• Journal of Microbiology and Biotechnology
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• v.23 no.7
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• pp.942-952
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• 2013

Monoliths are functional porous materials with a three-dimensional continuous interconnected pore structure in a single piece. A monolith with uniform shape based on poly(${\gamma}$-glutamic acid) (PGA) has been prepared via a thermally induced phase separation technique using a mixture of dimethyl sulfoxide, water, and ethanol as solvent. The morphology of the obtained monolith was observed by scanning electron microscopy and the surface area of the monolith was evaluated by the Brunauer Emmett Teller method. The effects of fabrication parameters such as the concentration and molecular mass of PGA and the solvent composition have been systematically investigated. The PGA monolith was cross-linked with hexamethylene diisocyanate to produce the water-insoluble monolith. The addition of sodium chloride to the phase separation solvent affected the properties of the cross-linked monolith. The swelling ratio of the cross-linked monolith toward aqueous solutions depended on the buffer pH as well as the monolith fabrication condition. Copper(II) ion was efficiently adsorbed on the cross-linked PGA monolith, and the obtained copper-immobilized monolith showed strong antibacterial activity for Escherichia coli. By combination of the characteristic properties of PGA (e.g., high biocompatibility and biodegradability) and the unique features of monoliths (e.g., through-pore structure, large surface area, and high porosity with small pore size), the PGA monolith possesses large potentials for various industrial applications in the biomedical, environmental, analytical, and separation fields.

• Resources Recycling
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• v.30 no.5
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• pp.17-24
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• 2021

Natural aggregate regular exploitation has led to environmental and resource depletion issues; consequently, construction waste has become an important raw material in the supply of aggregate smoothly. The recycled aggregate produced in the most of recycled aggregate processing company in Korea has a high adhesion ratio of cement paste and mortar, which affects the water absorption ratio and density. Therefore, the quality of recycled aggregate needs to be improved. In this study, we improved the quality of recycled aggregate through the use of a multistage separation ball mill. This ball mill has a sieve which protects the ball mix and improves the motion. Products produced by using multistage separation ball mill were compared with various quality standard for utilization as recycle aggregate. Finally, we confirmed that the multistage separation ball mill can efficiently separate cement paste and mortar from natural aggregate and that it is suitable for the production of recycled aggregates.

• Korean Journal of Materials Research
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• v.29 no.11
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• pp.703-708
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• 2019

In this study, we investigate the relationship between the peeling behavior of the backsheet of a photovoltaic(PV) module and its surface temperature in order facilitate removal of the backsheet from the PV module. At low temperatures, the backsheet does not peel off whereas, at high temperatures, part of the backsheet remains on the surface of the PV module after the peeling process. The backsheet material remaining on the surface of the PV module is confirmed by X-ray diffraction(XRD) analysis to be poly-ethylene(PE). Differential scanning calorimetry(DSC) is also performed to investigate the interfacial characteristics of the layers of the PV module. In particular, DSC provides the melting temperature($T_m$) of laminated ethylene vinyl acetate(EVA) and of the backsheet on the PV module. It is found that the backsheet does not peel off below the $T_m$ of ethylene of EVA, while the PE layer of the backsheet remains on the surface of the PV module above the $T_m$ of the PE. Thus, the backsheet is best removed at a temperature between the $T_m$ of ethylene and that of PE layer.

• Analytical Science and Technology
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• v.33 no.6
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• pp.245-251
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• 2020

Lead (Pb) has been shown to be a useful tracer of contamination sources and geochemical processes such as age dating and crustal evolution. These studies require a chromatographic technique for Pb separation from geological samples. This paper presents a comparison study on the effect of eluent concentration between 6M HCl and 8M HCl on the separation of Pb from Pb resin. The results showed that the separation of Pb using 6M HCl as the eluent was not effective compared to the separation using 8M HCl. To verify this method, we measured the Pb isotopic compositions of the Pb isotopic standard (NIST NBS981) and geological reference materials (BCR-2, GSP-2, and JG-1a) using a thermal ionization mass spectrometer (TIMS). The results correspond well with the reported values within the error range, implying that this method can be useful.

• Membrane Journal
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• v.31 no.6
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• pp.426-433
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• 2021

In this study, a novel material polyketone (PK) was chosen and PK micro/nano fiber membranes were fabricated via electrospinning method under various conditions. After that, the potential application in oil-water separation was thoroughly investigated. The surface of microfiber membrane formed under high humidity especially became much rougher than that formed under low humidity. When salt was added to the spinning solution, the diameter of fibers was reduced up to 90% and the nanofiber membranes could be formed. The oil/water emulsions were prepared and separated under gravity condition using the manufactured rPK-LNC and PK-H membranes. The separation characteristics was evaluated by measuring total organic carbon (TOC) and turbidity. Meanwhile, the changes in the physical properties of fiber membranes under various conditions and with or without salt, as well as the changes in oil water separation characteristics were also studied.

• Transactions of the Korean Society of Mechanical Engineers
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• v.17 no.5
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• pp.1106-1114
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• 1993

A composite material is composed of a reinforcement and a matrix, which determine mechanical characteristics of the molded part. There is no doubt that the properties of a composite material depend not only on the characteristics of the matrix but also on the structure of glass fiber mat and a fiber type of reinforcement. Therefore it is very important to study the composites of reinforcement and the matrix, and to control the fiber type in the process of molding of composite materials. In this study, the specimen was made of a glass fiber mat of 6-7mm thickness by scattering it in the air after cutting the glass fiber mat with needle punching makes change according to the type of needle and the number of times of stretching. First the sheet was made by means of a hot-press after accumulating a matrix and a glass fiber according to each mat structure of glass fiber. It was heated the manufactured sheet with the dry oven and molded it a secondary high temperature compression by a 30 ton oilhydraulic press. A definition of a correlation coefficient is showed up during this period and find it out with the relation of the fiber-matrix separation and the fiber orientation. We studied effects of the glass fiber mat structures on the correlation coefficient.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.06a
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• pp.342-343
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• 2009

Paper factories use a large amount of water and same amount of wastewater is generated. It is important to purity and recycle the wastewater because of water shortages and water pollution. The existing water treatment facilities like precipitation process need large-scale equipment and wide space to purity the wastewater of paper factory. High gradient magnetic separation (HGMS) system has the merits to purity rapidly because of large voids at filter and to occupy small space. In this paper, two types of superconducting magnets were used for HGMS systems. Cryo-cooled Bi-2223 superconducting magnet system with 70 mm room temperature bore and 200 mm of height was prepared. Cryo-cooled Nb-Ti superconducting magnet with 100 mm room temperature bore and 600 mm of height was used for magnetic separator. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets. The various magnetic seeding reactions were investigated to increase the reactivity of coagulation. The effects of magnetic separation of wastewater were investigated as variation of magnetic field strength and flow rate of wastewater.

• The Journal of Advanced Prosthodontics
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• v.2 no.3
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• pp.102-105
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• 2010

PURPOSE. The aims of this study were to suggest a method of fabrication of the record base using a light-polymerized resin by applying the two-phase fabrication method for the improvement of the fit of the record base and to compare the degree of fit according to the separation site. MATERIALS AND METHODS. In the edentulous cast of maxilla, four test groups were considered. In the first, second, third, and fourth test groups (n = 12 in each group) the separation was done at 0, 5, 10, and 15 mm, respectively below the alveolar crest along the palatal plane. For the control group, the record base was made without separating the two sections. The light-body silicone material was injected into the fitting surface of the record base. It was then placed onto the cast and finger pressure was applied to stabilize it in a seated position followed by immediate placement onto the universal test device. Finally, the mass of the impression material was measured after it was removed. ANOVA was performed using the SAS program. For the post-hoc test, the Wilcoxon Rank-Sum test and the Tukey-Kramer HSD test were performed ($\alpha$ = 0.05). RESULTS. The control group and Group 3, 4 showed significant differences. The Group 3 and 4 showed significantly smaller inside gaps than the control group which was not made with the two-phase fabrication method. CONCLUSION. The two-stage polymerized technique can improve the fit of the denture base particularly when the separation was made at 10 to 15 mm from the alveolar crest.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.05a
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• pp.4-4
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• 2009

Paper factories use a large amount of water and same amount of wastewater is generated. It is important to recycle the wastewater because of water shortages and water pollution. The existing water treatment facilities like precipitation process need large-scale equipment and wide space to purify the wastewater of paper factory. High gradient magnetic separation (HGMS) system has the merits to purify rapidly because of large voids at filter and to occupy small space. In this paper, two types of superconducting magnets were used for HGMS systems. Cryo-cooled Bi-2223 superconducting magnet system with 70 mm room temperature bore and 200 mm of height was prepared. Cryo-cooled Nb-Ti superconducting magnet with 100 mm room temperature bore and 600 mm of height was used for magnetic separator. Magnetic filters were designed by the analysis of magnetic field distribution at superconducting magnets. The various magnetic seeding reactions were investigated to increase the reactivity of coagulation. The effects of magnetic separation of wastewater were investigated as variation of magnetic field strength and flow rate of wastewater.

• Resources Recycling
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• v.18 no.3
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• pp.27-35
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• 2009

To solve resource exhaustion and waste management problems caused by mass consumption, there are many efforts to change from resource consumption system to recycling system. Specially, interests about management of construction waste have increased, but efficient recycling system of waste concrete is not established yet. In this study, high quality recycled aggregate processing circuit was developed to recycle waste concrete. From the waste concrete which is a hydrated compound with coarse aggregate, fine aggregate, and cement material, high quality recycled coarse aggregate for concrete making was produced by autogenous milling and heat pretreatment method. After then, refinement process was performed to separate fine aggregate and cement material from waste concrete fines by sink float separation and hindered-settling separation. As a result, high quality recycled aggregate was produced from waste concrete by developed processing circuit.