• 제목/요약/키워드: Metal replication

검색결과 30건 처리시간 0.029초

고대 금속활자의 복제를 위한 성분분석과 열역학적 주의 점 (Composition Analysis and Thermodynamic Care for Replication of Ancient Metallic Type)

  • 김기호
    • 한국표면공학회지
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    • 제45권3호
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    • pp.136-141
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    • 2012
  • 'Jikjisimcheyocheal (Jikji afterwards)' is known as a first book printed by the metal type in the world. The metal type used for printing this book has not been found yet. To help for replicating the original metal type, it is required to investigate the composition analysis of the copied metal type. In this study, the composition analysis and thermodynamic care for replicating of ancient metal type was performed on the basis of an analytical reports concerned with the ancient metal type which made after Jikji printing. Metal types were made by remelting and casting of the mother alloy which came from a cast of a mixed metals in accordance with the composition revealed in the literatures. Change of composition during remelting of mother alloy and casting of metal was detected by the EDS analysis. The reasons for variation in composition were discussed by metallurgical and thermodynamic point of view, and a mixing ratio of metals to get the original composition of ancient metal type is suggested. Some attention should be paid on mixing, melting and casting of metals to get an objected composition for copy of ancient metal type.

Three-Dimensional Digital-Mold Modeling and Sand-Printing for Replication of Bronze Mirror

  • Jo, Young Hoon;Lee, Jungmin
    • 보존과학회지
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    • 제37권1호
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    • pp.25-33
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    • 2021
  • To extend the application of digital technology to the replication of artifacts, meticulous details of the process and the diversity of three-dimensional (3D) printing output materials need to be supplemented. Thus, in this study, a bronze mirror with Hwangbichangcheon inscription was digitalized by 3D scanning, converted into a voxel model, and virtual conservation treatment was performed using a haptic device. Furthermore, the digital mold of the bronze mirror completed by Boolean modeling was printed using a 3D sand-printer. Such contactless replication based on digital technology reflects the stability, precision, expressivity, collectivity, durability, and economic feasibility of artifacts. Its application can be further extended to cultural products as well as such areas as education, exhibition, and research. It is expected to be in high demand for metal artifacts that require casting. If empirical studies through experimental research on casting are supplemented in the future, it could extend the application of digital technology-based contactless replication methods.

Fabrication of Hollow Metal Microcapsules with Mesoporous Shell Structure: Application as Efficient Catalysts Recyclable by Simple Magnetic Separation

  • Jang, Da-Young;Jang, Hyung-Gyu;Kim, Gye-Ryung;Kim, Geon-Joong
    • Bulletin of the Korean Chemical Society
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    • 제32권9호
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    • pp.3274-3280
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    • 2011
  • Monodispersed porous NiO and $Co_3O_4$ microcapsules with a hollow core were synthesized using SBA-16 silica sol and PS as a hard template. The porous hollow microcapsules were characterized by XRD, TEM and $N_2$ adsorption/desorption analysis. After $H_2$ reduction of metal oxide microspheres, they were conducted as an active catalyst in the reduction of chiral butylronitrile and cyanobenzene. The mesoporous metals having a hollow structure showed a higher activity than a nonporous metal powder and an impregnated metal on the carbon support.

메조기공을 갖는 다양한 금속 산화물 촉매를 이용한 사이클로헥사놀의 탈수소화 반응 (Highly Ordered Mesoporous Metal Oxides as Catalysts for Dehydrogenation of Cyclohexanol)

  • 이은옥;김명실;김지만
    • Korean Chemical Engineering Research
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    • 제51권4호
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    • pp.518-522
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    • 2013
  • 사이클로헥사논은 나일론의 단량체로 사용되는 카프로락탐의 원료로 중요한 중간체이며 사이클로헥사놀의 탈수소화반응을 통해 합성된다. 본 연구에서는 탈수소화 반응에 적용하기 위한 촉매로 다양한 메조기공을 가진 금속 산화물(meso-$WO_3$, meso-$TiO_2$, meso-$Fe_2O_3$, meso-CuO, meso-$SnO_2$, meso-NiO)을 나노 복제법에 의해 합성하였다. 그 결과 meso-$WO_3$ >> meso-$Fe_2O_3$ > meso-$SnO_2$ > meso-$TiO_2$ > meso-NiO > meso-CuO 순서로 촉매 활성이 나타났으며, 그 중 meso-$WO_3$가 가장 높은 촉매 활성을 보임을 알 수 있었다. 따라서 사이클로헥사놀을 이용한 탈수소화 반응에 meso-$WO_3$의 폭넓은 응용 가능성을 확인하였다.

Fabrication of Plasmon Subwavelength Nanostructures for Nanoimprinting

  • Cho, Eun-Byurl;Yeo, Jong-Souk
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제43회 하계 정기 학술대회 초록집
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    • pp.247-247
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    • 2012
  • Plasmon subwavelength nanostructures enable the structurally modulated color due to the resonance conditions for the specific wavelength range of light with the nanoscale hole arrays on a metal layer. While the unique properties offered from a single layer of metal may open up the potential applications of integrated devices to displays and sensors, fabrication requirements in nanoscale, typically on the order of or smaller than the wavelength of light in a corresponding medium can limit the cost-effective implementation of the plasmonic nanostructures. Simpler nanoscale replication technologies based on the soft lithography or roll-to-roll nanoimprinting can introduce economically feasible manufacturing process for these devices. Such replication requires an optimal design of a master template to produce a stamp that can be applied for a roll-to-roll nanoimprinting. In this paper, a master mold with subwavelength nanostructures is fabricated and optimized using focused ion beam for the applications to nanoimprinting process. Au thin film layer is deposited by sputtering on a glass that serves as a dielectric substrate. Focused ion beam milling (FIB, JEOL JIB-4601F) is used to fabricate surface plasmon subwavelength nanostructures made of periodic hole arrays. The light spectrum of the fabricated nanostructures is characterized by using UV-Vis-NIR spectrophotometer (Agilent, Cary 5000) and the surface morphology is measured by using atomic force microscope (AFM, Park System XE-100) and scanning electron microscope (SEM, JEOL JSM-7100F). Relationship between the parameters of the hole arrays and the corresponding spectral characteristics and their potential applications are also discussed.

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나노 복화공정의 역방향 적층법을 이용한 직접적 나노패턴 생성에 관한 연구 (Directly Nano-precision Feature Patterning on Thin Metal Layer using Top-down Building Approach in nRP Process)

  • 박상후;임태우;양동열;공홍진
    • 한국정밀공학회지
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    • 제21권6호
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    • pp.153-159
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    • 2004
  • In this study, a new process to pattern directly on a thin metal layer using improved nano replication printing (nRP) process is suggested to evaluate the possibilities of fabricating a stamp for nano-imprinting. In the nRP process, any figure can be replicated from a bitmap figure file in the range of several micrometers with nano-scaled details. In the process, liquid-state resins are polymerized by two-photon absorption which is induced by femto-second laser. A thin gold layer was sputtered on a glass plate and then, designed patterns or figures were developed on the gold layer by newly developed top-down building approach. Generally, stamps fur nano-imprinting have been fabricated by using the costly electron-beam lithography process combined with a reactive ion-etching process. Through this study, the effectiveness of the improved nRP process is evaluated to make a stamp with the resolution of around 200nm with reduced cost.

Expression and characterization of RNA-dependent RNA polymerase of Ectropis obliqua virus

  • Lin, Meijuan;Ye, Shan;Xiong, Yi;Cai, Dawei;Zhang, Jiamin;Hu, Yuanyang
    • BMB Reports
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    • 제43권4호
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    • pp.284-290
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    • 2010
  • Replication of positive-strand RNA virus is mediated by a virus-encoded RNA-dependent RNA polymerase (RdRp). To study the replication of Ectropis obliqua virus (EoV), a newly identified insect virus belonging to the family Iflaviradae, we expressed the RNA polymerase domain in Escherichia coli and purified it on a Ni-chelating HisTrap affinity column. It is demonstrated that EoV RdRp initiated RNA synthesis in a primer and poly (A)-dependent manner in vitro. Furthermore, the effect of primer concentration, temperature, metal ions ($Mg^{2+}$, $Mn^{2+}$, and $K^+$) on enzymatic activity were determined. Our study represented a first step towards understanding the mechanism of EoV replication.

나노 복화(複畵)공정을 이용한 PDMS 스탬프 제작 (Fabrication of a PDMS (Poly-Dimethylsiloxane) Stamp Using Nano-Replication Printing Process)

  • 박상후;임태우;양동열;공홍진
    • 대한기계학회논문집A
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    • 제28권7호
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    • pp.999-1005
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    • 2004
  • A new stamp fabrication technique for the soft lithography has been developed in the range of several microns by means of a nano-replication printing (nRP) process. In the nRP process, a figure or a pattern can be replicated directly from a two-tone bitmap figure with nano-scale details. A photopolymerizable resin was polymerized by the two-photon absorption which was induced by a femtosecond laser. After the polymerization of master patterns, a gold metal layer (about 30 ㎚ thickness) was deposited on the fabricated master patterns for the purpose of preventing a join between the patterns and the PDMS, then the master patterns were transferred in order to fabricate a stamp by using the PDMS (poly-dimethylsiloxane). In the transferring process, a few of gold particles, which were isolated from the master patterns, remained on the PDMS stamp. A gold selective etchant, the potassium iodine (KI) was employed to remove the needless gold particles without any damage to the PDMS stamp. Through this work, the effectiveness of the nRP process with the PDMS molding was evaluated to make the PDMS stamp with the resolution of around 200 ㎚.