• Title/Summary/Keyword: Materials characterization

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Review of Electrical Characterization of Ceramic Thin Films for the Next Generation Semiconductor Devices (차세대 반도체 소자용 세라믹 박막의 전기적 분석 방법 리뷰)

  • Lee, Donghyun;Yang, Kun;Park, Ju-Yong;Park, Min Hyuk
    • Ceramist
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    • v.22 no.4
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    • pp.332-349
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    • 2019
  • Ceramic thin films are key materials for fundamental electronic devices such as transistors and capacitors which are highly important for the state-of-the-art electronic products. Their characteristic dielectric properties enable accurate control of current conduction through channel of transistors and stored charges in capacitor electrodes. The electronic conduction in ceramic thin films is one of the most important part to understand the electrical properties of electronic device based on ceramic thin films. There have been numerous papers dealing with the electronic conduction mechanisms in emerging ceramic thin films for future electronic devices, but these studies have been rarely reviewed. Another interesting electrical characterization technique is one based on electrical pulses and following transient responses, which can be used to examine physical and chemical changes in ceramic thin films. In this review, studies on various conduction mechanisms through ceramic thin films and electrical characterization based on electric pulses are comprehensively reviewed.

Transparent Ceramics for Visible/IR Windows: Processing, Materials and Characterization

  • Jung, Wook Ki;Ma, Ho Jin;Kim, Ha-Neul;Kim, Do Kyung
    • Korean Journal of Materials Research
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    • v.28 no.10
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    • pp.551-563
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    • 2018
  • Visible and IR windows require a combination of high optical transparency and superior thermal and mechanical properties. Materials, fabrication and characterization of transparent ceramics for visible/IR windows are discussed in this review. The transparent polycrystalline $Y_2O_3$, $Y_2O_3-MgO$ nanocomposites and $MgAl_2O_4$ spinel ceramics are fabricated by advanced ceramic processing and the use of special sintering technologies. Ceramic processing conditions for achieveing fully densified transparent ceramics are strongly dependent on the initial powder characteristics. In addition, appropriate use of sintering technologies, including vacuum sintering, hot-pressing and spark plasama sintering methods, results in outstanding thermal and mechanical properties as well as high optical transparency of the final products. Specifically, the elimination of light scattering factors, including residual pores, second phases and grain boundaries, is a key technique for improving the characteristics of the transparent ceramics. This paper discusses the current research issues related to synthesis methods and sintering processes for yttria-based transparent ceramics and $MgAl_2O_4$ spinel.

Development of Piezoelectric Transducers For Measuring Dynamic Stiffness of Subsurface Materials (지반의 동적 물성치 측정을 위한 압전소자형 계측기 개발)

  • 목영진
    • Proceedings of the Earthquake Engineering Society of Korea Conference
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    • 1997.10a
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    • pp.101-108
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    • 1997
  • A pair of piezoelectric transducers was developed for geotechnical site characterization in rock materials. SH-wave measurement capability of the transducers can provide a more complete characterization. The performance of the transducers was tested at a limestone site.

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Materials Characterization and the Microstructure of Pure Cu and Cu-3vol%CNT Composite Fabricated From Optimization of SPS Processing Variables (SPS 공정 변수의 최적화에 의한 Pure Cu와 Cu-3vol%CNT composite의 미세구조와 소재특성)

  • Lee, Hee Chang;Kim, Hye Sung
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.4
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    • pp.185-192
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    • 2020
  • In this study, materials characterization of pure copper and copper based carbon nano-tube composite prepared by powder metallurgy method were investigated. Prior to evaluate materials characterization, spark plasma sintering processing variables such as sintering temperature, pressure, thickness and diameter of compacts was optimized to ensure the microstructure and materials property of pure Cu and Cu-CNT composite. In addition, corrosion behavior of Cu-based CNT composite produced by powder sintering method was investigated. It was confirmed from this study that the corroded surfaces of the composite shows less dissolution compared with pure copper in 3.5 wt% NaCl solution. The measured corrosion current density (Icorr) indicates improved corrosion property of Cu based composite containing small additions of CNTs in chloride containing media. Micro-galvanic activity between Cu and CNT was not observed in given sintering condition.

Smart geophysical characterization of particulate materials in a laboratory

  • Kwon, Tae-Hyuk;Cho, Gye-Chun
    • Smart Structures and Systems
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    • v.1 no.2
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    • pp.217-233
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    • 2005
  • Elastic and electromagnetic waves can be used to gather important information about particulate materials. To facilitate smart geophysical characterization of particulate materials, their fundamental properties are discussed and experimental procedures are presented for both elastic and electromagnetic waves. The first application is related to the characterization of particulate materials using shear waves, concentrating on changes in effective stress during consolidation, multi-phase phenomena with relation to capillarity, and microscale characteristics of particles. The second application involves electromagnetic waves, focusing on stratigraphy detection in layered soils, estimation of void ratio and its spatial distribution, and conduction in unsaturated soils. Experimental results suggest that shear waves allow studying particle contact phenomena and the evolution of interparticle forces, while electromagnetic waves give insight into the characteristics of the fluid phase and its spatial distribution.

A Study on the Antibacterial Properties of Ag Electropulsed Anodized Aluminium Alloy (Pulse도금법에 의한 Ag주입 양극산화 알루미늄 합금의 항균특성에 관한 기초연구)

  • Lim, Ki-Young;Ki, Joon-Seo;Jang, Yong-Seok;Lee, Woo-Min;Yoon, Jeong-Mo
    • Korean Journal of Materials Research
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    • v.16 no.10
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    • pp.639-646
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    • 2006
  • Over the last two decades, microbiologically influenced corrosion (MIC) of metallic materials has received considerable attention due to its serious effects on industrial field. In this context, it is important to devise control methods which inhibit biofilm formation on various metallic compounds and are compatible with environment. It was change of various conditions (duty cycle, current density, $AgNO_3$ concentration and pH) for injection of Ag particles in anodized Aluminum alloy pore using pulsed current. Optimal condition was obtained by means of FE-SEM, ICP analysis etc. The antibacterial metal's specimen were manufactured under optimal condition and this specimen were tested the antibacterial characterization and anticorrosion characterization. In result of test, we can confirmed that the antibacterial characterization and anticorrosion characterization of the specimens of injected Ag particles in anodized Aluminum alloy pore using pulsed current were better than the anodized Aluminum alloy specimens.

Properties of Carbon Pastes Prepared with Mixing Ratios of Nano Carbon and Graphite Flakes

  • Kim, Kwangbae;Song, Ohsung
    • Korean Journal of Materials Research
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    • v.28 no.11
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    • pp.615-619
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    • 2018
  • To produce carbon electrodes for use in perovskite solar cells, electrode samples are prepared by mixing various weight ratios of 35 nm nano carbon(NC) and $1{\mu}m$ graphite flakes(GF), GF/(NC+GF) = 0, 0.5, 0.7, and 1, in chlorobenzene(CB) solvent with a $ZrO_2$ binder. The carbon electrodes are fabricated as glass/FTO/carbon electrode devices for microstructure characterization using transmission electron microscopy, optical microscopy, and a field emission scanning electron microscopy. The electrical characterization is performed with a four-point probe and a multi tester. The microstructure characterization shows that an electrode with excellent attachment to the substrate and no surface cracks at weight ratios above 0.5. The electrical characterization results show that the sheet resistance is <$70{\Omega}/sq$ and the interface resistance is <$70{\Omega}$ at weight ratios of 0.5 and 0.7. Therefore, a carbon paste electrode with microstructure and electrical properties similar to those of commercial carbon electrodes is proposed with an appropriate mixing ratio of NC and GF containing a CB solvent and $ZrO_2$.

Effects of Temperature and Precursor-concentration on Characteristics of TiO2 Nanoparticles in Chemical Vapor Condensation Process -Part I: Real-time Particle Characterization by SMPS (화학기상응축 공정에서 TiO2 나노입자 특성에 미치는 반응온도와 전구체 농도의 영향 - Part I: SMPS를 이용한 실시간 입자특성 평가)

  • Lee, Chang-Woo;Yu, Ji-Hun;Im, Sung-Soon;Yun, Sung-Hee;Lee, Jai-Sung;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • v.13 no.5
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    • pp.323-327
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    • 2003
  • Properties of nanoparticles synthesized during gas phase reaction were studied in terms of particle behaviors using real-time particle characterization method. For this study, $TiO_2$ nanoparticles were synthesized in the chemical vapor condensation process(CVC) and their in-situ measurement of particle formation and particle size distribution was performed by scanning mobility particle sizer(SMPS). As a result, particle behaviors in the CVC reactor were affected by both of number concentration and thermal coagulation, simultaneously. Particularly, growth and agglomeration between nanoparticles followed two different ways of dominances from coagulations by increase of number concentration and sintering effect by increased temperature.