• Title/Summary/Keyword: Measurement Standard

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Measurement Uncertainty for Analytical Method of Hyaluronic Acid Used as a Dietary Supplement (식이보충제로 사용되는 히알루론산의 분석법에 대한 불확도 산정)

  • Park, Sang-Wook;Kim, Hyung Bum;Kim, Kwang Joon;Lee, Wonjae
    • KSBB Journal
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    • v.32 no.1
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    • pp.54-62
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    • 2017
  • This study aimed to estimate the measurement uncertainty related to determination of hyaluronic acid used as a dietary supplement by high-performance liquid chromatography. According to the guidelines of the Association of Official Analytical Chemists, the analytical processes for determination of hyaluronic acid were performed. And the measurement uncertainty obtained during the analytical processes were expressed in accordance with mathematical/ statistical guidances of GUM (Guide to the Expression of Uncertainty in Measurement) & EURACHEM (Focus for Analytical Chemistry in Europe) for the analytical operations. For the uncertainty in measurement produced based on this analytical method, the expanded uncertainty was calculated by using the relative standard uncertainty between analytical results and sources of uncertainty in measurement (sample weight, final volume, extraction volume, standard solution, matrix and instrument etc). In the results of 95% confidence interval, it was calculated that the uncertainty in measurement was $57.75{\pm}8.76{\mu}g/kg$ (k=2.0). Therefore, it showed that the measurement uncertainty obtained by this analytical method influences on 15.2% of the contents of hyaluronic acid as the analytical results.

Analysis on the Vibration Transmission Characteristics of the Standard Test Building by Using Standard Impact Source (경량 및 중량 충격원에 의한 표준 실험동의 진동전달 특성 분석)

  • Jin, Pil-Hwa;Kim, Heung-Sik;Kim, Do-Heong
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.11a
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    • pp.371-371
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    • 2006
  • The purpose of this study is to provide a fundamental data for efficient and economical reduction method and predict ion method of floor impact noise. In order to get the useful results, the measurement on the vibration transmission characteristics of standard test building with four rooms by using heavy and light-weighed impact source were carried out. In this measurement various conditions such as the change of test structure construction, the pick-up sensor location, the excitation posit ion, and the resilient material types were applied to get the vibration characteristics transmitted from excitation room to adjacent rooms.

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EM Coupling Effect of sprint inductors by isolation methode in standard CMOS process (Spiral 인덕터 간 격리방법에 따른 Electromagnetic 커플링 효과)

  • Choi, Moon-Ho;Kim, Han-Seok;Jung, Sung-Il;Kim, Yeong-Seuk
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.91-92
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    • 2005
  • The electromagnetic coupling effect in standard CMOS process is simulated and evaluated. EM coupling transfer characteristic between planar spiral inductors by isolation methode in standard CMOS have simulated and measured. Measurement results show that suppression of EM coupling effect by ground guardring. The evaluated structures are fabricated 1P5M(one poly, five metal) 0.25um standard CMOS process. These measurement results provide a isolation design guidelines in standard CMOS process for Rf coupling suppression.

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Development of Standard Calibration System for the Rain Gauges by Weighting Method (질량측정에 의한 우량계 표준교정시스템 개발)

  • Shin Gang-Wook;Hong Sung-Tack
    • Journal of Institute of Control, Robotics and Systems
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    • v.12 no.8
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    • pp.818-823
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    • 2006
  • Because the rain gauges of tipping bucket type can easily use the digital signal, the rain gauges are widely used for the meteorological observation. In general, the resolution of rain gauges of tipping bucket type can be categorized by the 0.1mm, 0.5mm, and 1.0mm classes. But, the error of the tipping bucket rain gauges is made by the intensity of rainfalls and is expected to make the standard calibration method for error measurement. Thus, we developed the hardware of standard calibration facility for rain gauges by weighting measurement method and proposed the standard procedure by rainfall intensity in this study Also, we calculated the uncertainty for the rainfall intensity and obtained useful result through the proposed calibration method.

Mass measuremeant of soilid density standard using weight exchanger (분동교환기를 이용한 고체밀도기준물의 질량측정)

  • 이용재;장경호;오재윤;정상덕
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1659-1662
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    • 2003
  • The mass measurement of solid density standards using weight exchanger is described. KRISS(Korea Research Institute od Standards and Science) has several solid density standards. Their mass have been measured manually only using a mass comparator(Mettler, 1kg - 0.01mg). However, the uncertaity of the manual mass measurement is up to 300 microgarm much more than 32 microgram of advanced NMIS(National Metrology Institutes) for 1 kg silicon sphere which is primary density standards due to an eccentric error and buoyancy correction error. The new system with a weight exchanger is designed and built to improve the measurement accuracy. It comprises a weight exchager, a mass comparator, air density instruments, and application program for automatic measurement. It is evaluated by measuring several elements in an air tight chamber to verify the performance of it.

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The effect of diffusers on the measurement of sound absorption in a reverberation room (잔향실법 흡음률 측정에 미치는 확산체의 영향)

  • Han, Hee-Kab;Kim, Kyung-Ho
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.05a
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    • pp.1194-1197
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    • 2006
  • Recently, international standard for measurement of sound absorption in a reverberation room has been amended. In the revised version, temperature, humidity and air pressure conditions are strictly restricted and also the concrete procedures are presented to reduce the differences in test results by adding inspection of diffusion, measurement uncertainty etc. In this paper, the systematic tests are conducted based on the inspection guide of diffusion defined by ISO 354 and the effects of diffusers on the measurement of sound absorption ratio are considered. As a result, we perceived that the averaged sound absorption ratio in mid and high frequency range is expected to measure around $0.05{\sim}0.1$ higher in high sound absorption material. Therefore, as for the reverberation room for measurement of sound absorption, we need to take into consideration not only the spatial standard deviation of sound pressure mandated by ISO 3741, but also, inspection regulation of diffusion showed by ISO 354.

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A Study on the Evaluation of Measurement Uncertainty for the National Calibration and Test Organizations (Liquid Flow) (국가교정검사기관(액체유량)의 측정불확도 평가 및 비교연구)

  • 임기원
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.12 no.11
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    • pp.1012-1019
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    • 2000
  • A proficiency test is one of programs which Korea Research Institute of Standards and Science(KRISS), as national metrology institute, is putting in operation for the mutual recognition arrangement. The Fluid Flow Group of KRISS evaluated the measurement capability for liquid flowmeter calibrator of the national calibration and test organizations. The uncertainty of national standard system was estimated in accordance with Guide to The Expression of Uncertainty in Measurement (ISO), and the turbine flowmeter, which was used for the round-robin test as a reference flowmeter, was characterized. The round-robin tests with the turbine flowmeter package were carried out in 1995 and 1999. The test results of the organizations and those of KRISS agreed within $\pm0.2$%. It is found thus that the organizations have the traceability of the national standard for liquid flow measurement.

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A Study on Estimation uncertainty of measurement in mechanical characteristic exam for Plastic materials (플라스틱재료의 기계적 특성시험 불확도추정에 대한 고찰)

  • Kim Won-kyung;Kwon Sung-Tae;Kim Jung-Nam
    • Proceedings of the KSR Conference
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    • 2003.10c
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    • pp.301-306
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    • 2003
  • Recently, uncertainty of measurement became a major concern for the people working on the laboratory evaluation and accreditation. 'uncertainty of measurement is a parameter associated with the result of a measurement that characteristics the dispersion of the value that could reasonably be attributed to the measured.' This study analysed how to estimate uncertainty of measurement in mechanical characteristic exam for Plastic material. its uncertainty was estimated according to International Organization for Standardization(ISO), they were named to A type uncertainty, B type uncertainty, combined standard uncertainty, and expanded uncertainty. We obtained that the combined standard uncertainty was 0.96697 MPa and the expanded uncertainty was 2.291MPa.

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Quantitative Evaluation of Rehabilitation Therapy Based on a Two-Finger Force Measurement System

  • Kim, Gab-Soon
    • Journal of Sensor Science and Technology
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    • v.23 no.6
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    • pp.357-361
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    • 2014
  • This paper describes the evaluation of the effectiveness of rehabilitation therapy for patients with finger paralysis based on a two-finger force measurement system (TFFMS). The paralyzed fingers can be recovered through rehabilitation therapies. The finger pressing force of the patients can be measured utilizing the TFFMS previously developed by the author [7]. The TFFMS, however, has not been fully adopted as a standard method for evaluating the therapy owing to the lack of a standard protocol. The pressing force of healthy volunteers and patients is analyzed with the TFFMS to explore the feasibility of the TFFMS as an evaluation device. The test confirms that the established standard protocol is useful to quantitatively assess the progress of finger rehabilitation therapy.

Analysis of Calibration Facilities for Acoustic Doppler Current Profilers (ADCPs) (초음파 도플러 유속계 교정 시설 현황)

  • Lee, Jung-Han;Hwang, Keun-Choon;Kim, Eun-Soo
    • Ocean and Polar Research
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    • v.33 no.2
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    • pp.171-183
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    • 2011
  • Despite technological developments and application advances of Acoustic Doppler Current Profilers (ADCPs), no standard procedure has been adopted or accepted for calibration of ADCPs. Limitations of existing facilities for calibrating ADCPs, the complexity of ADCP instruments, and rapid changes in ADCP technology are some of the reasons why a standard procedure has not been adopted. However, there is increasing realization of the need for effective Quality Assurance (QA) and as part of that the importance of standardized calibration. In this study, the significance of calibration and QA plans for ADCPs is discussed and the calibration facilities for ADCPs at home and abroad are reported. Furthermore, the method for calibrating ADCPs using a towed car and its limitations are discussed. This study contributes to discussions surrounding the establishment of standard procedures for calibrating ADCPs and QA plans, and the construction of calibration facilities in the future.