanical properties of insulation elements through mixing epoxy based micro- and nano particles. Regarding thermal properties, DSC and DMA were used to calculate crosslinking densities for various types of insulation elements. In a mechanical property of bending strength, shape and scale parameters were obtained using the Weibull plot. This study obtained the most excellent results of scale parameters, such as Vol 3.2%, in the bending strength of EMNCs.

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Development of Surface Treatment for Hydrophobic Property on Aluminum Surface (알루미늄의 발수 표면처리 기술 개발)

  • Byun, Eun-Yeon;Lee, Seung-Hun;Kim, Jong-Kuk;Kim, Yang-Do;Kim, Do-Geun
    • Journal of the Korean institute of surface engineering
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    • v.45 no.4
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    • pp.151-154
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    • 2012
  • A hydrophobic surface has been fabricated on aluminum by two-step surface treatment processes consisting of structure modification and surface coating. Nature inspired micro nano scale structures were artificially created on the aluminum surface by a blasting and Ar ion beam etching. And a hydrophobic thin film was coated by a trimethylsilane ($(CH_3)_3SiH$) plasma deposition to minimize the surface energy of the micro nano structure surface. The contact angle of micro nano structured aluminum surface with the trimethylsilane coating was $123^{\circ}$ (surface energy: 9.05 $mJ/m^2$), but the contact angle of only trimethylsilane coated sample without the micro nano surface structure was $92^{\circ}$ (surface energy: 99.15 $mJ/m^2$). In the hydrophobic treatment of aluminum surface, a trimethylsilane coated sample having the micro nano structure was more effective than only trimethylsilane coated sample without the micro nano structure.

Bonding Property of Silicon Wafer Pairs with Annealing Method (열처리 방법에 따른 실리콘 기판쌍의 접합 특성)

  • 민홍석;이상현;송오성;주영창
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.5
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    • pp.365-371
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    • 2003
  • We prepared silicon on insulator(SOI) wafer pairs of Si/1800${\AA}$ -SiO$_2$ ∥ 1800${\AA}$ -SiO$_2$/Si using water direct bonding method. Wafer pairs bonded at room-temperature were annealed by a normal furnace system or a fast linear annealing(FLA) equipment, and the micro-structure of bonding interfaces for each annealing method was investigated. Upper wafer of bonded pairs was polished to be 50 $\mu\textrm{m}$ by chemical mechanical polishing(CMP) process to confirm the real application. Defects and bonding area of bonded water pairs were observed by optical images. Electrical and mechanical properties were characterized by measuring leakage current for sweeping to 120 V, and by observing the change of wafer curvature with annealing process, respectively. FLA process was superior to normal furnace process in aspects of bonding area, I-V property, and stress generation.

Generation of Laser Scan Path Considering Resin Solidification Phenomenon in Micro-stereolithography Technology (마이크로 광 조형기술에서 수지경화현상을 고려한 레이저 주사경로 생성)

  • 조윤형;조동우
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.10a
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    • pp.1037-1040
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    • 2002
  • In micro-stereolithography technology, fabrication conditions that include laser power, laser scan speed, laser scan pitch, and material property of photopolymer such as penetration depth and critical exposure are considered as major process variables. But the existing scan path generation methods based only on CAD model have not taken them into account, which has resulted in cross-section dimension of low accuracy. Thus, to enhance cross-section dimensional accuracy, the physical resin solidification n phenomena should be reflected in laser scan path generation and stage operating code. In this paper, multi-line experiments based on single line solidification model are performed. And the method for improving cross-section dimensional accuracy is presented, which is to apply the database based on experimental results to laser scan path generation.

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Development and Verification of Micro-indentation Technique for Material Property Evaluation of Hyper-elastic Rubber (초탄성고무 물성평가용 미소압입시험법 개발 및 검증)

  • Lee, Hyung-Il;Lee, Jin-Haeng
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.132-137
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    • 2004
  • In this work, effects of hyper-elastic rubber material properties on the indentation load-deflection curve and subindenter deformation are first examined via [mite element (FE) analyses. An optimal data acquisition spot is selected, which features maximum strain energy density and negligible frictional effect. We then contrive two normalized functions. which map an indentation load vs. deflection curve into a strain energy density vs. first invariant curve. From the strain energy density vs. first invariant curve, we can extract the rubber material properties. This new spherical indentation approach produces the rubber material properties in a manner more effective than the common uniaxial tensile/compression tests. The indentation approach successfully measures the rubber material properties and the corresponding nominal stress.strain curve with an average error less than 3%.

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Characterization of Silica/EVOH Hybrid Coating Materials Prepared by Sol-Gel Method

  • Kim, Seong-Woo
    • Journal of the Korean Applied Science and Technology
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    • v.26 no.3
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    • pp.288-296
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    • 2009
  • In this study, the silica-based hybrid material with high barrier property was prepared by incorporating ethylene-vinyl alcohol (EVOH) copolymer, which has been utilized as packaging materials due to its superior gas permeation resistance, during sol-gel process. In preparation of this EVOH/$SiO_2$ hybrid coating materials, the (3-glycidoxy-propyl)-trimethoxysilane (GPTMS) as a silane coupling agent was employed to promote interfacial adhesion between organic and inorganic phases. As confirmed from FT-IR analysis, the physical interaction between two phases was improved due to the increased hydrogen bonding, resulting in homogeneous microstructure with dispersion of nano-sized silica particles. However, depending on the range of content of added silane coupling agent (GPTMS), micro-phase separated microstructure in the hybrid could be observed due to insufficient interfacial attraction or possibility of polymerization reaction of epoxide ring in GPTMS. The oxygen barrier property of the mono-layer coated BOPP (biaxially oriented polypropylene) film was examined for the hybrids containing various GPTMS contents. Consequently, it is revealed that GPTMS should be used in an optimum level of content to produce the high barrier EVOH/$SiO_2$ hybrid material with an improved optical transparency and homogeneous phase morphology.

Fabrication and Mechanical Properties of TiNi/Al2024 Composites by Hot-Press Method (고온 프레스법에 의한 TiNi/Al2024 복합재료의 제조 및 기계적 특성평가)

  • Son, Yong-Kyu;Bae, Dong-Su;Park, Young-Chul;Lee, Gyu-Chang
    • Transactions of Materials Processing
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    • v.18 no.1
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    • pp.45-51
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    • 2009
  • Shape memory alloy has been used to improve the tensile strength of composite by the occurrence of compressive residual stress in matrix using its shape memory effect. In order to fabricate shape memory alloy composite, TiNi alloy fiber and Al2024 sheets were used as reinforcing material and matrix, respectively. In this study, TiNi/Al2024 shape memory alloy composite was made by using hot press method. In order to investigate bonding condition between TiNi reinforcement and Al matrix, the micro-structure of interface was observed by using optical microscope and diffusion layer of interface was measured by using Electron Probe Micro Analyser. And the mechanical properties of composite with three parameters(volume fraction of fiber, cold rolling amount and test temperature) were obtained by tensile test. The most optimum bonding condition for fabrication the TiNi/Al2024 composite material was obtained as holding for 30min. under the pressure of 60MPa at 793K. The strength of composite material increased considerably with the volume fraction of fiber up to 7.0%. And the tensile strength of this composite increased with the reduction ratio and it also depends on the volume fraction of fiber.

Micro-silica Mixed Aqua-epoxy for Concrete Module Connection in Water : Part 1 - Material Development and Evaluation (해상 프리캐스트 콘크리트 부유체 모듈 가접합을 위한 마이크로 실리카 혼입 수중용 에폭시 접합 성능 검토 : Part 1 - 재료 개발 및 성능 검토)

  • Choi, Jin-Won;Kim, Young-Jun;You, Young-Jun;Kwon, Seung-Jun;Kim, Jang-Ho Jay
    • Journal of the Korea Concrete Institute
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    • v.27 no.1
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    • pp.21-28
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    • 2015
  • Recent studies on concrete floating structure development focused on connection system of concrete modules. Precast concrete modules are designed to be attached by prestressing in the water, exposing the structure to the loads from water and making the construction difficult. Therefore, a development of bond material became a key issue in successful connection of floating concrete modules. In this study, micro-silica mixed aqua epoxy (MSAE) is developed for the task. Existing primer aqua epoxy, originally used as a bond material for the retrofit of concrete structures using fiber reinforced polymers, is evaluated to find the optimum micro-silica added mix proportion. Micro-silica of 0~4 volume % was mixed in standard mixture of aqua epoxy. Then, the material property tests were performed to study the effect of micro-silica in aqua epoxy by controlling the epoxy silane proportion by 0, ${\pm}5$, ${\pm}10%$. The optimum mix design of MSAE was derived based on the test results. The MSAE was used to connect concrete module specimens with the epoxy thickness variation of 5, 10, and 20mm. Then, 3-point loading test was performed to verify the bond capacity of MSAE. The results show that MSAE improves the bond capacity of concrete module.

Physical properties of PU coated fabric with collagen (콜라겐을 첨가한 폴리우레탄 코팅직물의 물성)

  • 백천의;유효선
    • Journal of the Korean Society of Clothing and Textiles
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    • v.23 no.6
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    • pp.800-808
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    • 1999
  • The demand for PU coated synthetic leather is increasing as a high fashion material. But it has some faults of water vapor permeability surface tacky property and static electricity. Therefore the purpose of this study was the produce of PU coated fabric added collagen with hydrophilic property and soft touch. In the PU coated fabric water vapor permeability water vaper absorption and frictional electronic voltage were investigated surface bending and compression properties were also examined by the use of KES-FB System. The followings were the results of this study. 1. There was no Cr in the collagen so that Cr was not treated in the collagen. 2. The surface and cross sectional layer of PU coated fabric with collagen were highly developed by micro porous structure. 3. The water vapor permeability of PU coated fabric was increased as collagen concentration increased. 4. The water vapor absorption of PU coated fabric was increased as collagen concentration increased. 5. The frictional electronic voltage of PU coated fabric was decreased in accordance with the increase of collagen concentration. Especially it effectively decreased by the use of only 5% collagen concentration. 6,. The bending and compression properties of PU coated fabric were increased in accordance with the increase of collagen concentration so that it became stiff. 7. The Value of MIU, SMD was decreased in accordance with the increase of collagen concentration so that the PU coated fabric became smooth.

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Assessment of flexural performance of hybrid fiber reinforced concrete. (하이브리드 섬유보강 콘크리트의 휨성능 평가)

  • Kim, Hag-Youn;Kim, Nam-Ho;Park, Choon-Gun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05b
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    • pp.337-340
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    • 2005
  • In this study, an effect of fiber blending on material property of Hybrid Fiber Reinforced Concrete (HFRC) was evaluated. Also, Compare and evaluates collating and mechanical property by the mixing rate of fiber for HFRC was determine. Modulus of rupture and strength effectiveness of Hybrid Fiber Reinforced Concrete mixed with macro-fiber(steel fiber) and micro-fiber(glass fiber, carbon fiber, cellulose fiber). Test result shows, in the case of mono fiber reinforced concrete. As the steel fiber mixing rate increases to 1.5$\%$, the strength effectiveness promotion rate rises. However, when is 2.0$\%$, strength decreases. In the case of hybrid fiber reinforcement concrete, synergy effect of micro fiber and macro fiber happens and higher Modulus of rupture and strength effectiveness appears than mono-fiber reinforcement concrete. Use of hybrid fiber reinforcement in concrete caused a significant influence on its fracture behavior; consequently, caused increase by mixing rate of steel fiber + carbon fiber and contributed by steel fiber + glass fiber, steel fiber + celluloid fiber in reinforcement effect in order. And was expose that steel fiber(1.5$\%$) + carbon fiber(0.5$\%$) is most suitable association.

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