• 제목/요약/키워드: Metal Powder

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OPTIMIZATION OF VARIABLES AFFECTING CORROSION RESISTANCE OF VACUUM SINTERED STAINLESS STEELS

  • Klar, Erhard;Samal, Prasan
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 1995.11a
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    • pp.9-9
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    • 1995
  • MATERIAL AND PROCESS VARIABLES THAT STRONGLY AFFECT THE CORROSION RESISTANCE OF PA4 STAINLESS STEELS, INCLUDE : ALLOY COMPOSITION, POWDER CLEANLINESS, NITROGEN, OXYGEN AND GARBON CONTENTS, CHROMIUM DEPLETION DUE TO SURFACE EVAPORATION AND SINTERED DENSITY. THE OPTIMUM PROCESS PARAMETERS FOR DELUBRICATION AND SINTERING THAT RESULT IN LOWEST LEVELS OF NITROGEN, OXYGEN AND CARBON AND MINIMUM LEVELS OF CHROMIUM DEPLETION WILL BE PRESENTED, FOR A NUMBER OF AUSTENTIC AND FERRITIC STAINLESS STEELS. THE EFFECT OF SINTERED DENSITY ON THE CORROSION RESISTANCE OF BOTH AUSTENITIC AND FERRITIC GRADES OF STAINLESS STEEL WILL ALSO BE COVERED.

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Solid Freeform Fabrication of Metal Prototype Using Direct Metal Shaping Process (직접식 금속 적층공정을 이용한 금속 시제품 제작)

  • Kim, Jae-Do;Park, Jin-Yong;Cho, Myeong-Woo
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.10
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    • pp.56-62
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    • 2000
  • A fast and precise technique to make 3-dimensional object which is called direct metal shaping process is processed. It is very useful technique in design and inspection. Using this developed system, a solid object is made. In experiment, test parts are built by varying three factors, laser power, scan path, scan speed. This process used device, which is different from the widely used in rapid prototyping in that powder feeding device is used. Spraying powder directly at the focused laser beam and then three dimensional object is made by the deposit of melted metal powder. The optimum scanning path is found to be zigzag path, which had little thermal affection on base metal. As a result of these experiments, it was found that optimum scanning speed is 15mm/sec laser power is 50W. This constructed 3-dimensional object could be used in mold manufacturing directly.

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Analysis of Wafer Cleaning Solution Characteristics and Metal Dissolution Behavior according to the Addition of Chelating Agent (착화제 첨가에 따른 웨이퍼 세정 용액 특성 분석 및 금속 용해 거동)

  • Kim, Myungsuk;Ryu, Keunhyuk;Lee, Kun-Jae
    • Journal of Powder Materials
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    • v.28 no.1
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    • pp.25-30
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    • 2021
  • The surface of silicon dummy wafers is contaminated with metallic impurities owing to the reaction with and adhesion of chemicals during the oxidation process. These metallic impurities negatively affect the device performance, reliability, and yield. To solve this problem, a wafer-cleaning process that removes metallic impurities is essential. RCA (Radio Corporation of America) cleaning is commonly used, but there are problems such as increased surface roughness and formation of metal hydroxides. Herein, we attempt to use a chelating agent (EDTA) to reduce the surface roughness, improve the stability of cleaning solutions, and prevent the re-adsorption of impurities. The bonding between the cleaning solution and metal powder is analyzed by referring to the Pourbaix diagram. The changes in the ionic conductivity, H2O2 decomposition behavior, and degree of dissolution are checked with a conductivity meter, and the changes in the absorbance and particle size before and after the reaction are confirmed by ultraviolet-visible spectroscopy (UV-vis) and dynamic light scattering (DLS) analyses. Thus, the addition of a chelating agent prevents the decomposition of H2O2 and improves the life of the silicon wafer cleaning solution, allowing it to react smoothly with metallic impurities.

The Possibility of Utilizing Stone Powder Sludges as Adsorbents for Heavy Metals (중금속 흡착제로서 석분슬러지의 활용 가능성)

  • 진호일;민경원
    • Economic and Environmental Geology
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    • v.33 no.6
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    • pp.519-524
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    • 2000
  • This study has been performed to evaluate the possibility of utilizing stone powder sludges from stone quarry and manufacturing plant as adsorbents for heavy metals in industrial wastewater. The stone powder sludges from stone quarry (IS-01) have the most effective adsorption capacity (above 95% of initial concentrations) under the given experimental conditions of reaction times (Pb : 15 min, Cu : 2 hr, Zn : 48 hr), initial acidity of solution (pH>3) and dosage (sludge/liquid ratio : 0.02). The stone powder sludges from manufacturing plant (CW-01) show relatively high adsorption capacity (about 95% of initial concentrations) only for Pb with a reaction times of 12 hours, initial acidity of solution (pH>3) and dosage (sludge/liquid ratio : 0.02). The stone powder sludges (IS-01) from stone quarry having relatively excellent adsorption capacity under the given experimental conditions show their potential utilization as heavy metal adsorbents.

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Synthesis of $Fe_4N$ Powder and Its Magnetic Properties for Magnetic Recording (자기기록용 $Fe_4N$ 분말의 합성 및 자기특성)

  • 변태봉;오재희
    • Journal of the Korean Ceramic Society
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    • v.28 no.2
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    • pp.93-100
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    • 1991
  • For determination the optimum manufacturing condition Fe4N powder for magnetic recording media, we have studied the following important conditions : the effect of particle size of metal powder on the nitridation, the condition of nitridation on the formation and magnetic properties of Fe4N, and stability of Fe4N powder against temperature and change on standing. The results can be summarized as : 1) Single phase Fe4N is formed at 50v/o of ammonia concentration during the nitridation reaction, 2) Single phase Fe4N is formed above 40$0^{\circ}C$, 15min regardless of the metal powder sizes, 3) Coercivity and saturation magnetization of Fe4N powder almost constant value until 20 day-passing from preparation date.

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Attrition Milling and Reaction-Sintering of the Oxide-Metal Mixed Powders: I. Milling Behavior as the Powder Characteristics (산화물과 금속 복합 분말의 Attrition Milling 및 반응소결: I. 분말의 특성에 따른 분쇄 거동)

  • 황규홍;박정환;윤태경
    • Journal of the Korean Ceramic Society
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    • v.31 no.3
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    • pp.337-345
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    • 1994
  • The reaction-sintered alumina and zirconia-alumina ceramics having low firing shrinkage were prepared from the Al/Al2O3 or Al/ZrO2(Ca-PSZ) powder mixtures via the attrition milling. And in this milling process the effect of the characteristics of used powders was investigated. Attrition milling was much more effective in reducing the particle size of ceramic/metal mixed powders than ball milling. Powder mixtures of flake-type Al with coarse alumina was much more effectively comminuted by the attrition milling than the mixtures of globular-type Al with coarse alumina powders. And coarse alumina than fine alumina was much more beneficial in cutting and reducing the ductile Al particles. In the contrary to Al/Al2O3 powder mixtures, Al/ZrO2 powder mixtures was not effectively comminutd. But whether using the alumina ball media or attrition milled with Al2O3 powder rather than Al, the milling efficiency was much more increased.

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Green Body Behaviour of High Velocity Pressed Metal Powder

  • Jonsen, P.;Haggblad, H.A.;Troive, L.;Furuberg, J.;Allroth, S.;Skoglund, P.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.22-23
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    • 2006
  • High velocity compaction (HVC) is a production technique with capacity to significantly improve the mechanical properties of powder metallurgy (PM) parts. Investigated here are green body data such as density, tensile strength, radial springback, ejection force and surface flatness. Comparisons are performed with conventional compaction using the same pressing conditions. Cylindrical samples of a pre-alloyed water atomized iron powder are used in this experimental investigation. The HVC process in this study resulted in a better compressibility curve and lower ejection force compared to conventional quasi static pressing. Vertical scanning interferometry measurements show that the HVC process gives flatter sample surfaces.

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