• Title/Summary/Keyword: Metal Powders

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토양 제염에 있어서 magnetite 용해 거동 연구

  • 원휘준;김민길;김계남;박진호;오원진
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2003.04a
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    • pp.393-396
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    • 2003
  • Soil contains the several kinds of metal oxides. Magnetite in soil may contribute the generation of secondary waste during the decontamination of soil by citric acid. Dissolution of magnetite powders by citric acid was investigated in the pH range between 2.0 and 5.0. The dissolution behaviour of magnetite was well described by the equation, A[1 - $e^{-B(x-c)}$]. The parameters of the equation were optimized by the iteration method, and the physical meaning of each parameter was explained. Concentration of each of the dissociated chemical species of citric acid was calculated using the ionization constants. The dissolution reaction was explained by the concentration of the dissociated chemical species of citric acid.d.

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Powder Production of CuAINi Base Alloy via Rotating Disk Atomization (회전원반분사법에 의한 CuA1Ni계 합금 분말제조)

  • 류봉선
    • Journal of Powder Materials
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    • v.1 no.2
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    • pp.145-152
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    • 1994
  • Atomizing mode and powder characteristics of CuA1Ni base shape memory alloy in rotating disk atomization were investigated in accordance with disk materials and additional elements. Produced powders were classified into two types of spherical and flake shape. In the case of CuAlNiBTi and CuAlNiZr alloy, high yield rate and fine powder were obtained. This tendency was same when we used oxide coated disks. We concluded that this results were steno from the wetting characteristics change between molten metal and disk surface. Especially, due to the reactive properties of Ti and Zr with ceramic disk, the change of atomizing appearance and powder characteristics were noticeable.

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Study on Synthesis and Mechanical Properties of $B_4C$ by Self Propagating High Temperature Synthesis Chemical Furnace (SHS 화학로에 의한 $B_4C$ 합성 및 기계적 특성에 관한 연구)

  • Lee, Hyung-Bock;Cho, Duk-Ho;Park, Sung;Le, Jea-Won
    • Journal of the Korean Ceramic Society
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    • v.30 no.8
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    • pp.685-693
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    • 1993
  • Boron cabride was prepared from the mixture of metal boron and graphite powders in Argon atmosphere by Self-propagating High-temperature Synthesis Chemical furnace. The most excellent mechanical properties were in the case that Fe was added as a sintering agent before the synthesis of the B4C in the Chemical furnace. Sintered B4C-5wt% Fe specimen showed the relative density of 95%, of theoretical value, and 3-point-flexural strength of 380MPa.

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A Study on Synthesis and Characterization of $Ti_xZr_{1-x}C$ Solid-Solution by Self-propagation High Temperature Synthesis Method (SHS법에 의한 $Ti_xZr_{1-x}C$ 고용체의 합성 및 특성 연구)

  • 이형복;오유근;이성민
    • Journal of the Korean Ceramic Society
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    • v.34 no.7
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    • pp.731-737
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    • 1997
  • TixZr1-xC(0$0^{\circ}C$, 5.1 mm/sec respectively. The relative density, three point flexural strength, and the hardness of composites, which was sintered at 190$0^{\circ}C$ for 60 min by using hot-pressing under a pressure of 30 MPa, were 99%, 525 MPa and 24 GPa respectively.

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Synthesis and Characterization of Ti-B System Ceramics Prepared by Self-Propagating High-Temperature Synthesis Method (SHS법에 의한 Ti-B 계 세라믹스의 합성 및 소결특성)

  • 이형복;최일선;오응주;여철현
    • Journal of the Korean Ceramic Society
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    • v.28 no.3
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    • pp.234-242
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    • 1991
  • Ti-B system ceramics were prepared by the self-propagating high-temperature synthesis method from the mixture of metal titanium and boron powders The major crystalline phase as a function of boron content was TiB for mixtures containing 0.5 or 1.0mol B, and TiB2 for these containing over 1.3mol B. The combustion mode observed by a high-speed camera was steady-state. The Combustion velocity increased with increasing the boron content. Sintered TiB2 specimen showed the density of 97% of theoretical valve, Vicker's hardness of 2250kg/㎟ for 0.2kg load and three-point-flexure strength of 500MPa.

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TLP and Wire Bonding for Power Module (파워모듈의 TLP 접합 및 와이어 본딩)

  • Kang, Hyejun;Jung, Jaepil
    • Journal of the Microelectronics and Packaging Society
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    • v.26 no.4
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    • pp.7-13
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    • 2019
  • Power module is getting attention from electronic industries such as solar cell, battery and electric vehicles. Transient liquid phase (TLP) boding, sintering with Ag and Cu powders and wire bonding are applied to power module packaging. Sintering is a popular process but it has some disadvantages such as high cost, complex procedures and long bonding time. Meanwhile, TLP bonding has lower bonding temperature, cost effectiveness and less porosity. However, it also needs to improve ductility of the intermetallic compounds (IMCs) at the joint. Wire boding is also an important interconnection process between semiconductor chip and metal lead for direct bonded copper (DBC). In this study, TLP bonding using Sn-based solders and wire bonding process for power electronics packaging are described.

High Temperature Superconducting (HTS) Films by EPD Method addition with $BaF_2$ and PEG

  • Soh, Deawha;Korobova, N.;Park, Jung-Cheul;Jeun, Yong-Woo
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.250-254
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    • 2000
  • High temperature superconducting films deposited on metal Ag wire were prepared with YBCO powders by electrophoretic deposition method. $I_2$was used as additives for surface charge of YBCO particles. When 2~3 wt.% $BaF_2$ was added in the YBCO suspension, the pores and cracks of film surface were decreased and film density could be increased. In case of YBCO films, the critical current density ($J_{c}$) was calculated at the value of $1458{\;}A/\textrm{cm}^2$ (77K, 0K) by 4 point prove method.

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Properties and Shape Control of YAG Powder Prepared by Hydrothermal Reaction (수열반응 조건에 의한 YAG 분말의 특성과 형상제어)

  • 지성훈;김상문;구자인;김태옥
    • Journal of the Korean Ceramic Society
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    • v.37 no.8
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    • pp.739-744
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    • 2000
  • YAG(Y3Al5O12) as host material of YAG:Tb3+ was studied via hydrothermal synthesis of metal hydroxides. We changed the kind of mineralizer, the concentrations and process conditions in hydrothermal synthesis. As a result, we found, acicular YAG powders were obtained by the use of KOH as a mineralizer, the concentration of KOH affected the shape and size of YAG powder. Fine grained YAG were perpared by the use of NH4OH as a mineralizer and the concentration of NH4OH affected crystal phases but did not affect particle size. We could finally get the spherical looking YAG powder at 8 M NH4OH and at 35$0^{\circ}C$ for 12h. The average particle size was about 0.2${\mu}{\textrm}{m}$.

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Highly Donor-doped $Ba_{1-x}La_{x}TiO_{3}$ Semiconductive Ceramics

  • Soh, Dea-Wha;Korobova N.
    • Journal of information and communication convergence engineering
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    • v.1 no.1
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    • pp.31-34
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    • 2003
  • Sol-gel processing of $BaTiO_{3}$ ceramics doped with La (0.01∼1.00 at.%) were prepared from metal barium, titanium n-butoxide and lanthanum isopropoxide. Characterization of the sol-gel-derived powder using XRD, SEM is also reported. The obtained results suggested that insulator to semiconductor transition for highly donor-doped barium titanate was closely related to the incorporation of donor into the grains and to the resultant grain size, which were significantly affected by the sinterability of $BaTiO_{3}$ powders and sintering conditions used.