• Title/Summary/Keyword: Matrix phase

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Phase Decomposition and Strength of B2-Ordered (Ni,Co)Al (B2형 규칙(Ni,Co)Al의 상분리와 강도)

  • Han, Chang-Suck;Kim, Youn-Che
    • Journal of the Korean Society for Heat Treatment
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    • v.9 no.2
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    • pp.79-90
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    • 1996
  • Transmission electron microscopy(TEM) investigation on the phase decomposition of B2-ordered (Ni,Co)Al supersaturated with Ni and Co has revealed the precipitation of $(Ni,Co)_2Al$ which has not been expected from the reported equilibrium phase diagram. The $(Ni,Co)_2Al$ phase has a hexagonal struture and takes a rod-like shape with the long axis of the rod parallel to the <111> directions of the B2 matrix. By aging at temperatures below 873 K, a long period Superlattice Structure appears in the hexagonal $(Ni,Co)_2Al$ Phase. The orientation relationship between the $(Ni,Co)_2Al$ Precipitates and the B2-(Ni,Co)Al matrix is found to be$(0001)_p$ // $(111)_{B2}$ and $[\bar{1}2\bar{1}0]_P$ // $[\bar{1}10]_{B2}$, Where the suffix p and B2 denote the $(Ni,Co)_2Al$ precipitate and the B2-(Ni,Co)Al matrix, respectively. (Ni,Co)Al hardens appreciably by the fine precipitation of the $(Ni,Co)_2Al$ phase. Energy dispersive spectroscopy was used to analyze the compositions of each phase formed in B2-(Ni,Co)Al.

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Cavitating Flow Simulation Using Two-Fluid Two-Phase Flow Model and HLL Scheme (이유체 이상유동 모델과 HLL 스킴을 이용한 캐비테이션 유동 해석)

  • Yeom Geum-Su;Chang Keun-Shik
    • 한국전산유체공학회:학술대회논문집
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    • 2005.04a
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    • pp.219-222
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    • 2005
  • A compressible two-fluid two-phase flow computation model using the stiffened-gas equation of state is formulated. Since the conservation equation system is of mixed type, it gives complex eigenvalues. The sonic speeds obtained from the individual single phase have been simply used in the literature for the fastest wave speeds necessary in the HLL scheme. This method has worked fine but proved to be quite diffusive according to our test. To improve the accuracy, we here propose to utilize the analytic eigenvalues evaluated from an approximate Jacobian matrix lot the fastest wave speeds. The interfacial transfer terms were dropped in constituting the Jacobian matrix for this purpose. The present scheme proved efficient, robust and accurate in comparison with other existing methods. We solved the cavitating flow problem using the present scheme. The result shows more detailed wave structure in the cavitating process caused by the strong expansion waves.

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Study of Spectral Factorization using Circulant Matrix Factorization to Design the FIR/IIR Lattice Filters (FIR/IIR Lattice 필터의 설계를 위한 Circulant Matrix Factorization을 사용한 Spectral Factorization에 관한 연구)

  • 김상태;박종원
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.7 no.3
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    • pp.437-447
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    • 2003
  • We propose the methods to design the finite impulse response (FIR) and the infinite impulse response (IIR) lattice filters using Schur algorithm through the spectral factorization of the covariance matrix by circulant matrix factorization (CMF). Circulant matrix factorization is also very powerful tool used fur spectral factorization of the covariance polynomial in matrix domain to obtain the minimum phase polynomial without the polynomial root finding problem. Schur algorithm is the method for a fast Cholesky factorization of Toeplitz matrix, which easily determines the lattice filter parameters. Examples for the case of the FIR Inter and for the case of the IIR filter are included, and performance of our method check by comparing of our method and another methods (polynomial root finding and cepstral deconvolution).

Application of dynamic matrix control (Dynamic Matrix Control의 응용)

  • Moon, Il;Eyo, Young-Koo;Song, Hyung-Keun;Park, Won-Hee
    • 제어로봇시스템학회:학술대회논문집
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    • 1987.10b
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    • pp.652-657
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    • 1987
  • The Dynamic Matrix Control(DMC) technique was applied to nonlinear and nonminimum phase system. System model was identified by using Least Square method. Desired output trajectory was prespecified and input suppression parameter was also introduced. It was shown that DMC technique worked with great success in solving both nonminimum phase system and nonlinear system.

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Temperature Dependence of Thermo-Mechanical Properties of Banana Fiber-Reinforced Polyester Composites

  • Shaktawat, Vinodini;Pothan, Laly A.;Saxena, N.S.;Sharma, Kananbala;Sharma, T.P.
    • Advanced Composite Materials
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    • v.17 no.1
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    • pp.89-99
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    • 2008
  • Using a Dynamic Mechanical Analyzer (DMA), mechanical properties like modulus and phase transition temperature of polyester composites of banana fibers (treated and untreated) are measured simultaneously. The shifting of phase transition temperature is observed in some treatments. The performance of the composite depends to a large extent on the adhesion between polymer matrix and the reinforcement. This is often achieved by surface modification of the matrix or the filler. Banana fiber was modified chemically to achieve improved interfacial interaction between the fiber and the polyester matrix. Various silanes and alkalies were used to modify the fiber surface. Chemical modification was found to have a profound effect on the fiber/matrix interaction, which is evident from the values of phase transition temperatures. Of the various chemical treatments, simple alkali treatment with 1% NaOH was found to be the most effective.

Precipitation of Icosahedral Qusicrystal Phase in Mg-Zn-Y(ZW61) alloy (Mg-Zn-Y(ZW61) 합금에서 Icosahedral 준결정상의 석출)

  • Kwak, Ho-Yeon;Lee, Kap-Ho
    • Korean Journal of Materials Research
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    • v.21 no.3
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    • pp.168-173
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    • 2011
  • Precipitation of the ordered icosahedral quasicrystal in Mg-6wt%Zn-1wt%Y alloy has been characterized by transmission electron microscopy observations. The lamellar-type icosahedral qusicrystal phases (I-phase) with the face-centered icosahedral (FCI) structure are observed in alloy after solution treatment at $550^{\circ}C$. In the alloy annealed at $400^{\circ}C$, polygon-shaped I-phases are observed in the ${\alpha}$-Mg matrix. The interfaces of the I-phase with the matrix are facetted and the facets are on five-fold and two- fold plane of the I-phase. The orientation relationship of the I-phase with the matrix is determined to be $[I5]_I//[001]_{Mg}$, $(2f)_I//(2\overline{1}0)_{Mg}$ and $[I2]_I//[311]_{Mg}$, $(5f)_I//(0\overline{1}1)_{Mg}$. The icosahedral grains are occasionally found to be twinned with one of the five-fold axis as the twin axis. The twin boundaries appear to be fairly straight and perpendicular to the fivefold twin axis. The icosahedral twin can be expressed as a rotation of $63.4^{\circ}$ or $116.62^{\circ}$ around two fold zone axis.

A Control Strategy Based on Small Signal Model for Three-Phase to Single-Phase Matrix Converters

  • Chen, Si;Ge, Hongjuan;Zhang, Wenbin;Lu, Song
    • Journal of Power Electronics
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    • v.15 no.6
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    • pp.1456-1467
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    • 2015
  • This paper presents a novel close-loop control scheme based on small signal modeling and weighted composite voltage feedback for a three-phase input and single-phase output Matrix Converter (3-1MC). A small non-polar capacitor is employed as the decoupling unit. The composite voltage weighted by the load voltage and the decoupling unit voltage is used as the feedback value for the voltage controller. Together with the current loop, the dual-loop control is implemented in the 3-1MC. In this paper, the weighted composite voltage expression is derived based on the sinusoidal pulse-width modulation (SPWM) strategy. The switch functions of the 3-1MC are deduced, and the average signal model and small signal model are built. Furthermore, the stability and dynamic performance of the 3-1MC are studied, and simulation and experiment studies are executed. The results show that the control method is effective and feasible. They also show that the design is reasonable and that the operating performance of the 3-1MC is good.

Analytical Proof of Equivalence of ISF, and Floquet Vector-Based Oscillator Phase Noise Theories (ISF와 Floquet 벡터에 기초한 발진기 위상잡음 이론의 등가성에 대한 해석적 증명)

  • Jeon, Man-Young
    • Journal of IKEEE
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    • v.17 no.4
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    • pp.559-563
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    • 2013
  • This paper analytically proves the equivalence between two main oscillator phase noise theories, which are based on the ISF, and Floquet vector, respectively. For this purpose, this study obtains the power spectral density matrix from the ISF-based phase noise theory. As a result, one can prove that the power spectral density matrix obtained from the ISF-based phase noise theory is essentially equivalent to the power spectral density matrix presented by the Floquet vector-based phase noise theory, which manifests the equivalence of the two main theories. This study is intended to provide deeper insight into the relations between the two main theories.

Study on the Sintering, Repressing and Mechanical Properties of Al2O3 and Al-Cu-SiC Composites (Al2O3와 SiC 강화재가 첨가된 Al-Cu 기지 복합재료의 소결, 재압축 및 기계적 특성에 관한 연구)

  • 박정수;이성규;안재환;정형식
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.171-178
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    • 2004
  • Effects of liquid phase and reinforcing particle morphology on the sintering of Al-6 wt%Cu-10 vol% $Al_2O_3$ or SiC particles were studied in regards to densification, structure and transverse rupture properties. The Al-Cu liquid phase penetrated the boundaries between the aluminum matrix powders and the interfaces with reinforcing particles as well, indicating a good wettability to the powders. This enhanced the densification during sintering and the resulting strength and ductility. Since most of the copper added, however, was dissolved in the liquid phase and formed a brittle $CuAl_2$ phase upon cooling rather than alloyed with the aluminum matrix, the strengthening effect by the copper was not fully realized. Reinforcing particles of agglomerate type were found less suitable for the liquid phase sintering than solid type particles. $Al_2O_3$ and SiC particles protluced little difference on the sintering behavior but their size had a large effect. Repressing of the sintered composites increased density and bending properties but caused debonding at the matrix-particle interfaces and also fracturing of the particles.

Crystal Structure and Morphology of Nitride Precipitates in TiAl (TiAl에 석출한 질화물의 결정구조와 형태)

  • Han, Chang-Suk;Koo, Kyung-Wan
    • Korean Journal of Materials Research
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    • v.18 no.1
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    • pp.51-56
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    • 2008
  • The crystal structures and morphologies of precipitates in $L1_0$-ordered TiAl intermetallics containing nitrogen were investigated by transmission electron microscopy (TEM). Under aging at an approximate temperature of 1073 K after quenching from 1423 K, TiAl hardens appreciably due to the nitride precipitation. TEM observations revealed that needle-like precipitates, which lie only in one direction parallel to the [001] axis of the $L1_0$-TiAl matrix, appear in the matrix preferentially at the dislocations. Selected area electron diffraction (SAED) pattern analyses showed that the needle-shaped precipitate is perovskite-type $Ti_3AlN$ (P-phase). The orientation relationship between the P-phase and the $L1_0$-TiAl matrix was found to be $(001)_P//(001)_{TiAl}\;and\;[010]_P//[010]_{TiAl}$. By aging at higher temperatures or for longer periods at 1073 K, plate-like precipitates of $Ti_2AlN$ (H-phase) with a hexagonal structure formed on the {111} planes of the $L1_0$-TiAl matrix. The orientation relationship between the $Ti_2AlN$ and the $L1_0$-TiAl matrix is $(0001)_H//(111)_{TiAl}\;and\;_H//_{TiAl}$.