• Title/Summary/Keyword: Mg 입자

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The Spontaneous Infiltration Mechanism of Molten Al Alloy to AI$_2$O$_3$ Preform (AI$_2$O$_3$ Preform에 대한 용융 Al 합금의 자발적 침윤 기구)

  • 이동윤;박상환;이동복
    • Journal of the Korean Ceramic Society
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    • v.35 no.7
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    • pp.685-690
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    • 1998
  • The wetting behavior and the characteristic of spontaneous infiltration of pure Al and Al-(Si)-Mg alloys on {{{{ { {Al }_{ 2} O}_{3 } }} in vacuum argon and nitrogen atmosphere were investigated to find out the spontaneous in-filtration mechanism. The wetting of molten Al and Al alloys on {{{{ { {Al }_{ 2} O}_{3 } }} was only possible in cacuum at-mosphere but the sponataneous infiltration of molten Al-(Si)-Mg alloys was successfully made on {{{{ { {Al }_{ 2} O}_{3 } }} pre-form in nitrogen atmoshpere. The difference of wettability and spontaneous infiltration of molten Al and Al alloys on {{{{ { {Al }_{ 2} O}_{3 } }} were found to be related to formation of the Mg-N compound coated layer on {{{{ { {Al }_{ 2} O}_{3 } }} particles which was believd to increase wettability of molten Al alloys on {{{{ { {Al }_{ 2} O}_{3 }.

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Reaction Parameters on the Reactivity in the Preparation of B4C by SHS (자전연소합성법에 의한 B4C분말의 제조에 있어 반응성에 대한 반응변수의 고찰)

  • Shin, Chang-Yun;Yun, Ki-Seok;Park, Yeong-Cheol;Hayk, Nersisyan;Won, Chang-Whan
    • Journal of the Korean Ceramic Society
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    • v.42 no.1
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    • pp.22-27
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    • 2005
  • The preparation of B4C by SHS in $B_{2}O_{3}-Mg-C$ system was investigated in this study. In the preparation of B4C, the effect on reactivity and reaction products of the initial pressure of inert gas in reactor, the content of Mg and C in mixture was investigated. The minimum initial pressure of inert gas in reactor for SHS reaction in this system was 25 atm, and as the pressure increased, the concentration of unreacted Mg decreased and combustion temperature increased. At the initial inert gas pressure in reactor of 25 atm, the optimum composition for the preparation of pure B4C was $2B_{2}O_{3}+6.3Mg +0.94C$. The B4C synthesized in this condition had an irregular shape and the particle size of $1\~3{\mu}m$.

The Influence of Fe Particle Size on the Critical Properties of MgB2 Superconductor (MgB2 초전도체의 임계특성에 대한 Fe 입자 크기의 영향)

  • Jeong, Hyeondeok;Lee, Dong-Gun;Ryu, Sung-Soo;Park, Hai-Woong;Kim, Chan-Joong;Jun, Byung-Hyuk
    • Journal of Powder Materials
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    • v.26 no.5
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    • pp.432-436
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    • 2019
  • This study demonstrates the effect of addition of Fe particles of different sizes on the critical properties of the superconductor $MgB_2$. Bulk $MgB_2$ is synthesized by ball milling Mg and B powders with Fe particles at $900^{\circ}C$. When Fe particles with size less than $10{\mu}m$ are added in $MgB_2$, they easily react with B and form the FeB phase, resulting in a reduction in the amount of the $MgB_2$ phase and deterioration of the crystallinity. Accordingly, both the critical temperature and the critical current density are significantly reduced. On the other hand, when larger Fe particles are added, the $Fe_2B$ phase forms instead of FeB due to the lower reactivity of Fe toward B. Accordingly, negligible loss of B occurs, and the critical properties are found to be similar to those of the intact $MgB_2$.

Chitosan Nanoparticle System for Improving Blood Circulation (혈행개선을 위한 키토산 나노입자화)

  • Lee, Ji-Soo;Yoon, Hyun-Sook;Kim, Eun Suh;Nam, Hee Sop;Lee, Hyeon Gyu
    • Korean Journal of Food Science and Technology
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    • v.48 no.2
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    • pp.153-158
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    • 2016
  • The principal objective of this study was to produce a chitosan nanoparticle (NP) system for improving blood circulation. Chitosan NPs were prepared using fucoidan and $poly-{\gamma}-glutamic$ acid (PGA), denoted as CS/Fu and CS/Fu/PGA NPs, respectively. As the chitosan concentration was increased, the activated partial thromboplastin time (APTT) of the NPs significantly increased (p<0.05). When the concentration of fucoidan and ${\gamma}-PGA$ was 5-20 and $1-10{\mu}g/mL$, respectively, the size of the CS/Fu and CS/Fu/PGA NPs was approximately 200 and 100 nm, respectively. With an increase in the fucoidan and PGA concentration, the APTT of CS/Fu and CS/Fu/PGA NPs significantly increased (p<0.05). These results suggest that CS/Fu and CS/Fu/PGA NPs could be used as a potent NP system for improving blood circulation.

A study on the optimized coagulation for separation of liquid and solid from CMP waste (CMP 폐액의 고액 분리를 위한 최적 응집조건에 관한 연구)

  • Hong, Seongho;Oh, Suckhwan
    • Clean Technology
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    • v.7 no.1
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    • pp.27-34
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    • 2001
  • The waste slurry generated from CMP process contains particulate and heavy metals. It is hard to treat the waste slurry by conventional treatment method because the particulates in the waste are too fine to be easily separated the solid from the waste for the purpose of water recycling. The investigation was focused on finding the optimum condition of coagulation with two different coagulants. When the solid content in the waste slurry solution was 0.1wt%, the optimal ranges of pH and PACl concentration were 4~6 and 20~50 mg/L, respectively. When the solid content was increased to 0.5wt%, the optimal condition was 4~5 for pH and 50~100 mg/L for PACl concentration.

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Changes in Soluble Protein, Free Amino Acid and Starch of Jeungpyun Dough during Fermentation (발효과정 중 증편반죽의 가용성 단백질, 유리아미노산 및 전분의 변화)

  • 박영선;서정식
    • Korean journal of food and cookery science
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    • v.11 no.3
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    • pp.282-286
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    • 1995
  • Physicochemical properties of Jeungpyun dough were analyzed during fermentation in the ranges of 0 to 10 hours. Solube Protein and total content of free amino acid of Jeungpyun dough were decreased at the early stage of fermentation, recording minimum value, 0.292 mg/g-dry matter and 13.31 mg/100g-dry matter at fermentation time, 2 hours and 4 hours respectively while they were increased since then. It was observed that, although few changes occurred at the early stage of fermentation, the height of peak on X-ray diffractogram was decreased somewhat and some disintegration of starch granule on scanning electron micrograph occurred slightly in dough samples of above 6 hours of fermentation time.

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SPAD(Sulfur Particle Autotrophic Denitrification) 공법의 고농도 질산성 질소 함유 페수에 대한 파일럿 스케일 적용사례

  • Park, U-Sin;Kim, Seong-Yeon;Beom, Min-Su;Kim, In-Su
    • 한국생물공학회:학술대회논문집
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    • 2002.04a
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    • pp.68-71
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    • 2002
  • SPAD(Sulfur Particle Autotrophic Denitrification) process is a biological denitrification process which uses elemental sulfur as an electron donor and a mall amount of organic to assist autotrophic denitrification. $^{1)}$SPAD process was applied to a nitrate containing wastewater (200-300mg $NO_3\;^-$ -N/L) with high concentration of $Ca^{2+}$ ion(5000-15000mg/L) from S. Steel Co. in Ulsan city, to est the feasibility of SPAD process. This pilot was operated from November 2001 to early March 2002, and the inner temperature of the pilot was controlled around $20^{\circ}C$. In spite of low temperature, denitrification efficiency was maintained above 90% achieving the average effluent $NO_3\;^-N$ concentration around 20mg$NO_3\;^-$ -N/L.

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Mechanical Properties of SiC Particulate Reinforced Mg Matrix Composites Fabricated by Melt Stirring Method (용탕교반법에 의한 SiC 입자강화 Mg기 복합재료의 기계적 특성)

  • Lim, Suk-Won;Choh, Takao;Park, Young-Jin
    • Journal of Korea Foundry Society
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    • v.13 no.5
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    • pp.441-449
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    • 1993
  • SiC particulate reinforced magnesium matrix composites were fabricated by melt stirring method. The effet of several factors on mechanical properties and the efficiency of melt stirring method from the viewpoint of these properties were investigated. The tensile strength increased and the elongation decreased with decrease of the particle size or the increase of the paticulate volume fraction for pure magnesium matrix and Mg-5%Zn alloy matrix composites. A longer stirring time improved the tensile strength of these composites. The tensile strength of Mg-5%Ca alloy matrix composites which shows no uniform paticulate distribution was a little lower than that of matrix alloy. Rapid solidification rate is preferred for the improved tensile strength of these composites. The pure magnesium matrix and Mg-5%Zn alloy matrix composites have tensile strength of about 400MPa. This value agrees with the tensile strength of some magnesium matrix composites fabricated by liquid infiltration method or powder metallurgy method at the same volume fraction of reinforcements of whisker or particle. Therefore, the melt stirring method which has the advantages of simple process is considered to be efficient in fabricating magnesium matrix composites.

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Removal of Lead from Sea Water using Electrolysis and Coprecipitation Method (전기분해와 공침법을 이용한 해수중의 납 제거)

  • Jin, Hong-Sung;Lee, Jae-Ho
    • Journal of Korean Society of Environmental Engineers
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    • v.32 no.2
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    • pp.149-154
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    • 2010
  • The feasibility of lead removal by electrolytic coprecipitation was investigated. Electrolysis bath was divided into anode and cathode chamber with anion exchange resin filled membrane. Sea water was electrolyzed and pH of the electrolyte in cathode chamber was increased. Consequently it induced the formation of $Mg(OH)_2$ and $CaCO_3$. The colloidal type precipitates, hich have high surface area, adsorbed lead ions in sea water and coprecipitated. Sea water electrolyses were conducted at different current density. Concentrations of Mg, Ca and Pb in the solution were measured with titration and ASV method. Morphology and crystallography were analyzed with SEM, EDS and XRD. As pH and current density increased, most of lead ions in the sea water were successfully removed.

Influence of Microstructures on Thermal Expansion Behavior of $Al_2TiO_{5}$ Ceramics ($Al_2TiO_{5}$ Ceramics의 열팽창거동에 대한 미세구조의 영향)

  • 김익진;이기성
    • Proceedings of the KAIS Fall Conference
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    • 2001.05a
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    • pp.40-46
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    • 2001
  • The thermal stability of $Al_2TiO_{5}$ ceramics was improved by formation of solid solution with MgO, such as $MgAl_2O_4$ spinel through electrofusion in an arc furnance, and by limitation of grain size and microcracks with $SiO_2$, $ZrO_2$ and ${\alpha}$-$Al_2O_3$. The low thermal expansion properties of $Al_2TiO_{5}$ composites show the thermal hysteresis curves due to the strong anisotropy of $Al_2TiO_{5}$. These phenomena are explained by the opening and closing of microcracks. The relation between thermal hysteresis, microstructures and sintering temperature were studied by dilatometry.